The present invention relates to a process for removing polymer material from a gas-solids olefin polymerization reactor wherein the gas-solids olefin polymerization reactor is connected to the top part of an outlet vessel via a feed pipe wherein the powder surface of discharged polymer material and the barrier gas injection point are situated in the outlet vessel as such to fulfill the following criteria: R′=X/Y≤2.0; and R″=X/D≥1.0; wherein X=Distance between the powder surface and the barrier gas injection point; Y=Distance between the barrier gas injection point and the vessel outlet; and D=Equivalent outlet vessel diameter, an apparatus for continuously removing polymer material comprising a gas-solids olefin polymerization reactor, an outlet vessel and a feed pipe connecting the gas-solids olefin polymerization reactor with the top part of the outlet vessel and the use of said apparatus for polymerizing alpha-olefin homo- or copolymers having alpha-olefin monomer units of from 2 to 12 carbon atoms and for increasing the barrier gas efficiency of the gas-solids olefin reactor to at least 75%.

A trisilylamine preparation apparatus includes: a reactor in which a trisilylamine synthesis reaction occurs; a reactant supply pipe for supplying reactants to the reactor; a trisilylamine discharge pipe for discharging trisilylamine from the reactor; a reactor heating means for heating the reaction space of the reactor; and a gaseous by-product discharge pipe for discharging a gaseous by-product from the reactor. The reaction space of the reactor is maintained at a temperature that is lower than the decomposition temperature of a reaction by-product generated during the synthesis reaction, the reactor heating means heats the reaction space of the reactor to a temperature that is higher than or equal to the decomposition temperature after trisilylamine is discharged through the trisilylamine discharge pipe, and the gaseous by-product discharge pipe discharges a gaseous by-product comprising a pyrolysate of the reaction by-product, generated through pyrolysis by means of the reactor heating means.

Disclosed are a method and system for propylene polymerization utilizing a loop slurry reactor. The method can include polymerizing propylene in a loop slurry reactor under bulk polymerization conditions to produce polypropylene. The propylene polymerization system can include i) a loop slurry reactor and a heat exchange system that is configured to cool the legs of the loop slurry reactor and/or ii) an inlet manifold that is configured to connect flashline heaters to a separator.

An air lance for removing pellets from tubes includes a conduit body having an inlet end and a bottommost discharge opening, and a poker fixed relative to the conduit body and projecting beyond the bottommost discharge opening to serve as a spacer and poker; wherein a rigid member extends along said conduit body, such that that a hammering force applied to said rigid member where it extends outside of the tube will be transmitted through said rigid member to said poker for dislodging and breaking pellets.

A method of producing a composite product is provided. The method includes providing a fluidized bed of metal oxide particles in a fluidized bed reactor, providing a catalyst or catalyst precursor in the fluidized bed reactor, providing a carbon source in the fluidized bed reactor for growing carbon nanotubes, growing carbon nanotubes in a carbon nanotube growth zone of the fluidized bed reactor, and collecting a composite product comprising metal oxide particles and carbon nanotubes.

Oxidative dehydrogenation catalysts including mixed oxides of Mo, V, Nb, Te, and optionally a promoter may be dissolved in aqueous solutions of oxalic acid. This permits the removal of catalyst and catalyst residues from reactors for the oxidative dehydrogenation of paraffins and particularly ethane.

In an FCC apparatus and process structured packing should be located at the very top of the stripping section in an upper region. The lower region below the structural packing may be equipped with fluidization equipment such as stripping media distributors and one or more gratings. This arrangement enables stripping of entrained hydrocarbons off the incoming catalyst immediately upon entry into the stripping section allowing the entrained hydrocarbon to exit the stripping section with minimized residence time to minimize post-riser cracking. Revamp of stripping sections with tall stripping sections should conducted in this way to improve performance and reduce down-time for equipment installation.

A reactor for producing a synthesis gas from a fuel, with a housing (2) with a combustion part accommodating a first fluidized bed in operation, a riser (3) extending along a longitudinal direction of the reactor (1) and accommodating a second fluidized bed in operation, a down-comer (4) positioned parallel to the riser and extending into the first fluidized bed, and one or more feed channels (33) for providing the fuel to the reactor (1). The reactor (1) further has a riser air chamber section (B) connected to a lower part of the riser (3), the riser air chamber section (B) comprising a cylindrical wall (28) with a plurality of circumferentially located holes (24, 25).

The present invention includes a method for emptying a reactor containing at least one bed of spent catalyst particles and that comprises at least one dump tube, which opens into the reactor in the bottom portion of the bed of particles or underneath the latter. The method comprises the following: a first step of causing a proportion of the catalyst bed to flow out of the reactor via said dump tube; then a second step of expelling out of the reactor the catalyst remainder, by driving towards the opening of the dump tube the catalyst particles remaining in the reactor at the end of the first step, this step being performed by means of a removable device introduced into the reactor via the dump tube,
and is characterised in that said removable device comprises an articulated arm bearing one or more protuberances spirally disposed about a rotary axis.

A system for removing particle agglomerates from a particulate product stream. The system including a product stream inlet configured for receiving the particulate product stream, a diverter system configured for permitting a particulate product having a size less than or equal to a desired size to pass through the diverter system, a carrying fluid source connected to the diverter system configured to feed a carrying fluid into the diverter system to carry the particle agglomerate out of the diverter system during a discharge operation, a collector vessel connected to the diverter system, the collector vessel configured for receiving the particle agglomerate carried out by the carrying fluid from the diverter system during the discharge operation, and a particulate product outlet connected to the diverter system, the particulate product outlet configured for conveying the particulate product to a downstream process.