B01J8/1836

Reactor and production method of trichlorosilane
11241666 · 2022-02-08 · ·

An object of the present invention is to prevent stress-corrosion cracking of a header (40) of a reactor. A reactor for producing trichlorosilane by causing metal silicon powder and a hydrogen chloride gas to react with each other includes a cooler (70), the cooler including a plurality of heat transfer medium pipes (30) and a header (40), the plurality of heat transfer medium pipes being provided in a fluid bed (60) inside the reactor, the header being provided in a freeboard section (50) inside the reactor, the header being comprised of a corrosion-resistant material.

Apparatus for producing trichlorosilane and method for producing trichlorosilane

An apparatus for producing trichlorosilane in which metallurgical grade silicon powder supplied to a reactor is reacted with hydrogen chloride gas while being fluidized by the hydrogen chloride gas, thereby discharging trichlorosilane generated by the reaction from the reactor, includes: a plurality of gas flow controlling members which are installed along a vertical direction in an annular shape R from an inner peripheral wall of the reactor in an internal space of the reactor; and a heat transfer tube which is installed along the vertical direction in the annular space R and through which a heating medium passes.

System and method for preventing catalyst from overheating

A system for preventing a catalyst from overheating is provided. The system includes: a first reactor filled with a catalyst at least in part and configured to receive reaction gas and produce product gas; and a second reactor configured to cool a catalyst discharged from the first reactor. The catalyst is circulated between the first reactor and the second reactor by injecting the catalyst cooled in the second reactor into the first rector.

Method for preparing a light olefin using an oxygen-containing compound, and device for use thereof

A method for preparing a light olefin using an oxygen-containing compound, and a device for use thereof, more specifically, taking methanol and/or dimethyl ether as main starting materials, using a multi-stage (n≧2) dense phase fluidized bed reactor and a multi-stage (m≧2) catalyst regenerator, which solves the problem in the prior art of the uniformity of catalyst carbon deposition and the carbon content being difficult to control and the light olefin selectivity being low.

Fluidized bed reactor and a process using same to produce high purity granular polysilicon

The present invention relates to a fluidized bed reactor, comprising a reaction tube, a distributor and a heating device, the reaction tube and the distributor at the bottom of the reaction tube composing a closed space, the distributor comprising a gas inlet and a product outlet, and the reaction tube comprising a tail gas outlet and a seed inlet at the top or upper part respectively, characterized in that the reaction tube comprises a reaction inner tube and a reaction outer tube, and the heating device is an induction heating device placed within a hollow cavity formed between the external wall of the reaction inner tube and the internal wall of the reaction outer tube, wherein the hollow cavity is filled with hydrogen, nitrogen or inert gas for protection, and is able to maintain a pressure of about 0.01 to about 5 MPa; and also to a process of producing high purity granular polysilicon using the reactor. The fluidized bed reactor according to the present invention uses induction heating to heat directly the silicon particles inside the reaction chamber, such that the temperature of the reaction tube is lower than that inside the reaction chamber, which accordingly avoids deposition on the tube wall and results in more uniform heating, and thus is useful for large diameter fluidized bed reactors with much increased output for a single reactor.

REGENERATION METHOD FOR CATALYTIC CRACKING REACTION
20170267933 · 2017-09-21 ·

A regeneration method for catalytic cracking reaction, the method is applied in a catalytic reaction process of petroleum hydrocarbon materials, and the method comprises: feeding the regenerated and semi-regenerated catalyst from a regenerator separately into different positions of a reactor for reaction. A part of the semi-regenerated catalyst is firstly processed in a purification cooler for removing carried nitrogen, oxygen, carbon dioxide and impurity gases before being fed into the reactor. Spent catalyst or the purified and cooled semi-regenerated catalyst is fed into a catalyst mixing section of the reactor for controlling the temperature of the catalyst being contact with the oil material to be gasified, thereby achieving a three stage cycle of the catalyst in the reactor and a three stage control for the reaction outlets of the oil material gasification zone and the cracking reaction zone and the catalyst taking part in the reaction.

FLUIDIZED BED REACTOR FOR PRODUCING POLYCRYSTALLINE SILICON GRANULES AND METHOD FOR THE ASSEMBLY OF SUCH A FLUIDIZED BED REACTOR

Assembly of a fluidized bed reactor for the preparation of polycrystalline silicon granules by chemical vapor deposition of silicon onto seed particles and removal of polycrystalline silicon granules is facilitated without breakage and with gas tightness by a specific assembly sequence.

REACTOR AND MULTIFUNCTIONAL RISER AND DOWNER SIMULATOR INCORPORATING THE SAME
20170320036 · 2017-11-09 ·

A reactor comprises a reactor vessel defining a confined reactor volume, a support assembly extending about a periphery of the confined reactor volume, a basket positioned within the reactor vessel and supported by the support assembly, the basket having an interior surface and an exterior surface, a downflow zone being defined between the exterior surface of the basket and an interior surface of the confined reactor volume, an inlet screen positioned adjacent to one end of the interior surface and an outlet screen positioned adjacent to an opposite end of the interior surface, an upflow zone defined between the inlet screen and outlet screen, the inlet screen and the outlet screen containing a quantity of particulate catalyst, and a circulating device positioned above said upflow zone and configured to continuously circulate fluid upwardly though said upflow zone and downwardly through said downflow zone, the support assembly and the basket configured to promote the formation of a fluid vortex within a portion of the downflow zone.

Continuous preparation of calcined chemically-treated solid oxides

The present invention discloses a continuous calcination vessel which can be used to prepare calcined chemically-treated solid oxides from solid oxides and chemically-treated solid oxides. A process for the continuous preparation of calcined chemically-treated solid oxides is also provided. Calcined chemically-treated solid oxides disclosed herein can be used in catalyst compositions for the polymerization of olefins.

Process for the large-scale manufacture of zeolite-templated carbon

A method for the large-scale synthesis of a zeolite-templated carbon (ZTC). The method includes the steps of: introducing a bed material comprising a zeolite to a fluidized bed reactor and heating the bed material to a temperature between 550° C. and 800° C.; fluidizing the bed material with a fluidizing gas and maintaining the temperature of the bed material between 550° C. and 800° C.; introducing an organic carbon precursor while fluidizing the zeolite for a period of time such that carbon is deposited on the zeolite by chemical vapor deposition to produce a zeolite-carbon composite; and treating the zeolite-carbon composite with an acid solution such that the zeolite template is dissolved and the ZTC is obtained.