Patent classifications
B01J19/1862
Design of an Ethylene Oligomerization/Trimerization/Tetramerization Reactor
A process includes periodically or continuously introducing an olefin monomer and periodically or continuously introducing a catalyst system or catalyst system components into a reaction mixture within a reaction system, oligomerizing the olefin monomer within the reaction mixture to form an oligomer product, and periodically or continuously discharging a reaction system effluent comprising the oligomer product from the reaction system. The reaction system includes a total reaction mixture volume and a heat exchanged portion of the reaction system comprising a heat exchanged reaction mixture volume and a total heat exchanged surface area providing indirect contact between the reaction mixture and a heat exchange medium. A ratio of the total heat exchanged surface area to the total reaction mixture volume within the reaction system is in a range from 0.75 in.sup.1 to 5 in.sup.1, and an oligomer product discharge rate from the reaction system is between 1.0 (lb)(hr.sup.1)(gal.sup.1) to 6.0 (lb)(hr.sup.1)(gal.sup.1).
Single step lactide production process with hydrolysis of oligomers and catalyst by recovered water
The present invention relates to a process for synthesizing lactide comprising the steps of: providing one or more components to at least one reactor, the one or more components comprising lactic acid; converting at least part of the lactic acid into lactide and water and into lactic acid oligomers; recovering at least part of the lactide; recovering at least part of the water and at least part of the lactic acid oligomers; adding a feed, optionally comprising lactic acid oligomers, and optionally comprising water, to the recovered water and the recovered lactic acid oligomers, and mixing the feed with the recovered water and the recovered lactic acid oligomers to form a mixture; converting at least part of the lactic acid oligomers in the mixture into lactic acid and into lactic acid dimer; and removing at least part of the water from the mixture;
whereby at least part of the remainder of the mixture is provided as one of the one or more components that are provided to the at least one reactor; and, wherein the step of converting at least part of the lactic acid into lactide and water is performed in one step.
CHEMICAL REACTION METHOD USING CHEMICAL REACTION APPARATUS
A chemical reaction method includes preparing a chemical reaction apparatus including a horizontal flow reactor partitioned into multiple chambers by multiple partition plates. A liquid content horizontally flows with an unfilled space provided thereabove. a microwave generator and a waveguide that transmits microwaves to the unfilled space are also included. The reactor is inclined such that, in each of the chambers, a weir height on an inlet side is higher than a weir height on an outlet side by at least an overflow depth at the partition plate on the outlet side. The content is flowed over each of the multiple partition plates inside the reactor. The content flowing inside the reactor is irradiated with microwaves. The inclination angle of the reactor is changed in each of the chambers so that a weir height on an inlet side is higher than a weir height on an outlet side.
Continuous chemical reactor
A continuous chemical reactor may include a primary reaction unit and at least one secondary reaction unit. The primary reaction unit has a stirring device and a first temperature regulating device, and a feed inlet provided at an upper portion thereof. The secondary reaction unit is sleeved outside the primary reaction unit, and a reaction chamber is formed therebetween. By adding reaction materials to the primary reaction unit via the feed inlet and adjusting the temperature of the reaction materials by the first temperature regulating device, the reacted materials enter the reaction chamber, and the heat generated in the reaction chamber can be used to adjust the temperature of the materials in the primary reaction unit to more effectively use the heat, and the product after reaction can be discharged from a discharge hole at the lower end of the secondary reaction unit, thereby achieving continuous production.
Processes and apparatuses for operating a hydrocarbon conversion zone
Processes and apparatus for reforming hydrocarbons to reduce the impact of contaminants created by non-catalyst coking. The reaction zone receives sulfur to inhibit the impact, and a control index is used to control the determine conditions with generally lower pressures. Additionally, a compression zone, pressure control zone and combustion zone operation are provided for the operation of the reaction zone at the generally lower pressures.
CONTINUOUS STIRRED TANK REACTOR FOR ALDOL CONDENSATION REACTION
Provided is a continuous stirred tank reactor for an aldol condensation reaction and an apparatus for an aldol condensation reaction including the same, which prevent a decrease in a conversion rate due to dead zone occurrence even in the case of an increase of an installation scale, have a high output, have a significantly increased reaction surface area during the reaction, suppress layer separation between an aqueous phase and an organic phase, and have a significantly decreased average particle diameter of organic layer particles dispersed in the aqueous phase and a significantly decreased deviation thereof. In addition, a content of the catalyst used per unit yield may be significantly decreased as compared with the conventional reactor and apparatus, and costs required for wastewater treatment may be significantly reduced as compared with the conventional reactor and apparatus.
Systems and processes integrating steam cracking with dual catalyst metathesis for producing olefins
Processes for producing olefins include integration of steam cracking with a dual catalyst metathesis process. The processes include steam cracking a hydrocarbon feed to form a cracking reaction effluent containing butenes, separating the cracking reaction effluent to produce a cracking C4 effluent including normal butenes, isobutene, and 1,3-butadiene, subjecting the cracking C4 effluent to selective hydrogenation to convert 1,3-butadiene in the cracking C4 effluent to normal butenes, removing isobutene from a hydrogenation effluent to produce a metathesis feed containing normal butenes, and contacting the metathesis feed with a metathesis catalyst and a cracking catalyst directly downstream of the metathesis catalyst to produce a metathesis reaction effluent. Contacting with the metathesis catalyst causes metathesis of normal butenes to produce ethylene, propene, and C5+ olefins, and contacting with the cracking catalyst causes C5+ olefins produced through metathesis to undergo cracking reactions to produce additional propene, ethylene, or both.
Process and apparatus for synthesizing multiwall carbon nanotubes from high molecular polymeric wastes
This invention relates to a process and an apparatus for synthesizing multiwall carbon nanotubes from high molecular polymeric wastes. The process comprises using induction heating in combination with catalytic chemical vapour deposition (CVD) with an array of catalytic materials to synthesize high value carbon nanotubes with better yield and purity from high molecular polymeric wastes.
Method for the degrading of synthetic polymers and device for carrying out said method
A method for breaking down synthetic polymers, in particular polyolefins, is provided. In addition a system for carrying out said method and a product according to said method is provided.
Preparation of N-vinyl carboxamides in a series of reactor units
Disclosed herein is a process for producing polymers of an N-vinyl carboxamide, including the steps of flowing a reaction mixture containing an aqueous liquid containing at least one polymerization initiator, N-vinyl carboxamide monomer or a monomer mixture containing N-vinyl carboxamide into a reactor system, and polymerizing the monomer or monomer mixture to produce the polymer of a N-vinyl carboxamide. The polymers resulting therefrom may be hydrolyzed to provide polymers containing vinyl amine units. Also disclosed herein is an apparatus suitable for producing the polymers.