A method for nitrous decomposition can include: expanding liquid nitrous into gaseous nitrous in a decomposition chamber; injecting heated nitrogen gas into the decomposition chamber so as to mix with the gaseous nitrous, wherein the heated nitrogen gas is at a nitrous decomposition temperature; heating the gaseous nitrous with the heated nitrogen gas to the nitrous decomposition temperature; and decomposing the gaseous nitrous into nitrogen and oxygen. The method can include: heating the nitrogen to at least the nitrous decomposition temperature; heating the liquid nitrous prior to expansion into the decomposition chamber; and performing the decomposition without a catalyst or heating element in the decomposition chamber. A swirling device can be positioned at an inlet to the decomposition chamber. A swirling nozzle can be positioned at an inlet to the decomposition chamber.

The disclosure provides a reaction kettle, a polypeptide synthesis cleavage system and their use in polypeptide synthesis or cleavage. The reaction kettle comprises: (1) a kettle body; (2) a stirring device located at the upper part of the kettle body and extending to the interior of the kettle body; (3) a liquid feed port, a solid feed port, an inert gas inlet and an inert gas outlet located at the upper part of the kettle body; (4) a liquid discharge port and a liquid guiding groove at the bottom of the kettle body, wherein the liquid discharge port is located at the lowest point of the liquid guiding groove; (5) a filtering device located above the liquid guiding groove; (6) a solid discharge portpassing through the bottom of the kettle body and the filtering device; and (7) a discharge valve configured at the solid discharge port.

The invention generally relates to systems and methods for increasing reaction yield. In certain embodiments, the invention provides systems for increasing a yield of a chemical reaction that include a pneumatic sprayer configured to generate a liquid spray discharge from a solvent. The solvent includes a plurality of molecules, a portion of which react with each other within the liquid spray discharge to form a reaction product. The system also includes a collector positioned to receive the liquid spray discharge including the unreacted molecules and the reaction product. The system also includes a recirculation loop connected from the collector to the pneumatic sprayer in order to allow the unreacted molecules and the reaction product to be recycled through the pneumatic sprayer, thereby allowing a plurality of the unreacted molecules to react with each other as the unreacted molecules cycle again through the system.

Injection device (56) for discharging a gas (54), in particular a process gas (54), onto a material (12), in particular onto a battery cathode material (14) that is to be calcined, having at least one inlet (58) through which the gas (54) can be supplied to the injection device (56), and at least one outlet (60) through which the gas (54) can be discharged from the injection device (56), the inlet and outlet being connected to one another by a flow path (62) for the gas (54). According to the invention, the flow path (62) has a heat exchanger (64) with a heat exchanger housing (68) which is accessible from the outside for an ambient atmosphere (66) and in which a duct arrangement (70) is integrated. The duct arrangement (70) comprises a first flow duct (72.1) and a second flow duct (72.2) between which there is formed a redirection region (74.1) such that the gas (54) can flow through the first and second flow duct (72.1, 72.2) in different main flow directions. The invention further relates to a process gas system (52) for supplying a gas (54) and to a device (10) and a method for the thermal or thermo-chemical treatment of material.

A vessel for the downflow of a preferably hydrocarbon liquid, containing solid particles: a bottom comprising a cylindrical upper part (11), a lower part (12) with a decreasing cross section and a varying angle of inclination α with respect to the vertical axis (Z), and an outlet pipe (9); injections (5) and (6) of recirculated and/or of makeup liquid into the lower and upper parts respectively; injections (5) inclined with respect to the tangent to the wall of the lower part at the injection point by an angle β1 in the vertical plane (xz) and by an angle β2 in the horizontal plane (xy); injections (6) are inclined with respect to the wall of the upper part by an angle θ1 in the vertical plane (xz) and by an angle θ2 in the horizontal plane (xy).

A method for making a solid carbon material comprises: delivering a liquid comprising at least one liquid organic compound into a reaction region of a reactor; delivering a gas comprising at least one gaseous organic compound into the reaction region of the reactor; and inducing a chemical reaction between the at least one liquid organic compound and the at least one gaseous organic compound, wherein: the chemical reaction occurs in the reaction region of the reactor; the solid carbon material is made via the reaction; the solid carbon material is made during the reaction in the form of a dispersion comprising the solid carbon material dispersed in the liquid; and the chemical reaction is a homogeneous reaction comprising homogeneous nucleation of the solid carbon material in the reaction region of the reactor.

The steam saving device for a steam explosion system for the hydrothermal pre-treatment of biomass comprises a tubular body 30 with a first open end 32 and a second open end 34. The first open end 32 being adapted to be coupled to an outlet opening 14 of a steam explosion reactor vessel 10, the second open end 34 being adapted to be coupled to a discharge line 18. The inner surface 36 of the tubular body 30 of the nozzle 16 may comprise an engraved helical structure 38.

A hydroformylation system for making aldehydes includes: (a) a primary reactor provided with catalyst feed, syngas feed and olefin feed adapted to convert the olefin and syngas to product aldehyde; (b) a first liquid vapor separator coupled to the primary reactor for receiving output therefrom, adapted to separate the product aldehyde into a crude aldehyde product stream and a vent stream containing syngas and unreacted olefin; (c) a vent reactor coupled to the first liquid vapor separator to receive the vent stream therefrom, the vent reactor also being coupled to the primary reactor which is configured to provide catalyst thereto, wherein the vent reactor is operative to convert unreacted olefin in the vent stream from the first liquid vapor separator to additional product aldehyde. A second liquid vapor separator is coupled to the vent reactor to receive output therefrom and adapted to separate the output from the vent reactor into a liquid recycle stream containing additional product aldehyde and catalyst as well as another vent stream, the second liquid vapor separator also being coupled to the primary reactor so as to provide the recycle stream thereto.

The invention relates to a device (D) for distributing a fluid, which is able to be arranged in a fixed catalytic bed (C.sub.1, C.sub.2) of a reactor (R), said device comprising conveying means for conveying said fluid, comprising a plurality of pipes each directly receiving a distinct share of said fluid, distribution means for distributing said fluid, means for generating a local pressure drop in said fluid, such that: the device comprises manifold means (2a) for collecting said fluid together, and providing the fluidic connection between the pipes of said fluid conveying means and said fluid distribution means, said means for generating a local pressure drop are added on to said conveying or distribution or manifold (2a) means.

Gas injectors for providing uniform flow of fluid are provided herein. The gas injector includes a plenum body. The plenum body includes a recess, a protrusion adjacent to the recess and extending laterally away from the plenum body, and a plurality of nozzles extending laterally from an exterior surface of the plenum body. The plenum body has a plurality of holes in an exterior wall of the plenum body. Each nozzle is in fluid communication with an interior volume of the plenum body. By directing the flow of fluid, the gas injector provides for a uniform deposition.