B01J6/002

PRODUCTION OF CALCINED MATERIAL WITH SEPARATE CALCINATION OF EXHAUST DUST

A process for producing caustic calcined magnesia (CCM) includes calcining a magnesium containing material, such as magnesite, in a primary calciner to produce a primary calcined material and a primary exhaust comprising dust; subjecting the primary exhaust to separation to recover a dust material includes incompletely calcined dust particles; calcining the dust material in the secondary calciner to produce calcined dust, wherein the dust material is not co-calcined with the magnesium containing material or the primary calcined material. The primary calcined material and the calcined dues thus form two CCM products, which can be kept separate or combined. The primary calciner can be a multiple hearth furnace (MHF) while the secondary calciner can be a gas suspension calciner (GSC). Using a secondary calciner in such a manner can increase throughput of the primary calciner and provide other advantages for the calcination process.

Systems and methods for purifying and recycling lead from spent lead-acid batteries

The present disclosure relates to systems and methods by which lead from spent lead-acid batteries may be extracted, purified, and used in the production of new lead-acid batteries. The system includes a first phase separation device configured to: receive the first mixture from the basic lead stream digestion device, isolate a liquid component from one or more insoluble components of the first mixture, and output the liquid component. The system also includes a lead salt precipitation device configured to: receive and mix the liquid component and a carboxylate source to form a second mixture including a lead salt precipitate, and output the second mixture. The system further includes a second phase separation device configured to: receive the second mixture from the lead salt precipitation device, isolate the liquid component from the lead salt precipitate of the second mixture, and output the lead salt precipitate.

DEVICE FOR DRYING AND RECOVERING CARBON NANOTUBE PRODUCT AND METHOD FOR MANUFACTURING CARBON NANOTUBE USING SAME

The present invention relates to a device for drying and collecting a product such as a carbon nanotube pellet or aggregate, which can accelerate solvent evaporation by inserting and dispersing high temperature gas into a drying column as well as by a heat source inside and outside of the column, and can quickly remove the evaporated solvent. Further, the device can be used for drying and collecting processes while minimizing product breakage by regulating the gas flow rate and controlling flow of the product in the column. Thus, the device can be effectively applied to mass production of a carbon nanotube pellet product.

METHOD AND APPARATUS FOR PRODUCING HIGH-PURITY SYNTHETIC MAGNETITE BY OXIDIZING METAL WASTE
20180251382 · 2018-09-06 ·

The invention relates to a method for producing magnetite with a purity of no less than 90% and higher than 98%, by oxidation of pulverized wustite (iron oxide), at temperatures ranging from 200 C. to 800 C., with the addition of water in liquid or steam form, in counter-current or concurrently, in an externally heated reaction chamber with a controlled atmosphere. The amount of water used to oxidize the wustite being 60 to 500 ml per kilogram of wustite, the grains of wustite powder are injected into the reaction chamber having a size no greater than 100 m for optimal reaction.

Process and apparatus for preparing a molecular sieve and a catalytic cracking catalyst

A process for preparing a catalytic cracking catalyst, which process comprises: a molecular sieve is introduced into a gas-phase ultra-stabilization reactor, the molecular sieve is moved without the conveying of carrier gas from a molecular sieve inlet of the gas-phase ultra-stabilization reactor to a molecular sieve outlet of the gas-phase ultra-stabilization reactor, and the molecular sieve is contacted and reacted with a gaseous SiCl.sub.4 in the gas-phase ultra-stabilization reactor, the molecular sieve resulting from the contacting and the reacting is optionally washed, then mixed with a matrix and water into slurry, and shaped into particles.

METHODS FOR PURIFYING AND RECYCLING LEAD FROM SPENT LEAD-ACID BATTERIES
20170338530 · 2017-11-23 ·

The present disclosure relates to methods by which lead from spent lead-acid batteries may be extracted, purified, and used in the construction of new lead-acid batteries. A method includes: (A) forming a mixture including a carboxylate source and a lead-bearing material; (B) generating a first lead salt precipitate in the mixture as the carboxylate source reacts with the lead-bearing material; (C) increasing the pH of the mixture to dissolve the first lead salt precipitate; (D) isolating a liquid component of the mixture from one or more insoluble components of the mixture; (E) decreasing the pH of the liquid component of the mixture to generate a second lead salt precipitate; and (F) isolating the second lead salt precipitate from the liquid component of the mixture. Thereafter, the isolated lead salt precipitate may be converted to leady oxide for use in the manufacture of new lead-acid batteries.

SYSTEMS AND METHODS FOR PURIFYING AND RECYCLING LEAD FROM SPENT LEAD-ACID BATTERIES
20170338531 · 2017-11-23 ·

The present disclosure relates to systems and methods by which lead from spent lead-acid batteries may be extracted, purified, and used in the production of new lead-acid batteries. The system includes a first phase separation device configured to: receive the first mixture from the basic lead stream digestion device, isolate a liquid component from one or more insoluble components of the first mixture, and output the liquid component. The system also includes a lead salt precipitation device configured to: receive and mix the liquid component and a carboxylate source to form a second mixture including a lead salt precipitate, and output the second mixture. The system further includes a second phase separation device configured to: receive the second mixture from the lead salt precipitation device, isolate the liquid component from the lead salt precipitate of the second mixture, and output the lead salt precipitate.

Systems and methods for purifying and recycling lead from spent lead-acid batteries

The present disclosure relates to systems and methods by which lead from spent lead-acid batteries may be extracted, purified, and used in the production of new lead-acid batteries. The system includes a first phase separation device configured to: receive the first mixture from the basic lead stream digestion device, isolate a liquid component from one or more insoluble components of the first mixture, and output the liquid component. The system also includes a lead salt precipitation device configured to: receive and mix the liquid component and a carboxylate source to form a second mixture including a lead salt precipitate, and output the second mixture. The system further includes a second phase separation device configured to: receive the second mixture from the lead salt precipitation device, isolate the liquid component from the lead salt precipitate of the second mixture, and output the lead salt precipitate.

Methods for purifying and recycling lead from spent lead-acid batteries

The present disclosure relates to methods by which lead from spent lead-acid batteries may be extracted, purified, and used in the construction of new lead-acid batteries. A method includes: (A) forming a mixture including a carboxylate source and a lead-bearing material; (B) generating a first lead salt precipitate in the mixture as the carboxylate source reacts with the lead-bearing material; (C) increasing the pH of the mixture to dissolve the first lead salt precipitate; (D) isolating a liquid component of the mixture from one or more insoluble components of the mixture; (E) decreasing the pH of the liquid component of the mixture to generate a second lead salt precipitate; and (F) isolating the second lead salt precipitate from the liquid component of the mixture. Thereafter, the isolated lead salt precipitate may be converted to leady oxide for use in the manufacture of new lead-acid batteries.

Method for calcination of a carbon dioxide rich sorbent

A method for calcination includes providing a heated coarse solid particle stream with a carbon dioxide rich sorbent to a reactor having a rotatable container.