B01J8/10

Reactor for coating particles in stationary chamber with rotating paddles

A reactor for coating particles includes a stationary vacuum chamber to hold a bed of particles to be coated, a vacuum port in an upper portion of the chamber, a chemical delivery system configured to inject a reactant or precursor gas into a lower portion of the chamber, a paddle assembly, and a motor to rotate a drive shaft of the paddle assembly. The lower portion of the chamber forms a half-cylinder. The paddle assembly includes a rotatable drive shaft extending through the chamber along the axial axis of the half cylinder, and a plurality of paddles extending radially from the drive shaft such that rotation of the drive shaft by the motor orbits the plurality of paddles about the drive shaft.

PROCESS FOR PROVIDING A HOMOGENOUS SLURRY CONTAINING PARTICLES
20220023815 · 2022-01-27 ·

The present invention is concerned with a process for providing a homogeneous particle-containing slurry comprising the steps of:

(a) providing a vessel comprising at least one impeller rotating around a vertical axis of the vessel, the vessel further comprising an inlet and an outlet;
(b) introducing the particle-containing slurry into the vessel or introducing components forming the particle-containing slurry into the vessel;
(c) rotating the at least one impeller at least around the vertical axis for homogenizing and/or maintaining a homogeneous particle distribution within the slurry;
(d) withdrawing the homogeneous particle-containing slurry via the outlet;
(e) stopping the at least one impeller for a maximum time T, whereby T is calculated according to the following relations:

[00001] u T = 4 g ( ρ p - ρ f ) D p 3 ρ f C D ( 1 ) C D = 24 Re [ 1 + 0.173 Re 0.657 ] ( 2 ) T = h u T ( 3 )

PROCESS FOR PROVIDING A HOMOGENOUS SLURRY CONTAINING PARTICLES
20220023815 · 2022-01-27 ·

The present invention is concerned with a process for providing a homogeneous particle-containing slurry comprising the steps of:

(a) providing a vessel comprising at least one impeller rotating around a vertical axis of the vessel, the vessel further comprising an inlet and an outlet;
(b) introducing the particle-containing slurry into the vessel or introducing components forming the particle-containing slurry into the vessel;
(c) rotating the at least one impeller at least around the vertical axis for homogenizing and/or maintaining a homogeneous particle distribution within the slurry;
(d) withdrawing the homogeneous particle-containing slurry via the outlet;
(e) stopping the at least one impeller for a maximum time T, whereby T is calculated according to the following relations:

[00001] u T = 4 g ( ρ p - ρ f ) D p 3 ρ f C D ( 1 ) C D = 24 Re [ 1 + 0.173 Re 0.657 ] ( 2 ) T = h u T ( 3 )

Process of making polyolefins

The present invention relates to a process for the continuous production of a polyolefin, preferably polypropylene, in a horizontal stirred bed polymerization reactor by contacting one or more olefins, preferably propylene, with a catalyst system while stirring, said catalyst system comprising: * a procatalyst comprising i) titanium; ii) a magnesium-containing support, preferably a magnesium chloride-containing support, and iii) an internal electron donor; * optionally an external electron donor; and * a co-catalyst, being a alkyl aluminum catalyst having formula AlX.sub.nR.sub.3-n, wherein each X is independently a halide or a hydride and wherein n is 0, 1 or 2, preferably 0, and wherein R is an C1-C12 alkyl group, preferably ethyl, wherein the molar ratio of aluminum (Al) from the co-catalyst to titanium (Ti) from the procatalyst (Al/Ti) is at least 75. The present invention also relates to polyolefin prepared using said process and a shaped article comprising said polyolefin. The present invention moreover relates to the use of a titanium to aluminum ratio during the Ziegler-Natta polymerization of olefins in a horizontal stirred bed reactor to reduce the energy (power) consumption in view of a situation wherein the titanium to aluminum ratio is lower.

Process of making polyolefins

The present invention relates to a process for the continuous production of a polyolefin, preferably polypropylene, in a horizontal stirred bed polymerization reactor by contacting one or more olefins, preferably propylene, with a catalyst system while stirring, said catalyst system comprising: * a procatalyst comprising i) titanium; ii) a magnesium-containing support, preferably a magnesium chloride-containing support, and iii) an internal electron donor; * optionally an external electron donor; and * a co-catalyst, being a alkyl aluminum catalyst having formula AlX.sub.nR.sub.3-n, wherein each X is independently a halide or a hydride and wherein n is 0, 1 or 2, preferably 0, and wherein R is an C1-C12 alkyl group, preferably ethyl, wherein the molar ratio of aluminum (Al) from the co-catalyst to titanium (Ti) from the procatalyst (Al/Ti) is at least 75. The present invention also relates to polyolefin prepared using said process and a shaped article comprising said polyolefin. The present invention moreover relates to the use of a titanium to aluminum ratio during the Ziegler-Natta polymerization of olefins in a horizontal stirred bed reactor to reduce the energy (power) consumption in view of a situation wherein the titanium to aluminum ratio is lower.

SYSTEMS AND METHODS FOR MAKING CERAMIC POWDERS

Systems and methods for making ceramic powders configured with consistent, tailored characteristics and/or properties are provided herein. In some embodiments a system for making ceramic powders, includes: a reactor body having a reaction chamber and configured with a heat source to provide a hot zone along the reaction chamber; a sweep gas inlet configured to direct a sweep gas into the reaction chamber and a sweep gas outlet configured to direct an exhaust gas from the reaction chamber; a plurality of containers, within the reactor body, configured to retain at least one preform, wherein each container is configured to permit the sweep gas to flow therethrough, wherein the preform is configured to permit the sweep gas to flow there through, such that the precursor mixture is reacted in the hot zone to form a ceramic powder product having uniform properties.

SYSTEMS AND METHODS FOR MAKING CERAMIC POWDERS

Systems and methods for making ceramic powders configured with consistent, tailored characteristics and/or properties are provided herein. In some embodiments a system for making ceramic powders, includes: a reactor body having a reaction chamber and configured with a heat source to provide a hot zone along the reaction chamber; a sweep gas inlet configured to direct a sweep gas into the reaction chamber and a sweep gas outlet configured to direct an exhaust gas from the reaction chamber; a plurality of containers, within the reactor body, configured to retain at least one preform, wherein each container is configured to permit the sweep gas to flow therethrough, wherein the preform is configured to permit the sweep gas to flow there through, such that the precursor mixture is reacted in the hot zone to form a ceramic powder product having uniform properties.

Advanced oxidation process for the exfoliation of two dimensional matertals

A system for extracting two dimensional materials from a bulk material by functionalization of the bulk material in a reactor.

Advanced oxidation process for the exfoliation of two dimensional matertals

A system for extracting two dimensional materials from a bulk material by functionalization of the bulk material in a reactor.

Chemical Reactor with High Speed Rotary Mixing, for Catalytic Thermal Conversion of Organic Materials Into Diesel and Other Liquid Fuels, and Applications Thereof
20220008890 · 2022-01-13 · ·

Chemical reactor with high speed rotary mixing, system thereof, and method thereof, for catalytic thermal conversion of organic (hydrocarbon-containing) materials (coal, plastics, rubber, plant matter, wood shavings, biomass, organic wastes) into diesel and other liquid fuels (automobile or/and jet engine fuels). Relevant to non-conventional commercial scale production of liquid fuels, and to commercial scale processing and disposing of organic waste materials. Chemical reactor includes: integrated combination of a reactor stationary assembly (RSA), having only stationary components remaining stationary during chemical reactor operation, and a reactor rotary mixing assembly (RRMA), having only rotatable components rotating during chemical reactor operation. May include anti-abrasion shield for shielding inner surface of reactor central housing from abrasion during chemical reactor operation. Rotor may include a reinforcement disc. Rotor blades or/and reinforcement disc may include rotor-based performance and process control structural features (openings, or/and protrusions, or/and depressions), for additionally controlling performance of the rotor.