B01J4/004

WET DISPERSER

Embodiments provide a wet disperser for dispersing particulates in a mixture containing at least a dispersing medium and particulates. According to various embodiments, the wet disperser includes a through channel extending from an inflow port to an outflow port, and a mixture-passing plate having at least one passing hole defined. In the wet disperser, the through channel includes, on a downstream side of the through channel from a position provided with the mixture-passing plate, a dispersion part having a vibration body provided such that vibration causes at least a part of the vibration body to come into contact with at least a part of an opening periphery of the passing hole, and an inside surface defining the passing hole of the mixture-passing plate.

Alkylbenzene hydroperoxide production using dispersed bubbles of oxygen containing gas

An apparatus for oxidation of a C.sub.8-C.sub.12alkylbenzene reactant to a C.sub.8-C.sub.12 alkylbenzene hydroperoxide product, the re-actor can comprise: a flow reactor comprising a reactant inlet, an oxidate product outlet, wherein the reactor is configured to provide a liquid flow from the reactant inlet to the product outlet, a gas inlet configured to introduce an oxygen-containing gas into the reactor, and an inlet sparger configured to flow gas bubbles comprising the oxygen-containing gas within the liquid flow, and wherein: the inlet sparger is configured to flow the gas bubbles having a diameter of 1.0 mm to 5.0 mm over a gas bubble residence time from 1 to 200 seconds, and/or the inlet sparger configured to flow the gas bubbles such that greater than or equal to 80% of the gas bubbles do not coalesce into larger bubbles over a gas bubble residence time of 1 to 200 seconds.

System and Method for Preparing Alkali Metal Salt Emulsifying Agents
20180186641 · 2018-07-05 ·

A system and method combine a first reactant with a second reactant to create a reaction product. A first pump is in fluid communication with a reaction vessel and a source of the first reactant. A second pump is in fluid communication with the reaction vessel and a source of the second reactant. A gas sparger is located in the reaction vessel, and the gas sparger is in fluid communication with a gas source for providing gas to the reaction vessel. A controller is configured to execute a program stored in the controller to: (i) receive a sensor signal based on a force exerted by the reaction vessel in a direction toward the sensor, and (ii) operate the first pump and the second pump to deliver to the reaction vessel the first reactant and the second reactant thereby causing a reaction that creates the reaction product.

Hydrogen generator having reactant pellet with concentration gradient

A hydrogen generator is provided for generating hydrogen gas for a fuel cell stack. The hydrogen generator includes a container, and a liquid reactant storage area configured to contain a liquid including a first reactant. The hydrogen generator also includes a reaction area within the container, and a solid containing a second reactant within the reaction area and having a concentration gradient that varies along an axis such as length of the solid. The hydrogen generator further includes a liquid delivery member for delivering the liquid to the solid in the reaction area to generate hydrogen. The concentration gradient controls a reaction rate of the first and second reactants.

Process and Reactor System for Oxidizing Cycloalkylbenzene
20180148406 · 2018-05-31 ·

Disclosed are processes and systems for oxidizing cycloalkylbenzene such as cyclohexylbenzene to make an oxygenate such as a hydroperoxide thereof. A liquid distributor having multiple liquid ingress ports is used for supplying a cycloalkylbenzene-containing liquid into an oxidation reactor in the form of liquid streams forming part of the reaction medium. A gas distributor distributing an O.sub.2-containing gas into the reaction medium in the form of gas streams is preferably located below the liquid distributor. Preferably the gas bubbles upwards in the reaction medium. The agitation and mixing provided by the liquid streams, gas streams/bubbles result in sufficient homogeneity of cycloalkylbenzene concentration, cycloalkylbenzene hydroperoxide concentration, dissolved oxygen concentration, and temperature in the liquid phase.

Continuous reaction apparatus and apparatus for producing a toner
09983492 · 2018-05-29 · ·

Provided is a continuous reaction apparatus which can precisely control the path of flow of the liquid reaction mixture in the reaction vessel. Further, provided is a continuous reaction apparatus which can efficiently mix the liquid reaction mixture in the reaction vessel. The continuous reaction apparatus comprises a plurality of mixing vessel units and a plurality of partition units. These units are connected in the state of being alternately stacked on one another. Each mixing vessel unit has an agitating blade disposed in the inner space thereof. The relationship between the inner diameter D1 of the mixing vessel unit, the height H of the mixing vessel unit, and the outer diameter d1 of the agitating blade satisfies the formula (1): 10(D1/H)1.5, and the formula (2): 0.99(d1/D1)0.7. The agitating blade is a circular disc-type agitating blade.

Gas Distribution in Oxidation Reactions
20180141018 · 2018-05-24 ·

Systems, methods, and apparatus for distribution of oxygen-containing gas within a gas-liquid oxidation reaction are provided herein. The invention is particularly suited for oxidation of liquid-phase organic reactants with oxidizing gas, such as the oxidation of cyclohexylbenzene to cyclohexylbenzene hydroperoxide using an oxygen-containing gas. The oxygen-containing gas is distributed through a gas distributor and into a liquid-phase reaction medium within an oxidation reactor. In some aspects, this achieves a high degree of uniformity of oxygen concentration within the liquid-phase reaction medium. The gas distributor is disposed within a lower portion of the reactor, and may comprise a network of conduits in fluid communication with each other, which are arranged within a plane that is substantially parallel to a bottom surface of the reactor. A plurality of orifices are disposed on the conduits, such that oxygen-containing gas flows through the conduits and into the liquid-phase reaction medium via the orifices.

Airlift Reactor Assembly with Helical Sieve Plate
20180119083 · 2018-05-03 ·

The present invention discloses an airlift reactor assembly with a helical sieve plate, comprising a reaction tank, wherein a draft tube and a gas sparger are assembled in the reaction tank, the gas sparger is arranged just below an riser section of the draft tube, a helical sieve plate is arranged in the riser section of the draft tube, and a body of the helical sieve plate is helical upwards to guide a part of two/three-phase flow in the riser section, and the body of the helical sieve plate is provided with a plurality of sieve meshes to guide the remaining two/three-phase go through the helical sieve plate in the riser section and to break bubbles. The present invention gives consideration to both macroscopic mixing and microscopic mixing processes. In addition to driving liquid to circularly flow by using ejected gas, the helical sieve plate can be used for breaking large bubbles into small bubbles thereby effectively preventing the bubbles from coalescing, increasing gas holdup and increasing a volumetric oxygen transfer coefficient.

Delivery device, methods of manufacture thereof and articles comprising the same

Disclosed herein is a delivery device comprising a chamber; a gas inlet; a gas outlet; and a dip tube contained within the chamber and having an upper portion and a lower portion, the upper portion of the dip tube being in fluid communication with the gas inlet and being operative to permit the entry of a carrier gas; the lower portion of the dip tube extending into the chamber, the lower portion of the dip tube terminating in an outlet end; and a sleeve; where the sleeve has a first end and a second end; the first end being in an interference fit with the lower portion of the dip tube; and where the sleeve vibrates upon being subjected to a disturbance.

Apparatus for introduction of droplets of a monomer solution into a reactor

An apparatus for introducing droplets of a monomer solution for production of poly(meth)acrylate into a reactor for droplet polymerization, comprising at least one channel or a dropletizer head, the channel or the dropletizer head being sealed at its base by a dropletizer plate, the dropletizer plate having holes through which the monomer solution is introduced into the reactor, and the dropletizer plate being configured such that holes that, in an axially symmetric dropletizer plate or in an annular dropletizer plate or in one configured as a ring segment, are not on a center line of the dropletizer plate or, in the case of a circular dropletizer plate, are not at the center of the dropletizer plate are aligned such that monomer solution is introduced through the holes into the reactor at an angle to the vertical, and the holes in the case of a radial alignment of axially symmetric dropletizer plates being aligned such that the angle at which the monomer solution is introduced into the reactor decreases in the direction of the axis of the reactor and, in the case of dropletizer plates arranged parallel to one another or of concentrically arranged dropletizer plates, each being aligned on a line parallel to the center line or line running concentrically about the center, such that the angle at which the monomer solution is introduced into the reactor is constant.