B01J19/1862

Turbomachine chemical reactor and method for cracking

Chemical reactor (10) and method for cracking are disclosed. A process fluid is accelerated with axial impulse impellers (40A, 40B) to a velocity greater than Mach 1 and, in turn, generating a shock wave (90) in the process fluid by decelerating it in a static diffuser (70) having diverging diffuser passages (72). Temperature increase of the process fluid downstream of the shockwave cracks or splits molecules, such as hydrocarbons entrained in the process fluid, in a single pass, through a unidirectional flow path (F), within a single stage, without recirculating the process fluid for another pass through the same stage. In some embodiments, a system involving at least two turbomachine chemical reactors (110) may provide multiple successive stages of one or more axial impulse impellers (40A, 40B), paired with a diverging passage, static diffuser (70).

SYSTEMS AND METHODS FOR USING SOLID HIGH-LEVEL DISINFECTION CHEMISTRIES TO PRODUCE DISINFECTANT SOLUTIONS
20210322607 · 2021-10-21 ·

Systems and methods for using solid high-level disinfection chemistries to producing disinfectant solutions. In an embodiment, an apparatus comprises: a first container and a second container. The first container is configured to receive water, sodium percarbonate and tetraacetylethylenediamine. The water, the sodium percarbonate, the tetraacetylethylenediamine react within the first container to produce a mixture comprising peroxyacetic acid. The second container is in fluid communication with the first container, wherein the second container is configured to receive an acid and the mixture. The mixture and the acid mix in the second container to produce a disinfectant solution having a pH between 5.0 and 7.0.

Methods for Production of High Impact Polystyrene Having an Improved Rubber Morphology
20210324128 · 2021-10-21 ·

A process for producing high impact polystyrene comprising introducing to a reactor a partially-polymerized mixture comprising at least one vinyl aromatic monomer, an elastomer and reacted vinyl aromatic monomer wherein the partially-polymerized mixture has not undergone phase inversion; polymerizing the partially-polymerized mixture in the reactor to the phase inversion point to form a phase-inverted mixture; recovering a portion of the phase-inverted mixture from the reactor wherein the phase-inverted mixture comprises high impact polystyrene; and introducing another portion of the phase-inverted mixture to another reactor.

DEVICE AND METHOD FOR CONTINUOUSLY PRODUCING CATALYSTS BASED ON LOW-TEMPERATURE COPRECIPITATION
20210316294 · 2021-10-14 ·

The present disclosure discloses a device and a method for continuously producing catalysts based on low-temperature coprecipitation. The device mainly includes: a metal salt preparation kettle, a primary reaction kettle, a secondary reaction kettle, a precipitant preparation kettle, a circulating refrigeration system, an automatic control system, a non-aqueous solvent storage tank and a water storage tank. Independent preparation kettles are provided for rapid dissolution of the raw materials, and can be used to prepare the raw materials for the next batch during the reactions that are carried out in the primary and secondary reaction kettles; the circulating refrigeration system refrigerates the primary and secondary reaction kettles, and thus during the reaction, the low-temperature precipitant makes it possible to offset the precipitation reaction heat and the heat caused by the stirring in the primary reaction kettle, and improve the refrigeration efficiency of the primary reaction kettle.

A METHOD FOR THE PRECIPITATION OF PARTICLES OF A METAL CARBONATE MATERIAL WITHOUT USE OF A CHELATING AGENT

In a method for the precipitation of particles of a metal carbonate material comprising nickel and manganese in an atomic ratio of 0≤Ni:Mn≤1:3, aqueous solutions comprising sulfates or nitrates of nickel and manganese are mixed with aqueous solutions of carbonates or mixtures of carbonates and hydroxides of sodium or potassium in a stirred reactor at pH>7.5 without the use of a chelating agent. Thereby agglomerated particles are formed without any subsequent process steps, in particular no subsequent process at temperatures higher than the precipitation temperature.

SYSTEM FOR GENERATING H2S IN AN ALKALINE MEDIUM AND METHOD OF USING THE SAME
20210276864 · 2021-09-09 ·

Method of producing hydrogen sulfide in an alkaline environment. A mixture having a sodium salt, elemental sulfur (S) and water is added to a reactor for the purpose of generating hydrogen sulfide (H.sub.2S) gas as the main product and sodium sulfate (Na.sub.2SO.sub.4) as a byproduct.

TURBOMACHINE CHEMICAL REACTOR AND METHOD FOR CRACKING

Chemical reactor (10) and method for cracking are disclosed. A process fluid is accelerated with axial impulse impellers (40A, 40B) to a velocity greater than Mach 1 and, in turn, generating a shock wave (90) in the process fluid by decelerating it in a static diffuser (70) having diverging diffuser passages (72). Temperature increase of the process fluid downstream of the shockwave cracks or splits molecules, such as hydrocarbons entrained in the process fluid, in a single pass, through a unidirectional flow path (F), within a single stage, without recirculating the process fluid for another pass through the same stage. In some embodiments, a system involving at least two turbomachine chemical reactors (110) may provide multiple successive stages of one or more axial impulse impellers (40A, 40B), paired with a diverging passage, static diffuser (70).

Esterification unit for producing crude methyl methacrylate, esterification process using said unit and plant comprising said unit

The invention relates to an esterification unit (150) and esterification process for producing crude methyl methacrylate (MMA) from methacrylamide (MAM), which enable particularly to improve the yield, meaning that the organics spent acids are low; and at the same time, providing crude MMA with rather good quality, meaning that MMA concentration in crude MMA is rather high and preferably from 50 wt % to 80 wt %. According to the invention, the esterification unit comprises esterification reactors (1, . . . , 5 (or 6) set up in a serial way so that there is a counter current flow between gaseous phase and liquid phase, the liquid phase flowing from first reactor (1) of the series to last reactor (5 (or 6)), and the gaseous phase flowing from reactor to first reactor (1).

Systems and methods for using solid high-level disinfection chemistries to produce disinfectant solutions
11071800 · 2021-07-27 · ·

Systems and methods for using solid high-level disinfection chemistries to producing disinfectant solutions. In an embodiment, an apparatus comprises: a first container and a second container. The first container is configured to receive water, sodium percarbonate and tetraacetylethylenediamine. The water, the sodium percarbonate, the tetraacetylethylenediamine react within the first container to produce a mixture comprising peroxyacetic acid. The second container is in fluid communication with the first container, wherein the second container is configured to receive an acid and the mixture. The mixture and the acid mix in the second container to produce a disinfectant solution having a pH between 5.0 and 7.0.

SYSTEMS AND PROCESSES INTEGRATING STEAM CRACKING WITH DUAL CATALYST METATHESIS FOR PRODUCING OLEFINS

Processes for producing olefins include integration of steam cracking with a dual catalyst metathesis process. The processes include steam cracking a hydrocarbon feed to form a cracking reaction effluent containing butenes, separating the cracking reaction effluent to produce a cracking C4 effluent including normal butenes, isobutene, and 1,3-butadiene, subjecting the cracking C4 effluent to selective hydrogenation to convert 1,3-butadiene in the cracking C4 effluent to normal butenes, removing isobutene from a hydrogenation effluent to produce a metathesis feed containing normal butenes, and contacting the metathesis feed with a metathesis catalyst and a cracking catalyst directly downstream of the metathesis catalyst to produce a metathesis reaction effluent. Contacting with the metathesis catalyst causes metathesis of normal butenes to produce ethylene, propene, and C5+ olefins, and contacting with the cracking catalyst causes C5+ olefins produced through metathesis to undergo cracking reactions to produce additional propene, ethylene, or both.