A method of operating a polyethylene reactor system includes feeding ethylene, an optional first comonomer, a diluent, and a chromium-based catalyst to a first polymerization reactor. The method further includes contacting ethylene and the comonomer with the catalyst in the first polymerization reactor to form a first product including a first polyethylene. The method further includes feeding the first product from the first polymerization reactor to a second polymerization reactor. The method further includes contacting ethylene and a second optional comonomer with catalyst from the first reactor in the second polymerization reactor to form a second product including the first polyethylene and a second polyethylene. The method further includes controlling one or both of a molecular weight or a breadth of molecular weight distribution of the second product by adjusting a rate of hydrogen fed to one or both of the first polymerization reactor or the second polymerization reactor.

A method of operating a polyethylene reactor system includes feeding ethylene, an optional first comonomer, a diluent, and a chromium-based catalyst to a first polymerization reactor. The method further includes contacting ethylene and the comonomer with the catalyst in the first polymerization reactor to form a first product including a first polyethylene. The method further includes feeding the first product from the first polymerization reactor to a second polymerization reactor. The method further includes contacting ethylene and a second optional comonomer with catalyst from the first reactor in the second polymerization reactor to form a second product including the first polyethylene and a second polyethylene. The method further includes controlling one or both of a molecular weight or a breadth of molecular weight distribution of the second product by adjusting a rate of hydrogen fed to one or both of the first polymerization reactor or the second polymerization reactor.

The present invention provides an all-in-one type continuous reactor for preparing a positive electrode active material for a lithium secondary battery. The continuous reactor includes a flange unit provided at one side of a cylinder; at least one reactant inlet port provided on the flange unit; a reaction product outlet port provided at the other side of the cylinder; a plurality of extra ports provided between the reactant inlet port and the reaction product outlet port; a temperature control unit disposed between an inner circumferential surface and outer circumferential surface; a pulverizing unit provided in the reactant inlet port; a flow rate sensor provided in at least one of the reactant inlet port; and a flow rate control unit configured to control the flow rate of the reactant.

The present invention provides an all-in-one type continuous reactor for preparing a positive electrode active material for a lithium secondary battery. The continuous reactor includes a flange unit provided at one side of a cylinder; at least one reactant inlet port provided on the flange unit; a reaction product outlet port provided at the other side of the cylinder; a plurality of extra ports provided between the reactant inlet port and the reaction product outlet port; a temperature control unit disposed between an inner circumferential surface and outer circumferential surface; a pulverizing unit provided in the reactant inlet port; a flow rate sensor provided in at least one of the reactant inlet port; and a flow rate control unit configured to control the flow rate of the reactant.

A reservoir for one or more chemical reactants has means for heating the reactants and optional means for stirring the reactants. A pumped reactant feed line and a return line provide fluid communication between the reservoir and a 4-way valve system. The 4-way valve system is also in fluid communication with a reactor vessel and a source of inert gas for purging the system. In a first state, the 4-way valve provides fluid communication between the reservoir and the reactor. In a second state, the 4-way valve provides a continuous circulation path for the heated reactants from the reservoir, to the valve system, and back to the reservoir via the return line. In a third state, the 4-way valve provides a fluid pathway for purging the reactor with inert gas. In a fourth state, the 4-way valve provides a fluid pathway for purging the reservoir with inert gas.

A reservoir for one or more chemical reactants has means for heating the reactants and optional means for stirring the reactants. A pumped reactant feed line and a return line provide fluid communication between the reservoir and a 4-way valve system. The 4-way valve system is also in fluid communication with a reactor vessel and a source of inert gas for purging the system. In a first state, the 4-way valve provides fluid communication between the reservoir and the reactor. In a second state, the 4-way valve provides a continuous circulation path for the heated reactants from the reservoir, to the valve system, and back to the reservoir via the return line. In a third state, the 4-way valve provides a fluid pathway for purging the reactor with inert gas. In a fourth state, the 4-way valve provides a fluid pathway for purging the reservoir with inert gas.

The invention relates to a process for the production of thermoplastic moulding compounds, in particular for the production of acrylonitrile-butadiene-styrene (ABS), wherein at least a first reagent (11) and a second reagent (12) of the thermoplastic moulding compounds are fed to a loop conduit (29) which comprises a static mixer (36), wherein the reagents (11, 12) are pressed in loops through the loop conduit (29) and passing the static mixer (36), whereby the reagents (11, 12) are dispersed to form a dispersion (15) in the static mixer (36). The invention also relates to a thermoplastic moulding compound that is produced by the inventive process.

Provided is a continuous reaction apparatus which can precisely control the path of flow of the liquid reaction mixture in the reaction vessel. Further, provided is a continuous reaction apparatus which can efficiently mix the liquid reaction mixture in the reaction vessel. The continuous reaction apparatus comprises a plurality of mixing vessel units and a plurality of partition units. These units are connected in the state of being alternately stacked on one another. Each mixing vessel unit has an agitating blade disposed in the inner space thereof. The relationship between the inner diameter D1 of the mixing vessel unit, the height H of the mixing vessel unit, and the outer diameter d1 of the agitating blade satisfies the formula (1): 10(D1/H)1.5, and the formula (2): 0.99(d1/D1)0.7. The agitating blade is a circular disc-type agitating blade.

Provided is a continuous reaction apparatus which can precisely control the path of flow of the liquid reaction mixture in the reaction vessel. Further, provided is a continuous reaction apparatus which can efficiently mix the liquid reaction mixture in the reaction vessel. The continuous reaction apparatus comprises a plurality of mixing vessel units and a plurality of partition units. These units are connected in the state of being alternately stacked on one another. Each mixing vessel unit has an agitating blade disposed in the inner space thereof. The relationship between the inner diameter D1 of the mixing vessel unit, the height H of the mixing vessel unit, and the outer diameter d1 of the agitating blade satisfies the formula (1): 10(D1/H)1.5, and the formula (2): 0.99(d1/D1)0.7. The agitating blade is a circular disc-type agitating blade.

Techniques for converting a portion of a carbonate to hydroxide include receiving an alkaline carbonate solution that includes between 0.1M (moles per liter of solution) to 4.0M hydroxide and between 0.1M to 4.1M carbonate; reacting, in a slaking process, quicklime (CaO) and a low carbonate content fluid to yield a slurry of primarily slaked lime (Ca(OH).sub.2); and reacting the Ca(OH).sub.2 slurry and the alkaline carbonate solution to grow calcium carbonate (CaCO.sub.3) crystal aggregates of 0.0005 mm.sup.3 to 5 mm.sup.3 in volume in a fluidized-bed reactive crystallizer.