B01J19/1856

Drive System for Static Batch Reactor
20170113197 · 2017-04-27 ·

A device for driving a plurality of rotatable agitators for use in a static batch reactor system, a reactor bottle cap for use with the rotatable agitator driving device and a static batch reactor system which includes the rotatable agitator driving device and bottles fitted with the reactor bottle cap are disclosed. The rotatable agitator driving device includes a planar case having first and second opposite faces, a plurality of drive heads projecting from the case through the second face and a gear train protectively housed in the case. The gear train includes a driver gear having a coupling for receiving drive from a motor, a set of idler gears and a set of driven gears. Each driven gear attached to a respective drive head for driving a rotatable agitator. The gear train is configured to cause the drive heads to rotate at the same rate.

Ethylene Oligomerization/Trimerization/Tetramerization Reactor
20170081257 · 2017-03-23 ·

A process includes periodically or continuously introducing an olefin monomer and periodically or continuously introducing a catalyst system or catalyst system components into a reaction mixture within a reaction system, oligomerizing the olefin monomer within the reaction mixture to form an oligomer product, and periodically or continuously discharging a reaction system effluent comprising the oligomer product from the reaction system. The reaction system includes a total reaction mixture volume and a heat exchanged portion of the reaction system comprising a heat exchanged reaction mixture volume and a total heat exchanged surface area providing indirect contact between the reaction mixture and a heat exchange medium. A ratio of the total heat exchanged surface area to the total reaction mixture volume within the reaction system is in a range from 0.75 in.sup.1 to 5 in.sup.1, and an oligomer product discharge rate from the reaction system is between 1.0 (lb)(hr.sup.1)(gal.sup.1) to 6.0 (lb)(hr.sup.1)(gal.sup.1).

Method of manufacturing diester-based compound

The present invention relates to a method of manufacturing a diester-based compound, and, more particularly, to a method of manufacturing a diester-based compound, which is performed using a continuous process including a reaction part in which a total of n reaction units spanning from a first reaction unit to an nth reaction unit are connected in series, wherein each of the reaction units includes a reactor, and the method includes: supplying a feed stream including a dicarboxylic acid and an alcohol into the first reactor; esterifying the feed stream to prepare a reaction product; and supplying a lower discharge stream including the reaction product into the reactor of the rear reaction unit. In this case, a conversion rate of the esterification reaction in the first reactor is controlled in a range of 50 to 80%.