The disclosure is directed to a sample preparation apparatus for grinding or homogenizing test samples. More specifically, the disclosure relates to grinding samples using rotational and linear motion. Grinding samples can be accomplished with an apparatus with a slider-crank mechanism that is attached to an oscillating connecting linkage. The amplitude of oscillatory motion can be greater than or equal to a length of a sample processing chamber.

A method for starting a grinding tube with an assigned drive device, wherein during the operation of the grinding tube a grinding mode and a charge release mode can be set such that a particularly reliable monitoring of the state of charge located in the grinding tube is ensured, where the grinding tube is rotated and, at a first rotational angle, a first actual torque is detected, a setpoint torque is calculated for a second, relatively large rotational angle based on the first actual torque, an actually occurring, second actual torque is detected when the second rotational angle is reached, an investigation is performed to determine the difference of the second actual torque from the setpoint torque, and the charge release mode of the grinding tube is set when the second actual torque is within the threshold range, otherwise the grinding tube is operated in the grinding mode.

A method for starting a grinding tube with an assigned drive device, wherein during the operation of the grinding tube a grinding mode and a charge release mode can be set such that a particularly reliable monitoring of the state of charge located in the grinding tube is ensured, where the grinding tube is rotated and, at a first rotational angle, a first actual torque is detected, a setpoint torque is calculated for a second, relatively large rotational angle based on the first actual torque, an actually occurring, second actual torque is detected when the second rotational angle is reached, an investigation is performed to determine the difference of the second actual torque from the setpoint torque, and the charge release mode of the grinding tube is set when the second actual torque is within the threshold range, otherwise the grinding tube is operated in the grinding mode.

The subject of the invention is a drive for an ultra-high-energy pulsatory-rotary mill that can be applied in the laboratory-class equipment. The objective of the invention is the use of the drive for an ultra-high-energy pulsatory-rotary mill which allows to accomplish the three-dimensional milling process in three axes with simultaneous control of amount of the supplied mechanical energy in real time. The rotary-planetary drive comprises an alternating-current motor (1) constituting the rotary motion drive and powered through an inverter (2) connected with the rotary mechanical energy counter (3), and an alternating-current motor (4) driving actuator (5) constituting the pulsatory motion drive and powered by inverter (6) connected with the pulsatory mechanical energy counter (7). Signals from mechanical energy counters (7) and (3) are conveyed to the digital recorder (8).

The subject of the invention is a drive for an ultra-high-energy pulsatory-rotary mill that can be applied in the laboratory-class equipment. The objective of the invention is the use of the drive for an ultra-high-energy pulsatory-rotary mill which allows to accomplish the three-dimensional milling process in three axes with simultaneous control of amount of the supplied mechanical energy in real time. The rotary-planetary drive comprises an alternating-current motor (1) constituting the rotary motion drive and powered through an inverter (2) connected with the rotary mechanical energy counter (3), and an alternating-current motor (4) driving actuator (5) constituting the pulsatory motion drive and powered by inverter (6) connected with the pulsatory mechanical energy counter (7). Signals from mechanical energy counters (7) and (3) are conveyed to the digital recorder (8).

A sample crushing device is provided having a function of stably absorbing vibration of a support member supporting a sample container and vibration of other members which accompanies the vibration. When a rotating shaft 20 is rotated and driven by rotation driving mechanism, revolving motions of a first support member 12 around an axis line C1 of a rotating shaft 20 and rotational movement of an inclined shaft 10 around an axis line C2 arm restrained by a base 1 via first elastic members 14. As a result, the first support member 12 and sample containers 41 are vibrated in plural directions, and samples housed in the sample containers 41 are crushed by crushing media.

Vibration of the first support member 12 in plural directions is absorbed by a base 1 via the first elastic members 14 coupled with each of the first support member 12 and the base 1.

This invention is directed to a sample preparation apparatus for grinding or homogenizing test samples. More specifically, but without restriction to the particular embodiments hereinafter described in accordance with the best mode of practice, this invention relates to a reciprocating apparatus based upon a slider-crank mechanism for grinding or homogenizing of a sample within a sample vial attached to an oscillating connecting linkage that has an amplitude of oscillatory motion equal to or greater than the length of the sample processing chamber.

A holding and opening mechanism for a pivoting element which is mounted to be pivotable relative to a supporting element about a first axle via a joint, with a pivoting arm acting between the pivoting element and the supporting element is provided. The pivoting arm is pivotally mounted about a second axle wherein the free end of the pivoting arm acts on a control surface of a guide element. A torsion spring is provided which acts on the pivoting arm in the direction around the second axle, a fixed part and a part pivotable relative thereto likewise provided, with the one part including the guide element and the other part including the pivoting arm. The pivotable part is adapted to be pivotable relative to the fixed part about the joint and the first axle, the pivotable part is connected to the pivoting arm and the pivoting element and the fixed part is connected to the supporting element, the control surface in cooperation with the torsion spring and the pivoting arm determines the holding and opening force via the pivot angle of the pivoting element.

Machine having a rotor which is mounted in a cantilevered fashion on a bearing and has a rotational axis along which a free, subsequently non-mounted rotor end runs starting from the bearing, the rotor end having a rotor end side which is spaced apart from a fixed rotor opposing side by a gap, and which, during operation of the machine when the rotor is rotating, is deflected with respect to the rotational axis as a result of imbalance of the free, non-mounted rotor end, or as a result of externally applied forces, wherein the rotor end side is curved or beveled so as to drop away at least in its end region towards its edge and in a direction towards the bearing.

Machine having a rotor which is mounted in a cantilevered fashion on a bearing and has a rotational axis along which a free, subsequently non-mounted rotor end runs starting from the bearing, the rotor end having a rotor end side which is spaced apart from a fixed rotor opposing side by a gap, and which, during operation of the machine when the rotor is rotating, is deflected with respect to the rotational axis as a result of imbalance of the free, non-mounted rotor end, or as a result of externally applied forces, wherein the rotor end side is curved or beveled so as to drop away at least in its end region towards its edge and in a direction towards the bearing.