Disclosed is an apparatus and method for providing asymmetric oscillations to a container. The container may include a fluid, a particle, and/or a gas. A vibration driver attached to the container provides asymmetric oscillations. A controller connected to the vibration driver controls an amplitude, frequency, and shape of the asymmetric oscillations. An amplifier amplifies the asymmetric oscillations in response to the controller. A sensor disposed on the vibration driver provides feedback to the controller.

A system for extracting two dimensional materials from a bulk material by functionalization of the bulk material in a reactor.

The present invention is concerned with a process for providing a homogeneous particle-containing slurry comprising the steps of: (a) providing a vessel comprising at least one impeller rotating around a vertical axis of the vessel, wherein a rotational speed n.sub.1 of the at least one impeller is higher than n.sub.min according to equation (1), the vessel further comprising an inlet and an outlet; (b) introducing a particle-containing slurry into the vessel or introducing components forming the particle-containing slurry into the vessel; (c) rotating the at least one impeller at least around the vertical axis for homogenizing and/or maintaining a homogeneous particle distribution within the slurry; (d) withdrawing the homogeneous particle-containing slurry via the outlet; (e) reducing the rotational speed n.sub.1 of the at least one impeller to a reduced rotational speed n.sub.red, whereas n.sub.red is lower than n.sub.1 and higher or equal gas inlet than n.sub.min according to equation (1):

[00001]$\begin{array}{cc}{n}_{\min }=\frac{S{v}^{0.1}{D_p^{0.2}\left(g\frac{\Delta \rho }{{\rho }_f}\right)}^{0.45}{B}^{0.13}}{D_a^{0.85}}& \left(1\right)\end{array}$

A methane cracking apparatus includes a supply pipeline that supplies a gas, a reactor having an interior space, and in which a catalyst for decomposing the gas may be disposed in the interior space, an agitator provided in the interior space and that agitates a material in the interior space, a first discharge pipeline connected to the reactor and that discharges decomposition materials generated as the gas may be decomposed, and a second discharge pipeline connected to the reactor, that discharges the decomposition materials, and disposed on an upper side of the first discharge pipeline.

According to one or more embodiments, non-agglomerated, nano-sized ZSM-22 zeolites may be synthesized by methods comprising operating a mechanical rotation drum unit at a first temperature of from 40° C. to 60° C. and a first speed of from 200 rpm to 1000 rpm for a first time period of from 1.3 hours to 2.7 hours; operating the mechanical rotation drum unit at a second speed of from 30 rpm to 90 rpm for a second time period of from 0.05 hours to 0.4 hours; heating the mechanical rotation drum unit at a ramping temperature of from 8° C./minute to 12° C./minute to a second temperature of from 115° C. to 185° C. at the second speed; operating the mechanical rotation drum unit at the second temperature and the second speed for a third time period of from 30 hours to 90 hours; and cooling the mechanical rotation drum unit at a fourth speed of 0 rpm.

An apparatus to simulate biocide performance in crude oil pipeline conditions is disclosed. The apparatus includes: a reactor to simulate a two-phase crude oil pipeline which includes a crude oil phase above a water phase. The reactor has an agitator to control a flow of the water phase in the reactor in response to a motor that drives an agitation rate of the agitator. A crude oil inlet supplies crude oil to the reactor for the crude oil phase. A water inlet supplies water to the reactor for the water phase. A control circuit is configured by code to control a proportion of the water to the crude oil supplied to the reactor and to control the motor to drive a desired agitation rate of the agitator. A biocide inlet supplies biocide to the reactor. A water sample outlet enables sampling of the water phase of the reactor.

The present invention is concerned with a process for providing a homogeneous particle-containing slurry comprising the steps of: (a) providing a vessel comprising at least one impeller rotating around a vertical axis of the vessel, the vessel further comprising an inlet and an outlet; (b) introducing the particle-containing slurry into the vessel or introducing components forming the particle-containing slurry into the vessel; (c) rotating the at least one impeller at least around the vertical axis for homogenizing and/or maintaining a homogeneous particle distribution within the slurry; (d) withdrawing the homogeneous particle-containing slurry via the outlet; (e) stopping the at least one impeller for a maximum time T, whereby T is calculated according to the following relations: $\begin{array}{cc}{u}_T=\sqrt{\frac{4g\left({\rho }_p-{\rho }_f\right)D_p}{3{\rho }_f{C}_D}}& \left(1\right)\\ C_D=\frac{24}{\mathrm{Re}}[1+0.173{\mathrm{Re}}^{0.657}\end{array}$

A method of manufacture of high-solids hydroxide slurries from caustic calcined carbonate powder is described, whereby the properties of the slurry are its low resistance to shear thinning to facilitate transport, a high stability for transport and storage, ease of reconstitution after long periods of storage, and, as required, a high concentration of chemically reactive species at the particle surface. The method achieves these specifications by mixing caustic calcined carbonate or hydroxide powder with water in an insulated reactor vessel, and agitating the slurry sufficiently such that the hydration reaction causes the water to spontaneously boil, such that the remaining hydration proceeds spontaneously under the fixed conditions of boiling through the water loss. The mixing process is preferably carried out by a shear pump. A viscosity modifier, such as acetic acid, is used to thin the slurry to enable the mixing system to maintain uniform mixing. The reaction is terminated when the boiling has spontaneously ceased and the temperature has spontaneously dropped to a set point though the reactor heat losses, where the processing time is sufficiently long that the slurry meets the desired specifications.

The present invention is concerned with a process for providing a homogeneous particle-containing slurry comprising the steps of: (a) providing a vessel comprising at least one impeller rotating around a vertical axis of the vessel, wherein a rotational speed n.sub.1 of the at least one impeller is higher than n.sub.min according to equation (1), the vessel further comprising an inlet and an outlet; (b) introducing a particle-containing slurry into the vessel or introducing components forming the particle-containing slurry into the vessel; (c) rotating the at least one impeller at least around the vertical axis for homogenizing and/or maintaining a homogeneous particle distribution within the slurry; (d) withdrawing the homogeneous particle-containing slurry via the outlet; (e) reducing the rotational speed n.sub.1 of the at least one impeller to a reduced rotational speed n.sub.red, whereas n.sub.red is lower than n.sub.1 and higher or equal gas inlet than n.sub.min according to equation (1): $\begin{array}{cc}{n}_{\min }=\frac{{\mathrm{Sv}}^{0.1}{D_p^{0.2}\left(g\frac{\Delta \rho }{{\rho }_f}\right)}^{0.45}{B}^{0.13}}{D_a^{0.85}}.& \left(1\right)\end{array}$

According to one or more embodiments, non-agglomerated, nano-sized ZSM-22 zeolites may be synthesized by methods comprising operating a mechanical rotation drum unit at a first temperature of from 40° C. to 60° C. and a first speed of from 200 rpm to 1000 rpm for a first time period of from 1.3 hours to 2.7 hours; operating the mechanical rotation drum unit at a second speed of from 30 rpm to 90 rpm for a second time period of from 0.05 hours to 0.4 hours; heating the mechanical rotation drum unit at a ramping temperature of from 8° C./minute to 12° C./minute to a second temperature of from 115° C. to 185° C. at the second speed; operating the mechanical rotation drum unit at the second temperature and the second speed for a third time period of from 30 hours to 90 hours; and cooling the mechanical rotation drum unit at a fourth speed of 0 rpm.