The present invention relates to a process for the preparation of Sevelamer carbonate from polyallylamine hydrochloride.

The reaction of sodium hypochlorite with sodium bromide is slow, and commonly only part of the bromide is converted to hypobromite. Methods to accelerate the reaction by adding a regulated amount of acid to a solution comprising bleach and bromide are provided, whereby the yield of hypobromite can be increased. The amount of acid added can be predetermined based on the content of a base in the bleach, and acid can be added to neutralize the base. The amount of acid added can be based on a measured parameter of the reaction that is indicative of reaction kinetics. For example, the amount of acid can be actively controlled by measuring pH, absorbance of visible or near Ultraviolet light, or temperature of the reacting solution and adjusting acid.

Provided herein are methods of producing halomethylfuroic and acyloxymethylfuroic acid and ester compounds from furfural starting compounds. For example, 5-chloromethyl-2-furoic acid may be produced from 5-chloromethylfurfural, in the presence of various oxidants. Salts of the furoic acids may also be produced.

Bromine containing compounds, such as calcium bromide, sodium bromide and the like, are prepared in high purity and more quickly with less waste by using a process with two bromination stages and often a third step wherein the crude product mixture can be adjusted to meet specific product requirements. In the first bromination stage, the majority, but not all, of a substrate is brominated using a reductive bromination reaction, the remaining unreacted substrate is converted to product in the second stage through another a reductive bromination reaction, although the specific reagents may be different, wherein the addition of bromine and a reducing agent are carefully monitored.

The disclosed embodiments relate to the manufacture of a precursor co-precipitate material for a cathode active material composition. During manufacture of the precursor co-precipitate material, an aqueous solution containing at least one of a manganese sulfate and a cobalt sulfate is formed. Next, a NH.sub.4OH solution is added to the aqueous solution to form a particulate solution comprising irregular secondary particles of the precursor co-precipitate material. A constant pH in the range of 10-12 is also maintained in the particulate solution by adding a basic solution to the particulate solution.

The present disclosure provides a method for preparing full-gradient particle precursors, and the full-gradient particle precursor prepared thereby. By controlling different types of anion compositions and/or cation compositions gradually changed to other types, and adjusting the pH to match with the species, precipitated particles are deposited to form a slurry, collecting the precipitated particle, treating with water, and drying to yield the particle precursor. After being washed and dried, the particle precursor is further mixed with lithium source, after calcining to yield cathode active particles. The cathode active particles can be used to prepare cathode of lithium-ion battery.

The invention relates to a neutralization plant (100) comprising at least one reaction chamber (102) having a first feed (114) for an acid-containing product and at least one further feed (116) for a base-containing product, wherein at least one of the feeds (114, 116) comprises at least one valve means (118, 120) for controlling the inflow amount into the reaction chamber (102), wherein the ion controller apparatus (104, 204, 205) comprises at least one evaluation device (106, 206) set up for determining at least one actual ion concentration based on an actual pH of the mixture (122) present in the reaction chamber (102) and wherein the ion controller apparatus (104, 204) comprises at least one ion controller device (108, 208) comprising at least one ion controller (110, 210.1, 210.2, 211) set up for controlling the valve means (118, 120) according to the actual ion concentration and a target ion concentration.

The instant disclosure is related to fluidic distributors, fluidic systems, and associated methods and articles. Certain embodiments are related to fluidic distributors that comprise bays including fluidic connections with relative positions that substantially correspond to each other. In some embodiments, a fluidic distributor may comprise bays with electrical interfaces with relative positions that substantially correspond to each other.

The present invention relates to a process for the preparation of Sevelamer carbonate from polyallylamine hydrochloride.

The present invention provides a method for extracting Tremella polysaccharides by using buffer solution, which comprises the following steps: leaching Tremella powder in a buffer solution with heating to obtain the leachate; subjecting the said leachate to solid-liquid separation and obtaining the liquid component which contains Tremella polysaccharides; subjecting the said liquid component to alcohol precipitation, and the precipitate obtained is Tremella polysaccharides. According to the method of the invention, various buffer solutions can achieve the extraction rates of Tremella polysaccharides up to 33:12%, which is 3 to 4 times of that of the traditional water extraction method, and greatly improve the extraction yields of Tremella polysaccharides.