Patent classifications
B01J6/004
METHOD FOR PREPARING CALCIUM OXIDE USING A MULTISTAGE SUSPENSION PREHEATER KILN
The disclosure discloses a method for preparing calcium oxide using multistage suspension preheater kiln. The steps of the method are: (1) the limestone powder is fed to the multistage suspension preheater kiln for preheating to 800 C. to 900 C.; (2) A preheated material is fed to a decomposition furnace, and calcined at 900 C. to 1100 C. for 25 s to 35 s; (3) A calcined material is fed to a rotary kiln, and calcined at 1100 C. to 1300 C. for 25 to 35 minutes, and finally cooled to obtain calcium oxide.
CONTINUOUS PROCESSING CHAMBERS
This disclosure is directed to a continuous processing chamber that includes: a material shaft through which the material introduced by an inlet may be transported and discharged through an outlet; optionally an inner gas transfer tube in fluid communication with the material shaft with an inner filtration wall that encases at least a portion of the inner gas transfer tube and is in fluid communication with both the material shaft and the inner gas transfer tube; optionally an outer filtration wall that encases at least a portion of the material shaft and is in fluid communication with the material shaft and associated with an outer gas transfer tube. The continuous processing chamber may be incorporated into methods for treating the material to produce a lithiated product.
Process for making a lithiated transition metal oxide
Process for manufacturing a lithiated transition metal oxide, said process comprising the steps of (a) mixing at least one lithium salt and a precursor selected from transition metal oxides, transition metal oxyhydroxides, transition metal hydroxides, and transition metal carbonates, (b) pre-calcining the mixture obtained in step (a) at a temperature in the range of from 300 to 700 C., and (c) calcining the pre-calcined mixture according to step (b) in a multi-stage fluidized bed reactor at a temperature in the range of from 550 C. to 950 C.,
wherein the temperatures in step (b) and (c) are selected in a way that step (c) is being performed at a temperature higher than that of step (b).
Process and apparatus for manufacture of calcined compounds for the production of calcined products
A process for producing a highly calcined and uniformly calcined product from a feedstock. The process comprising the steps of grinding the feedstock to powder, preheating the powder, and calcining the powder in a reactor plant that comprises a number of reactor segments in which a flash calciner is used in each progressive reactor segment to incrementally react the powder by raising the temperature in each segment. The last segment may be a high-temperature reactor that has a controlled residence time and temperature that may allow controlled finishing of the calcination process to achieve a desired degree of calcination and sintering of the product; and cooling of the product.
DEVICE AND METHOD FOR THERMAL OR THERMO-CHEMICAL TREATMENT OF MATERIAL
The invention relates to a device for the thermal or thermo-chemical treatment, more particularly calcination, of material (12), more particularly battery cathode material (14), comprising a housing (16), in which a process space (20) is located. The material (12), or carrying structures (40) loaded with the material (12), can be conveyed in a conveying direction (30) into or through the process space (20) by means of a conveying system (28). A process space atmosphere (50) prevailing in the process space (20) can be heated by means of a heating system (48). There is a process gas system (64), by means of which a process gas (66) can be fed to the process space (20), said process gas being required for the thermal treatment of the material (12). The process gas system (64) comprises a plurality of local injection units (68), which are arranged and configured such that process gas (66) can be released in a targeted manner onto the material (12) or onto the carrying structures (40) loaded with material (12), the process gas being released in a plurality of local process gas streams (70), each having a main stream direction (72). The invention also specifies a method for the thermal or thermo-chemical treatment of material (12), in which process gas (66) is released in a targeted manner onto the material (12) or onto the carrying structures (40) loaded with material (12), the process gas being released in a plurality of local process gas streams (70), each having a main stream direction (72).
PROCESS FOR PRODUCING LITHIATED TRANSITION METAL OXIDES
Provided are processes for the formation of electrochemically active materials such as lithiated transition metal oxides that solve prior issues with throughput and calcination. The processes include forming the materials in the presence of a processing additive that includes potassium prior to calcination that produces active materials with increased primary particle grain sizes.
PROCESS FOR MAKING A LITHIATED TRANSITION METAL OXIDE
Process for manufacturing a lithiated transition metal oxide, said process comprising the steps of (a) mixing at least one lithium salt and a precursor selected from transition metal oxides, transition metal oxyhydroxides, transition metal hydroxides, and transition metal carbonates, (b) pre-calcining the mixture obtained in step (a) at a temperature in the range of from 300 to 700 C., and (c) calcining the pre-calcined mixture according to step (b) in a multi-stage fluidized bed reactor at a temperature in the range of from 550 C. to 950 C.,
wherein the temperatures in step (b) and (c) are selected in a way that step (c) is being performed at a temperature higher than that of step (b).
PROCESSES FOR QUANTITATIVE CALCIUM SULFATE PHASE ANALYSIS AND USES THEREOF
The present disclosure relates generally to processes for phase analysis of calcium sulfate materials useful in making gypsum products. In various aspects, the disclosure provides processes for providing a computer-implemented system for determining a phase content of a test calcium sulfate material; processes for determining the phase content of a test calcium sulfate material; processes for providing stucco feedstocks; and production processes for gypsum products.
Method and device for the heat treatment of granular solids
A method for the heat treatment of granular solids includes initially introducing solids into a first reactor configured as a flash reactor or fluidized bed reactor where they are brought into contact with hot gases at temperatures in the range 500 C. to 1500 C. Next, the solids are passed through a residence time reactor in which they are fluidized. The residence time reactor is configured in a manner such that it has various regions which are separated from one another, from which the solid can be withdrawn in a manner such that it is provided with a variety of residence times in the residence time reactor.
Two-stage calcination method, and plant for same
A method for the calcination of powdery or fine-particled plaster, comprising two steps: the plaster is subjected to a flash-calcination in a calcinator and the hot plaster is post-calcinated in a reaction vessel. Post-calcination is carried out in the reaction vessel by adding humid gas, said reaction vessel not being heated. The postcalcination takes place over a long period of time, that is at least 10 times, preferably 50-100 times longer than the amount of time taken for flash calcination. Calcination takes place without expending additional energy, and the remaining dihydrate produced during the flash calcination is also transformed into semi-hydrate and undesired anhydrite fractions are reduced. The method can ensure consistency in the product quality and also increase product quality. The temperature in the upstream calcinator can be lowered thus saving more energy. The method can also be used to accelerate the ageing of calcinated plaster.