The subject of the invention is a drive for an ultra-high-energy pulsatory-rotary mill that can be applied in the laboratory-class equipment. The objective of the invention is the use of the drive for an ultra-high-energy pulsatory-rotary mill which allows to accomplish the three-dimensional milling process in three axes with simultaneous control of amount of the supplied mechanical energy in real time. The rotary-planetary drive comprises an alternating-current motor (1) constituting the rotary motion drive and powered through an inverter (2) connected with the rotary mechanical energy counter (3), and an alternating-current motor (4) driving actuator (5) constituting the pulsatory motion drive and powered by inverter (6) connected with the pulsatory mechanical energy counter (7). Signals from mechanical energy counters (7) and (3) are conveyed to the digital recorder (8).

The present invention relates to a container for a stirrer used in a stirrer stirring objects through a centrifugal force. The container for the stirrer includes a container body of which the top is opened and in which a receiving space is formed, an outer lid coupled to the top of the container body, and a crushing unit including a supporting member disposed in the receiving space, and a crushing member extending outward from the supporting member and crushing and stirring the objects received in the receiving space. Thus, nanoparticle-sized objects can be rapidly crushed and stirred without agglomeration.

The present invention relates to a container for a stirrer used in a stirrer stirring objects through a centrifugal force. The container for the stirrer includes a container body of which the top is opened and in which a receiving space is formed, an outer lid coupled to the top of the container body, and a crushing unit including a supporting member disposed in the receiving space, and a crushing member extending outward from the supporting member and crushing and stirring the objects received in the receiving space. Thus, nanoparticle-sized objects can be rapidly crushed and stirred without agglomeration.

A unit for grinding biological samples, comprising a grinding device including at least two tubes having different volumes, suitable for being mounted on a support of the grinding device, each tube comprising an inner space having a height (h) along the axis of the corresponding tube, and being intended to contain samples to be ground, means for driving the support in a precession movement, the support having an axis the position of which varies by describing a cone, each tube being subjected to a movement (d) defined by the projection, onto the axis of said cone, of the distance between the extreme positions of a same point of the tube during the precession movement.

A unit for grinding biological samples, comprising a grinding device including at least two tubes having different volumes, suitable for being mounted on a support of the grinding device, each tube comprising an inner space having a height (h) along the axis of the corresponding tube, and being intended to contain samples to be ground, means for driving the support in a precession movement, the support having an axis the position of which varies by describing a cone, each tube being subjected to a movement (d) defined by the projection, onto the axis of said cone, of the distance between the extreme positions of a same point of the tube during the precession movement.

Methods for forming black phosphorus alloys and exfoliating black phosphorus alloys. A method for forming black phosphorus alloys includes providing phosphorus inside a vessel and providing an element inside the vessel. Media is provided inside the vessel and the phosphorus, the element, and the media are sealed under a gas within the vessel. The phosphorus and the element are mechanically milled with the media to produce black phosphorus that is covalently bonded with the element. A method for exfoliating a black phosphorus alloy includes mixing a milled black phosphorus alloy with a solvent and mixing a milled black phosphorus alloy with a solvent. The milled black phosphorus alloy and solvent mixture are then extracted from the milling apparatus, which may be a planetary ball mill, a vibratory mill, a tumbler ball mill, a mixer mill, a rod mill, an attrition mill, or a shaker mill.

Methods for forming black phosphorus alloys and exfoliating black phosphorus alloys. A method for forming black phosphorus alloys includes providing phosphorus inside a vessel and providing an element inside the vessel. Media is provided inside the vessel and the phosphorus, the element, and the media are sealed under a gas within the vessel. The phosphorus and the element are mechanically milled with the media to produce black phosphorus that is covalently bonded with the element. A method for exfoliating a black phosphorus alloy includes mixing a milled black phosphorus alloy with a solvent and mixing a milled black phosphorus alloy with a solvent. The milled black phosphorus alloy and solvent mixture are then extracted from the milling apparatus, which may be a planetary ball mill, a vibratory mill, a tumbler ball mill, a mixer mill, a rod mill, an attrition mill, or a shaker mill.

A method of adapting a centrifugal machine that is a dual asymmetric centrifugal mixer or a planetary mill, used for mixing materials, for grinding one or more materials; it includes positioning in a container of the machine, non-spherical grinding media, and securing a lid on the opening of the container, wherein the bases of the units of the non-spherical grinding media are prevented from toppling by having a shortest distance between the center of mass of the unit of non-spherical grinding media and a base be less than half of the width of the base; or securing the lid sufficiently near the top of the units of the non-spherical grinding media such that when a unit of the non-spherical grinding media tilts, the unit of the non-spherical grinding media contacts the lid, the lid acting as an obstacle preventing the unit of the non-spherical grinding media from toppling.

A method of adapting a centrifugal machine that is a dual asymmetric centrifugal mixer or a planetary mill, used for mixing materials, for grinding one or more materials; it includes positioning in a container of the machine, non-spherical grinding media, and securing a lid on the opening of the container, wherein the bases of the units of the non-spherical grinding media are prevented from toppling by having a shortest distance between the center of mass of the unit of non-spherical grinding media and a base be less than half of the width of the base; or securing the lid sufficiently near the top of the units of the non-spherical grinding media such that when a unit of the non-spherical grinding media tilts, the unit of the non-spherical grinding media contacts the lid, the lid acting as an obstacle preventing the unit of the non-spherical grinding media from toppling.

A sonic reactor for transferring kinetic energy to a process fluid medium has a resonant element horizontally oriented and mounted to the two resonance units using two or more nodal support rings located at the nodal positions of the resonant element. The nodal support rings are adjustable in position relative to the resonant element and the resonance units to permit positioning of the rings directly at the nodal positions during operation. The sonic reactor has a grinding or mixing chamber mounted at one or both of the free ends of the resonant element. The sonic reactor is used for applications that include fly ash beneficiation, pulverization and dispersion; fine ore grinding; preparing ready mix cement formulations; oil sands cuttings for oil recovery; spilled oil, water and oily water storage treatment; organic and inorganic industrial wastewater treatment; environmental remediation of contaminated soils; sodium dispersion and destruction of PCBs; biosludge conditioning; cellulosic biofuels processing; lignin processing; dispersion and deagglomeration of pigments; and dye destruction.