An apparatus and a method to withdraw samples from a polymerization plant using a defined sequence of steps combined with locking devices for valves opened by a single key.

A reactor system comprising a first reactor assembly, a first pressure transition assembly, a second reactor assembly and a second pressure transition assembly.

An ebullated bed hydroprocessing system is upgraded using a dual catalyst system that includes a heterogeneous catalyst and dispersed metal sulfide particles, which permits recycling of vacuum bottoms without recycle buildup of asphaltenes. The dual catalyst system more effectively converts asphaltenes in the ebullated bed reactor and increases asphaltene conversion by an amount that at least offsets higher asphaltene concentration resulting from recycling of vacuum bottoms. In this way, there is no recycle buildup of asphaltenes in upgraded ebullated bed reactor notwithstanding recycling of vacuum bottoms. In addition, residual dispersed metal sulfide catalyst particles in the vacuum bottoms can maintain or increase the concentration of the dispersed metal sulfide catalyst in the ebullated bed reactor.

A control system for automatic operation of a fluid catalytic cracking unit is shown. The control system includes a reactor severity control device operable to modulate a temperature affecting volume gain within the fluid catalytic cracking unit and a controller. The controller includes a processing circuit configured to calculate the volume gain within the fluid catalytic cracking unit by comparing a volume based on one or more input oil feeds to the fluid catalytic cracking unit to a volume of one or more output oil products of the fluid catalytic cracking unit. The processing circuit is further configured to use a neural network model to generate a target severity predicted to optimize the volume gain within the fluid catalytic cracking unit. The processing circuit is further configured to operate the reactor severity control device using the target severity to modulate the temperature affecting the volume gain within the fluid catalytic cracking unit.

Processes and apparatus for preparing bimodal polymers are provided. In some embodiments, processes include introducing a monomer, a first diluent, a catalyst, hydrogen, at a first hydrogen concentration, and optional comonomer, to a first loop reactor to produce, under polymerization conditions, a first slurry of polymer solids. Processes may also include continuously discharging the first slurry of polymer solids from the loop reactor as a first polymerization effluent to a first flash tank; separating the first polymerization effluent in the first flash tank to provide a first concentrated polymer slurry with significantly lower hydrogen concentration; and transferring the first concentrated polymer slurry from the flash tank to a re-slurry mixer. Processes may further include introducing a re-slurry mixer diluent to the first concentrated polymer slurry to form a second concentrated polymer slurry in the re-slurry mixer that can be pumped to a second slurry loop reactor.

A catalyst loading and unloading system for chemical reactors has an extendable catalyst transfer tube that is fed by a catalyst hopper and controlled by a tube displacement mechanism; more particularly, by a winch mechanism. As the reactor chamber fills with catalyst, a lower end of the extendable catalyst transfer tube is displaced upward by the tube displacement mechanism to correspond with the rising height of the catalyst bed within the chamber. The extendable catalyst transfer tube may further be used to vacuum old catalyst out of the reactor chamber.

Device for metering powder, in particular in clean-rooms, which includes a vessel containing powder and a sealing head with a septum for the vessel, wherein the sealing head is connectable powder-tight with the vessel and the septum powder-tight with the sealing head and the device further includes a vessel holder, which serves to hold the sealing head of the vessel, and the vessel with its opening points downwards, so that the powder can flow out of the vessel, wherein a gap is provided between the sealing head and a holding bowl of the vessel holder, in which a gas flow between the holding bowl and the sealing head can be created. The invention also relates to a use of the device and a metered addition method.

Methods and apparatus are disclosed for removing catalyst, absorbents and other materials from a reactor, guard bed, or other refinery or petrochemical vessel via a robotic or remotely operated device. A vacuum hose is connected to the device for removing the material from the vessel for ex-situ regeneration or disposal. The device moves around on the surface of the catalyst using motorized screws that grip to the catalyst material. The device is powered by hydraulic, pneumatic or electric motors attached to the frame of the device with supply and return hoses extending in and out of the vessel in line with the vacuum hose.

Device for metering powder, in particular in clean-rooms, which includes a vessel containing powder and a sealing head with a septum for the vessel, wherein the sealing head is connectable powder-tight with the vessel and the septum powder-tight with the sealing head and the device further includes a vessel holder, which serves to hold the sealing head of the vessel, and the vessel with its opening points downwards, so that the powder can flow out of the vessel, wherein a gap is provided between the sealing head and a holding bowl of the vessel holder, in which a gas flow between the holding bowl and the sealing head can be created. The invention also relates to a use of the device and a metered addition method.

Apparatus for feeding doses of fluidisable materials comprising one upper Intel pipe (1′, 1″), one lower outlet pipe (2′, 2″) and a Pausing (6′,6″). and a fluidising element (5′,5″) for controlling outflow of materials through the outlet pipe (2′, 2″), The apparatus further comprising a control volume constituted by a chamber (3′,3″) between the Intel pipe (1′, 8″) and the outlet pipe (2′,2″) and a fluidising element (4′, 4″) for controlling inflow of materials Into the chamber (3′, 3″). A diverter (7′,7″) la arranged between the Inlet pipe (1′, 8″) and the outlet pipe {2′, 2″) defining said chamber (3′, 3″) between said Inlet pipe (1′,8″) diverter (7′,7″) the housing (6′, 6″) and the fluidising element (5′,5″). The Invention also relates to a method for feeding doses of fluidisable materials by the apparatus.