B01J2208/00725

Systems for improving yields of hydrocarbon fuels from alcohols
11352568 · 2022-06-07 · ·

Systems are provided that permit temperature control of a catalyst bed for conversion of alcohols to fuel hydrocarbons by modulating the water content of the alcohol feed stream provided to the catalyst bed. In some embodiments a secondary catalyst bed is provided for the conversion of light hydrocarbons found in the initial hydrocarbon product to fuel hydrocarbons that are liquid at ambient temperature and pressure.

Method for filling reactors and for examining catalytic reactors

Disclosed are methods of assistance and documentation of a filling of tubular reactors including recording of filling materials and fill levels of filling materials and documenting the filling materials used, fill levels and results of a catalysis process of tubular reactors produced in such a way.

Apparatus and method for the production of solid dosage forms
11331642 · 2022-05-17 · ·

An apparatus for the production of solid dosage forms is presented, wherein the apparatus comprises a material processing chamber which is operable for manufacturing a product according to a pre-set product formation process path. The apparatus has at least one sensor for continuously monitoring formation of the product in the material processing chamber during the product formation process non-invasively in real time by sensing at least one product functional attribute value and a means for comparing each sensed product functional attribute value with a desirable product functional attribute value for that point on the product formation process path. A controller controls operation of the material processing chamber in response to the sensed product functional attribute value for maintaining the product on the product formation process path.

PROCESS FOR PRODUCING POLYCRYSTALLINE SILICON GRANULATE

Silicon granulate is produced in a fluidized bed reactor having a fluidized bed region fluidized by a gas flow and heated by a heating apparatus. Seed particles and a feed gas including hydrogen and silane and/or halosilane is continuously supplied, and elemental silicon is deposited on the seed particles to form the silicon granulate, which is discharged as a continuous product stream from the reactor. The fluidized bed temperature affects the quality and formation of the product stream, which may be determined as the temperature of an offgas stream from the fluidized bend region. The temperature, as a responding variable may be determined and controlled by means of the mass and energy balance of a defined scheme.

Slurry loop reactor polymerization rate and quality controller

A process and system for maintaining optimum polymerization production in a loop polymerization reactor by continuously and periodically obtaining polymerization results, such as melt index (MI), production rate and ash content of the polymer produced, determining whether each of the results is within desired ranges, storing and averaging recently obtained results in a database within a reaction rate controller program, and when one of the results is out of the desired range modifying at least one reaction parameter set-point such as monomer concentration, catalyst feed rate and reactor temperature to drive any out-of-range polymerization result(s) toward the desired range for that result.

Apparatus and Method for the Production of Solid Dosage Forms
20220097017 · 2022-03-31 ·

An apparatus for the production of solid dosage forms is presented, wherein the apparatus comprises a material processing chamber which is operable for manufacturing a product according to a pre-set product formation process path. The apparatus has at least one sensor for continuously monitoring formation of the product in the material processing chamber during the product formation process non-invasively in real time by sensing at least one product functional attribute value and a means for comparing each sensed product functional attribute value with a desirable product functional attribute value for that point on the product formation process path. A controller controls operation of the material processing chamber in response to the sensed product functional attribute value for maintaining the product on the product formation process path.

Controlling reactor split and a product parameter

A method including a) polymerizing at least one monomer in a gas phase reactor in the presence of a supported multimodal catalyst system to form a multimodal polyethylene product having a reactor split equal to respective weight fractions of resin components in the polyethylene product; b) applying a predetermined formula for a product parameter of the multimodal polyethylene product; c) obtaining incorporation data and production rate data from the reaction based upon the predetermined formula; d) determining an actual hydrogen leading indicator; e) comparing the actual hydrogen leading indicator to a target value for a hydrogen leading indicator to determine a deviation of the actual hydrogen leading indicator from the target value; and f) adjusting an amount of a catalyst precursor being fed to the gas phase reactor to control reactor split and a product parameter.

SYSTEMS FOR IMPROVING YIELDS OF HYDROCARBON FUELS FROM ALCOHOLS
20210269723 · 2021-09-02 ·

Systems are provided that permit temperature control of a catalyst bed for conversion of alcohols to fuel hydrocarbons by modulating the water content of the alcohol feed stream provided to the catalyst bed. In some embodiments a secondary catalyst bed is provided for the conversion of light hydrocarbons found in the initial hydrocarbon product to fuel hydrocarbons that are liquid at ambient temperature and pressure.

Systems and methods for improving yields of hydrocarbon fuels from alcohols
11034891 · 2021-06-15 · ·

Systems and methods are provided that permit temperature control of a catalyst bed for conversion of alcohols to fuel hydrocarbons by modulating the water content of the alcohol feed stream provided to the catalyst bed. Heat generated by exothermic reactions in the catalyst bed can be utilized to pre-heat the alcohol feed stream. In some embodiments a secondary catalyst bed is provided for the conversion of light hydrocarbons found in the initial hydrocarbon product to fuel hydrocarbons that are liquid at ambient temperature and pressure.

COMPUTERIZED SYSTEMS AND METHODS FOR TEMPERATURE PROFILE CONTROL IN A REACTOR WITH A SERIES OF FIXED BEDS
20210268463 · 2021-09-02 ·

Disclosed are systems, servers and methods for improving temperature profile control in a reactor with at least three fixed beds, exothermic reactions and interstage cooling. A model of the temperature differential across the first bed is developed and its error is used to infer unmeasured feed composition disturbances, which are used in the control of the downstream fixed beds for faster response to unmeasured feed composition changes and improved control of the temperature profile throughout the reactor. The first bed model error is then used as an input into an overall model that predicts reactor temperature profiles, which provides advanced notice of reactions in downstream beds, and enables efficient adjustment and compensation to a feed composition change. A Model Predictive Control (MPC) algorithm is applied to adjust the bed intercooling and first bed feed temperature so that the reactor temperature profile can be more precisely controlled.