B01J4/004

Method and system for distributing liquid in (meth)acrylic monomer process vessels

A method for uniformly distributing a process liquid within a process vessel includes providing a process liquid to a fouling-resistant liquid distributor installed within a process vessel having a cross-sectional area; causing rotational movement of the fouling-resistant liquid distributor; uniformly distributing the process liquid over the cross-sectional area within the process vessel; and simultaneously self-rinsing the fouling-resistant liquid distributor with a portion of the process liquid during uniform distribution. A system is also disclosed which includes a supply of process fluid, a stationary conduit and a liquid distribution head attached to the conduit. The liquid distribution head is motive, powered by a fluid, and includes at least one process liquid delivery port. The at least one process liquid delivery port is configured to provide a +10 or greater angle of liquid coverage when the liquid distribution head is moving.

Wet disperser

Embodiments provide a wet disperser for dispersing particulates in a mixture containing at least a dispersing medium and particulates. According to various embodiments, the wet disperser includes a through channel extending from an inflow port to an outflow port, and a mixture-passing plate having at least one passing hole defined. In the wet disperser, the through channel includes, on a downstream side of the through channel from a position provided with the mixture-passing plate, a dispersion part having a vibration body provided such that vibration causes at least a part of the vibration body to come into contact with at least a part of an opening periphery of the passing hole, and an inside surface defining the passing hole of the mixture-passing plate.

Design of an Ethylene Oligomerization/Trimerization/Tetramerization Reactor
20200071243 · 2020-03-05 ·

A process includes periodically or continuously introducing an olefin monomer and periodically or continuously introducing a catalyst system or catalyst system components into a reaction mixture within a reaction system, oligomerizing the olefin monomer within the reaction mixture to form an oligomer product, and periodically or continuously discharging a reaction system effluent comprising the oligomer product from the reaction system. The reaction system includes a total reaction mixture volume and a heat exchanged portion of the reaction system comprising a heat exchanged reaction mixture volume and a total heat exchanged surface area providing indirect contact between the reaction mixture and a heat exchange medium. A ratio of the total heat exchanged surface area to the total reaction mixture volume within the reaction system is in a range from 0.75 in.sup.1 to 5 in.sup.1, and an oligomer product discharge rate from the reaction system is between 1.0 (lb)(hr.sup.1)(gal.sup.1) to 6.0 (lb)(hr.sup.1)(gal.sup.1).

SYSTEMS AND PROCESSES FOR MOLTEN MEDIA PYROLYSIS

Systems and methods for molten media pyrolysis for the conversion of methane into hydrogen and carbon-containing particles are disclosed. The systems and methods include the introduction of seed particles into the molten media to facilitate the growth of larger, more manageable carbon-containing particles. Additionally or alternatively, the systems and methods can include increasing the residence time of carbon-containing particles within the molten media to facilitate the growth of larger carbon-containing particles.

SYSTEMS AND PROCESSES FOR MOLTEN MEDIA PYROLYSIS

Systems and methods for molten media pyrolysis for the conversion of methane into hydrogen and carbon-containing particles are disclosed. The systems and methods include the introduction of seed particles into the molten media to facilitate the growth of larger, more manageable carbon-containing particles. Additionally or alternatively, the systems and methods can include increasing the residence time of carbon-containing particles within the molten media to facilitate the growth of larger carbon-containing particles.

FLUID DISTRIBUTION SYSTEM FOR A REACTOR VESSEL
20200055008 · 2020-02-20 ·

A fluid distribution system (208) is provided for a reactor vessel (200) defining a reaction chamber (202). The fluid distribution system (208) may include a radial distribution component (224) positionable within the reaction chamber (202) and adjacent a vessel inlet (212) at an end portion of the reactor vessel (200). The radial distribution component (224) may include one or more annular distribution conduits (230) configured to receive a fluid mixture provided to the reactor vessel (200). The fluid distribution system (208) may also include an axial distribution component (226) positionable within the reaction chamber (202) to extend from the radial distribution component (224) along a longitudinal axis of the reactor vessel (200). The axial distribution component (230) may include a plurality of helical conduits (236) fluidly coupled with the one or more annular distribution conduits (230) and configured to receive the fluid mixture from the one or more annular distribution conduits (230) and to disperse the fuel mixture uniformly within the reaction chamber (202).

Method for producing dihydroxy compounds

The invention is directed to the use of an upflow reactor for producing a dihydroxy compound, to a method for producing a dihydroxy compound, and to a method for manufacturing polycarbonate. The upflow reactor for producing a dihydroxy compound of the invention comprises: a vessel; a catalyst bed disposed in said vessel; a distributor in fluid communication with an inlet through which reactants are introduced to said distributor, said distributor being disposed at a lower end of said vessel and comprising distributor perforation(s) disposed in said distributor, at least part of which distributor perforations are in a direction facing away from said catalyst bed; and a collector through which said product dihydroxy compound is removed, said collector being disposed at an upper end of said vessel.

SPARGE FOR A HIGH-PRESSURE VESSEL
20200001259 · 2020-01-02 · ·

A sparge for use in a high-pressure vessel operated at elevated temperatures and having high energy agitators for suspending mineral containing particles in a slurry. The sparge injects reagent fluids into the slurry to reduce reaction times and for controlling process parameters for extracting valuable minerals from the particles. The sparge has a vapour lock to inhibit the flow of particulate material and detritus material under low or no fluid flow situations which occur commonly in the operation of high pressure autoclaves. The sparge has a fluid flow path that increases in cross-sectional area in the direction of flow of reagent fluids so as to keep reagent fluids flowing at a velocity below a critical impingement velocity that can cause metal materials of the sparge to either wear rapidly, combust and in the worst case lead to loss of containment and violent and rapid depressurisation of the highpressure vessel.

Systems and methods for periodic nodal surface based reactors, distributors, contactors and heat exchangers

The present disclosure relates to a transport mechanism apparatus for transporting at least one of a gas or a fluid. The transport mechanism may have an inlet, an outlet and an engineered cellular structure forming a periodic nodal surface, which may include a triply periodic minimal surface (TPMS) structure. The structure is formed in a layer-by-layer three dimensional (3D) printing operation to include cells propagating in three dimensions, where the cells include non-intersecting, continuously curving wall portions having openings, and where the opening in the cells form a plurality of flow paths throughout the transport mechanism from the inlet to the outlet, and where portions of the cells form the inlet and the outlet.

Apparatus for preparing oligomer

The present disclosure relates to an apparatus for preparing an oligomer, the apparatus including: a reactor for oligomerizing a feed stream containing a fed monomer; a stirrer inserted into a hole formed in an upper portion of the reactor; and a solvent transfer line extending inward from a side of the reactor, wherein the stirrer includes a rotating shaft vertically extending downward from the upper portion of the reactor, and a blade having a conical shape whose vertex is positioned at a lower end of the rotating shaft and outer diameter increases from a bottom toward a top, and the solvent transfer line has a plurality of spray nozzles formed in a direction toward the blade.