B01J8/1809

Continuous process for conversion of lignin to useful compounds

This specification discloses an operational continuous process to convert lignin as found in ligno-cellulosic biomass before or after converting at least some of the carbohydrates. The continuous process has been demonstrated to create a slurry comprised of lignin, raise the slurry comprised of lignin to ultra-high pressure, deoxygenate the lignin in a lignin conversion reactor over a catalyst which is not a fixed bed without producing char. The conversion products of the carbohydrates or lignin can be further processed into polyester intermediates for use in polyester preforms and bottles.

Systems and Methods for Measuring Particle Accumulation on Reactor Surfaces
20170320034 · 2017-11-09 · ·

Systems and methods for monitoring a particle/fluid mixture are provided. The method can include flowing a mixture comprising charged particles and a fluid past a particle accumulation probe. The method can also include measuring electrical signals detected by the probe as some charged particles pass the probe without contacting the probe while other charged particles contact the probe. The measured electrical signals can be manipulated to provide an output. The method can also include determining from the output if the charged particles contacting the probe have, on average, a different charge than the charged particles that pass the probe without contacting the probe.

REGENERATION METHOD FOR CATALYTIC CRACKING REACTION
20170267933 · 2017-09-21 ·

A regeneration method for catalytic cracking reaction, the method is applied in a catalytic reaction process of petroleum hydrocarbon materials, and the method comprises: feeding the regenerated and semi-regenerated catalyst from a regenerator separately into different positions of a reactor for reaction. A part of the semi-regenerated catalyst is firstly processed in a purification cooler for removing carried nitrogen, oxygen, carbon dioxide and impurity gases before being fed into the reactor. Spent catalyst or the purified and cooled semi-regenerated catalyst is fed into a catalyst mixing section of the reactor for controlling the temperature of the catalyst being contact with the oil material to be gasified, thereby achieving a three stage cycle of the catalyst in the reactor and a three stage control for the reaction outlets of the oil material gasification zone and the cracking reaction zone and the catalyst taking part in the reaction.

Fluidized bed biogasifier and method for gasifying biosolids

A fluidized bed biogasifier is provided for gasifying biosolids. The biogasifier includes a reactor vessel and a feeder for feeding biosolids into the reactor vessel at a desired feed rate during steady-state operation of the biogasifier. A fluidized bed in the base of the reactor vessel has a cross-sectional area that is proportional to at least the fuel feed rate such that the superficial velocity of gas is in the range of 0.1 m/s (0.33 ft/s) to 3 m/s (9.84 ft/s). In a method for gasifying biosolids, biosolids are fed into a fluidized bed reactor. Oxidant gases are applied to the fluidized bed reactor to produce a superficial velocity of producer gas in the range of 0.1 m/s (0.33 ft/s) to 3 m/s (9.84 ft/s). The biosolids are heated inside the fluidized bed reactor to a temperature range between 900° F. (482.2° C.) and 1700° F. (926.7° C.) in an oxygen-starved environment having a sub-stoichiometric oxygen level, whereby the biosolids are gasified.

METHODS OF CONTROLLING POLYOLEFIN MELT INDEX

The use of induced condensing agent (ICA) in fluidized bed gas phase reactor systems enables higher production rates but can affect the resulting polyolefins melt index. The effect the increased ICA concentration may have on a melt index may be counteracted, if necessary, by altering the concentration of olefin monomer within the reactor system.

Bubble size minimizing internals for fluidized bed reactors

The present invention relates to internals useful for minimizing bubble size in a bubbling fluidized bed reactor. One use for the invention is in an apparatus and method for producing trichlorosilane in which metallurgical grade silicon is reacted with hydrogen chloride gas and while being fluidized by the hydrogen chloride gas, thereby producing trichlorosilane.

Method, an arrangement and use of an arrangement for olefin polymerisation
11208507 · 2021-12-28 · ·

An olefin polymerisation method and arrangement comprising polymerising at least one olefin in gas phase in a fluidised bed in the presence of an olefin polymerisation catalyst in a polymerisation reactor having a vertical body; a generally conical downwards tapering bottom zone; a generally cylindrical middle zone, above and connected to said bottom zone; and a generally conical upwards tapering top zone above and connected to said middle zone wherein (i) fluidisation gas is introduced to the bottom zone of the reactor from where it passes upwards through the reactor; (ii) the fluidisation gas is withdrawn from the top zone of the reactor; (iii) a fluidised bed is formed within the reactor where the growing polymer particles are suspended in the upwards rising gas stream; and wherein the polymerisation reactor has an operating temperature set point and which reactor comprises at least one temperature measurement sensor, wherein a temperature difference (DT) between the temperature measurement sensor (Tm), and the operating temperature set point (Ts) of the reactor is equal to or less than 10° C.

Device and method for catalytically converting chemical substances at dwell times in the range of 0.1-10 seconds
11207652 · 2021-12-28 · ·

Disclosed herein is an apparatus and a method for catalytic conversion of chemical substances in the presence of pulverulent catalysts in a trickle bed reactor with residence times in the range of 0.1-10 seconds, wherein the apparatus includes a trickle bed reactor (2), the inlet side of which is functionally connected to a catalyst reservoir vessel (1) and a reactant feed, and the outlet side of which is functionally connected to a separator (3). The separator (3) has an exit conduit for leading off product stream, wherein the apparatus has the characteristic feature that the exit conduit disposed on the separator (3) for leading off product stream has a continuously acting valve connected via a controller to a pressure measurement sensor, wherein the continuously acting valve and the pressure measurement sensor form a pressure control circuit with a controller.

DEVICE AND METHOD FOR SINGLE-STAGE CONTINUOUS PREPARATION OF CARBON NANOTUBES
20210395090 · 2021-12-23 ·

An apparatus for continuous preparation of carbon nanotubes, based on a fluidized bed reactor. The fluidized bed reactor comprises an annular varying diameter zone, a raw material gas inlet, a catalyst feeding port, a protective gas inlet, and a pulse gas controller. The annular varying diameter zone is located at a zone from a ¼ position starting from the bottom to the top. The pulse gas controller is disposed at the arc-shaped top portion of the annular varying diameter zone. The catalyst feeding port is located at the top of the fluidized bed reactor. The raw material gas inlet and the protective gas inlet are located at the bottom of the fluidized bed reactor. The device is also provided with a product outlet and a tail gas outlet. The device has a simple structure and low cost, is easy to operate, has a high raw material utilization rate, can effectively control the problem of carbon deposition on the inner wall of a primary reactor, can manufacture high-purity carbon nanotubes, and is suitable for large-scale industrial production.

NITRO COMPOUND HYDROGENATION REACTION PROCESS AND HYDROGENATION REACTION APPARATUS
20210371370 · 2021-12-02 ·

The present invention relates to a nitro compound hydrogenation reaction process and hydrogenation reaction apparatus, which can achieve the objects of the continuous reaction of the nitro compound and the long-period run of regeneration and activation. The nitro compound hydrogenation reaction process comprises a hydrogenation step, a regeneration step, an optional activation step and a recycling step. There exists at least one step of degassing the spent catalyst between the hydrogenation step and the regeneration step. According to circumstances, there exists at least one step of degassing the regenerated catalyst between the regeneration step and the activation step.