B01J2219/182

Initiator injection into high pressure LDPE reactors

Methods for operating a high pressure olefin polymerization reactor include the steps of introducing an initiator stream containing ethylene and an initiator compound through an initiator nozzle into the reactor, introducing an olefin stream containing ethylene and an optional comonomer through an olefin nozzle into the reactor, and polymerizing ethylene and optionally the comonomer in the presence of the initiator stream in the reactor under high pressure polymerization conditions to produce an ethylene polymer. The amount of ethylene in the initiator stream is from 0.01 to 2 wt. % of the amount of ethylene in the olefin stream. An injection nozzle that can be used in conjunction with the high pressure reactor also is described.

CHEMICAL REACTOR WITH HIGH SPEED ROTARY MIXING, FOR CATALYTIC THERMAL CONVERSION OF ORGANIC MATERIALS INTO DIESEL AND OTHER LIQUID FUELS, AND APPLICATIONS THEREOF
20220379282 · 2022-12-01 · ·

Chemical reactor with high speed rotary mixing, system thereof, and method thereof, for catalytic thermal conversion of organic (hydrocarbon-containing) materials (coal, plastics, rubber, plant matter, wood shavings, biomass, organic wastes) into diesel and other liquid fuels (automobile or/and jet engine fuels). Relevant to non-conventional commercial scale production of liquid fuels, and to commercial scale processing and disposing of organic waste materials. Chemical reactor includes: integrated combination of a reactor stationary assembly (RSA), having only stationary components remaining stationary during chemical reactor operation, and a reactor rotary mixing assembly (RRMA), having only rotatable components rotating during chemical reactor operation. May include anti-abrasion shield for shielding inner surface of reactor central housing from abrasion during chemical reactor operation. Rotor may include a reinforcement disc. Rotor blades or/and reinforcement disc may include rotor-based performance and process control structural features (openings, or/and protrusions, or/and depressions), for additionally controlling performance of the rotor.

Thermal conversion vessel used in a process for amidification of acetone cyanohydrin

The invention relates to a thermal conversion vessel (200) used during amidification step of acetone cyanohydrin (ACH), in the industrial process for production of a methyl methacrylate (MMA) or methacrylic acid (MAA). The thermal conversion vessel (200) is used for converting an hydrolysis mixture of α-hydroxyisobutyramide (HIBAM), α-sulfatoisobutyramide (SIBAM), 2-methacrylamide (MACRYDE) and methacrylique acid (MAA), into a mixture of 2-methacrylamide (MACRYDE). It comprises:—at least one compartment (C1, C2, C3, . . . Ci) comprising an inner wall (206a, 206b, . . . 206i) separating said compartment into two communicating parts (C1a, C1b) by a passage provided between the bottom of said vessel and said inner wall,—said compartment having a space above said inner wall, for separating gas phase from liquid phase during thermal conversion,—said compartment being connected to an outlet valve (204a, 204b, . . . 204i). Such vessel allows obtaining a high yield thermal conversion in very safe conditions.

Chemical reaction apparatus

In order to provide a chemical reaction apparatus that can suppress a situation where microwaves are concentrated on a partial portion in a reactor, and that can more uniformly irradiate a content with the microwaves, a chemical reaction apparatus includes: a horizontal flow-type reactor in which a liquid content horizontally flows with an unfilled space being provided thereabove; a microwave generator that generates microwaves; and a waveguide that transmits the microwaves generated by the microwave generator to the unfilled space in the reactor, wherein a top of the reactor is curved with respect to a flow direction of the content.

Multi-compartment reactor and method for controlling retention time in a multi-compartment reactor

A method is disclosed for controlling retention time in a reactor, such as an autoclave, having a plurality of compartments separated by dividers with underflow openings. A retention time of the reaction mixture is calculated and compared with an optimal retention time, and the volumes of the reaction mixture in the compartments are adjusted while maintaining the flow rate of the reaction mixture, so as to change the retention time to a value which is closer to the optimal retention time. The reactor may include a level sensor in the last compartment for generating volume data; a control valve for controlling the liquid level in the last compartment; and a controller which receives volume data from the level sensor and controls operation of the control valve.

SURFACE TREATING METHOD USING TAYLOR REACTOR
20170334726 · 2017-11-23 · ·

Disclosed herein is a surface treating method using a Taylor reactor wherein a washing, neutralization, heavy metal removal, etc. can be efficiently carried out, while saving a surface treating time and a treatment liquid and enhancing a treatment efficiency by using a Taylor eddy current which in general is formed at a Taylor reactor. The surface treatment method using a Taylor reactor formed of a cylindrical reaction chamber and a cylindrical rotation body which is configured to rotate in the reaction chamber may include (1) a supply step wherein a surface treatment thing and a surface treatment liquid are supplied into the reaction chamber; and (2) a treatment step wherein the surface treatment thing is stayed in the reaction chamber while rotating the cylindrical rotation body, and the stay time of the surface treatment thing is in a range of 1 minute to 6 hours.

METHOD FOR THERMAL PRECONDITIONING OF NATURAL GRAPHITE FLAKES USING ELECTROMAGNETIC WAVES

An apparatus for processing graphite particles is disclosed. The apparatus may comprise an electromagnetic radiation emitting device including a microwave device coupled to the reaction chamber for the creation of electromagnetic waves, the electromagnetic waves comprising microwaves. The apparatus may also comprise an inlet attached to the reaction chamber for introducing graphite particles, and an outlet attached to the reaction chamber for allowing processed graphite particles to exit the reaction chamber. The graphite particles in the reaction chamber thermally altered by exposure to the electromagnetic radiation such that the graphite particles are heated

Reactor for Multi-Phase Composition

A reactor comprising a first portion having a generally cylindrical housing, an inlet at one end of said first portion housing, the opposed end of said first portion housing being the outlet of said first portion, where said first portion includes a rotatable shaft positioned axially within said housing and including at least two shearing paddles extending radially from said rotatable shaft and a second portion having a generally frustoconical housing having a first end larger than a second end, said first end constituting an inlet to said second portion and coextensive with said opposed end of said first portion housing, and an outlet at said second end, where said second portion includes a rotatable shaft positioned axially within said housing and including at least one generally helical flight extending radially from said rotatable shaft.

POLY-SILICON MANUFACTURING APPARATUS AND METHOD USING HIGH-EFFICIENCY HYBRID HORIZONTAL REACTOR

According to the present invention, there is provided a polysilicon production apparatus including: a horizontal reaction tube having an inlet port through which gaseous raw materials including reactant gases and a reducing gas are supplied, an outlet port through which residual gases exit, a reaction surface with which the gaseous raw materials come into contact, and bottom openings through which molten polysilicon produced by the reactions of the gaseous raw materials is discharged; and first heating means adapted to heat the reaction surface of the horizontal reaction tube. The horizontal reaction tube includes reaction regions consisting of first reaction regions where polysilicon is deposited and second reaction regions where reaction by-products are converted to the reactant gases. The first reaction regions are connected in series with the second reaction regions. Also provided is a polysilicon production method using the polysilicon production apparatus.

Method for Temperature Data Acquisition

A method for determining temperature information for a plurality of tubes in a furnace where one or more digital images provide temperature information for imaged tubes, and temperature information for non-imaged tubes is determined from the temperature information for the imaged tubes and measured temperatures of combined effluent from the imaged and non-imaged tubes.