B01J4/004

Method and system for treatment of spent chloroaluminate ionic liquid catalyst and alkaline wastewater

A method and a system for treatment of a spent chloroaluminate ionic liquid catalyst and an alkaline wastewater, where the method includes: 1) mixing the catalyst with a concentrated brine for hydrolysis reaction until residual activity of the catalyst is completely eliminated, to obtain an acidic hydrolysate and an acid-soluble oil; 2) mixing the acidic hydrolysate with an alkaline solution containing the alkaline wastewater for neutralization reaction until this reaction system becomes weak alkaline, to obtain a neutralization solution; 3) fully mixing the neutralization solution with a flocculant, carrying out sedimentation and separation, collecting the concentrated brine at an upper layer for reuse in the hydrolysis reaction, and collecting concentrated flocs at a lower layer; 4) dehydrating the concentrated flocs to obtain concentrated brine for reuse into the hydrolysis reaction, and collecting a wet solid slag; and 5) drying the wet solid slag to obtain a dry solid slag.

Gas/liquid separation column containing a dispensing device

Gas/liquid separation column, containing a device for dispensing a liquid, intended for a gas/liquid separation column, comprising: a plate, in which several orifices are arranged, through which the liquid is able to leave the dispensing device; a plurality of stacks extending from the plate, each stack being configured to be followed by the gas; a plurality of plugging means respectively arranged at one end of one of the stacks, each plugging means having a gutter shape allowing a first portion of the liquid to be collected; a plurality of troughs for directly collecting a second portion of the liquid, at least one part of the orifices being distributed in the base of said troughs, each plugging means comprising a first open longitudinal end and a second closed longitudinal end.

DISTRIBUTION DEVICE COMPRISING A DISTRIBUTOR WITH POLYGONAL CHANNELS AND CONTACTING ASSEMBLY COMPRISING SUCH A DISTRIBUTION DEVICE

The invention relates to a distribution device having a container having side walls and a bottom with perforations; a distributor arranged beneath the container and provided with distribution channels that each have a polygonal cross-section; and mechanical connection bodies between the distributor and the linear elements, which extend beneath the distribution channels and fluidically connect the distribution channels to the linear elements when the distribution device is built into the contacting assembly.

Reverse-phase polymerisation process

A reverse-phase suspension polymerization process for the manufacture of polymer beads comprising forming aqueous monomer beads comprising an aqueous solution of water-soluble ethylenically unsaturated monomer or monomer blend and polymerizing the monomer or monomer blend to form polymer beads while suspended in a non-aqueous liquid, and recovering polymer beads, in which the process comprises, providing in a vessel (1) a volume (2) of non-aqueous liquid wherein the volume of non-aqueous liquid extends between at least one polymer bead discharge point (3) and at least one monomer feed point (4), feeding the aqueous monomer or monomer blend through orifices (5) into, or onto, the non-aqueous liquid to form aqueous monomer beads, allowing the aqueous monomer beads to flow towards the polymer bead discharge point subjecting the aqueous monomer beads to polymerization conditions to initiate polymerization to form polymerizing beads, wherein the polymerizing beads have formed polymer beads when they reach the polymer bead discharge point, removing a suspension of the polymer beads in non-aqueous liquid from the vessel at the polymer bead discharge point and recovering water soluble or water swellable polymer beads from the suspension. The invention also relates to the apparatus suitable for carrying out a reverse-phase suspension polymerization and polymer beads obtainable by the process or employing the apparatus.

DEVICE AND METHOD FOR OXIDIZING ORGANIC SUBSTANCE
20210402363 · 2021-12-30 ·

Disclosed are a device and method for oxidizing an organic substance, particularly a method for preparing ethylbenzene hydroperoxide by reacting ethylbenzene with an oxygen-containing gas. The device comprises a vertical bubbling reactor (1) and a horizontal bubbling reactor (11) connected to a reaction product outlet of the vertical bubbling reactor (1), wherein the horizontal bubbling reactor (11) is internally provided with a plurality of reaction compartments (21) which are arranged along the axial direction thereof, and a liquid phase channel (22) is provided between adjacent reaction compartments (21).

Oligomerization method using a reaction device comprising a dispersion means

The present invention relates to an oligomerization process using a reaction device comprising a dispersion means. In particular, the process relates to the oligomerization of ethylene to give linear α-olefins, such as 1-butene, 1-hexene or 1-octene, or a mixture of linear alpha-olefins.

GAS-SOLID CONTACTING DEVICE

A device for processing a flow of particulate material by contact with a gas flow includes a housing defining a processing chamber. This chamber includes a gas distribution plate having openings. The gas distribution plate separates a lower gas plenum from a solid-gas contact zone. The contact zone has at least one cylindrical partition upstanding from the gas distribution plate dividing an inner section from an adjacent annular outer section. The at least one partition is provided with a transfer opening for the particulate material. The housing is also provided with an inlet for supplying particulate material to the inner section and an outlet for discharging processed particulate material from the annular outer section.

In situ production and functionalization of carbon materials via gas-liquid mass transfer and uses thereof

A method for making a solid carbon material comprises: delivering a liquid comprising at least one liquid organic compound into a reaction region of a reactor; delivering a gas comprising at least one gaseous organic compound into the reaction region of the reactor; and inducing a chemical reaction between the at least one liquid organic compound and the at least one gaseous organic compound, wherein: the chemical reaction occurs in the reaction region of the reactor; the solid carbon material is made via the reaction; the solid carbon material is made during the reaction in the form of a dispersion comprising the solid carbon material dispersed in the liquid; and the chemical reaction is a homogeneous reaction comprising homogeneous nucleation of the solid carbon material in the reaction region of the reactor.

Process for multistage hydroprocessing in a single reactor

The present invention provides a multistage single reactor system for hydroprocessing and a process of carrying out multistage hydroprocessing in the said reactor assembly consisting of, a fixed bed solid catalyst system, a feed injection system enabling axial flow of hydrogen saturated hydrocarbon feed, a hydrogen dispensing system inside the reactor enabling minimum required hydrogen flow in cross-flow pattern, also using multitudes of integrated separation and withdrawal limbs for continuous staging. The innovative reactor disclosed in the present invention enables continuous separation and withdrawal of gaseous products along the reactor length by means of combined horizontal reactor orientation and vertical separation limbs provided at the top of the horizontally oriented reactor. The advantage of the reactor assembly includes effective heat sink of exothermic reactions and lower severity of operation due to removal of inhibitory gaseous products.

APPARATUS FOR PREPARING OLIGOMER

The present disclosure relates to an apparatus for preparing an oligomer, the apparatus including: a reactor for oligomerizing a feed stream containing a fed monomer; a stirrer inserted into a hole formed in an upper portion of the reactor; and a solvent transfer line extending inward from a side of the reactor, wherein the stirrer includes a rotating shaft vertically extending downward from the upper portion of the reactor, and a blade having a conical shape whose vertex is positioned at a lower end of the rotating shaft and outer diameter increases from a bottom toward a top, and the solvent transfer line has a plurality of spray nozzles formed in a direction toward the blade.