B22F1/065

Method for Manufacturing Porous Metal Body, and Porous Metal Body
20230084462 · 2023-03-16 ·

A method for manufacturing a porous metal body according to the present invention includes: a surface oxidizing step of heating a titanium-containing powder in an atmosphere containing oxygen at a temperature of 250° C. or more for 30 minutes or more to provide a surface-oxidized powder; and a sintering step of depositing the surface-oxidized powder in a dry process, and sintering the surface-oxidized powder by heating it in a reduced pressure atmosphere or an inert atmosphere at a temperature of 950° C. or more.

SPHERICAL Ti-BASED POWDER AND MANUFACTURING METHOD THEREFOR

A spherical Ti-based powder and a manufacturing method therefor are provided. The spherical Ti-based powder has a 50% particle size (D50) of 1 to 250 μm in a cumulative particle size distribution based on volume, in which a total amount of oxygen and hydrogen is less than 3000 ppm by mass, an area defect rate in a cross-section of the spherical Ti-based powder is less than 0.100%, and an area circularity of the spherical Ti-based powder in a secondary projection image is 0.90 or more. The spherical Ti-based powder can be obtained by subjecting a pulverized Ti-based powder to a fusion and solidification treatment using a thermal plasma in which a flow rate of hydrogen gas as a working gas is adjusted to less than 0.3 l/min.

SPHERICAL Ti-BASED POWDER AND MANUFACTURING METHOD THEREFOR

A spherical Ti-based powder and a manufacturing method therefor are provided. The spherical Ti-based powder has a 50% particle size (D50) of 1 to 250 μm in a cumulative particle size distribution based on volume, in which a total amount of oxygen and hydrogen is less than 3000 ppm by mass, an area defect rate in a cross-section of the spherical Ti-based powder is less than 0.100%, and an area circularity of the spherical Ti-based powder in a secondary projection image is 0.90 or more. The spherical Ti-based powder can be obtained by subjecting a pulverized Ti-based powder to a fusion and solidification treatment using a thermal plasma in which a flow rate of hydrogen gas as a working gas is adjusted to less than 0.3 l/min.

SPHERICAL Ti-BASED POWDER AND MANUFACTURING METHOD THEREFOR

A spherical Ti-based powder and a manufacturing method therefor are provided. The spherical Ti-based powder has a 50% particle size (D50) of 1 to 250 μm in a cumulative particle size distribution based on volume, in which a total amount of oxygen and hydrogen is less than 3000 ppm by mass, an area defect rate in a cross-section of the spherical Ti-based powder is less than 0.100%, and an area circularity of the spherical Ti-based powder in a secondary projection image is 0.90 or more. The spherical Ti-based powder can be obtained by subjecting a pulverized Ti-based powder to a fusion and solidification treatment using a thermal plasma in which a flow rate of hydrogen gas as a working gas is adjusted to less than 0.3 l/min.

ADDITIVELY MANUFACTURED MEDICAL IMPLANTS, METHODS FOR FORMING SAME, AND ZIRCONIUM ALLOY POWDER FOR FORMING SAME

The present disclosure provides zirconium powder particles comprising pure zirconium powder particles with an oxide layer ranging from 0.05 to 5 microns in thickness and/or zirconium alloy powder particles with an oxide layer ranging from 0.05 to 5 microns in thickness. In some embodiments, the zirconium powder particles may be spherical particles, the zirconium powder particles may range from 5 microns to 125 microns in diameter, and/or the zirconium powder particles may have a median particle size ranging from 25 to 70 microns in diameter. The present disclosure further provides methods of producing medical implants or medical implant components by a process that comprises selectively applying energy to such zirconium powder particles to build the medical implants or the medical implant components. In some embodiments, the methods comprise repeatedly forming a layer of zirconium powder particles and irradiating the layer of zirconium powder particles with an energy source.

Methods of nanostructure formation and shape selection
11471939 · 2022-10-18 · ·

Methods for forming nanostructures of various shapes are disclosed. Nanocubes, nanowires, nanopyramids and multiply twinned particles of silver may by formed by combining a solution of silver nitrate in ethylene glycol with a solution of poly(vinyl pyrrolidone) in ethylene glycol. Hollow nanostructures may be formed by reacting a solution of solid nanostructures comprising one of a first metal and a first metal alloy with a metal salt that can be reduced by the first metal or first metal alloy. Nanostructures comprising a core with at least one nanoshell may be formed by plating a nanostructure and reacting the plating with a metal salt.

Methods of nanostructure formation and shape selection
11471939 · 2022-10-18 · ·

Methods for forming nanostructures of various shapes are disclosed. Nanocubes, nanowires, nanopyramids and multiply twinned particles of silver may by formed by combining a solution of silver nitrate in ethylene glycol with a solution of poly(vinyl pyrrolidone) in ethylene glycol. Hollow nanostructures may be formed by reacting a solution of solid nanostructures comprising one of a first metal and a first metal alloy with a metal salt that can be reduced by the first metal or first metal alloy. Nanostructures comprising a core with at least one nanoshell may be formed by plating a nanostructure and reacting the plating with a metal salt.

Method for producing magnetic powder and magnetic powder

A method for producing a magnetic powder includes the steps of: mixing neodymium oxide, boron, and iron to prepare a first mixture; adding and mixing calcium to the first mixture to prepare a second mixture; mixing an alkali metal with the second mixture to prepare a third mixture; and placing a carbon sheet on the third mixture, placing silica sand (SiO.sub.2 sand) thereon, and then heating the same to a temperature of 800° C. to 1100° C.

Boron-containing titanium-based composite powder for 3D printing and method of preparing same

This invention discloses a boron-containing titanium-based composite powder for 3D printing, consisting of 0.5%-2% by weight of titanium diboride and 98%-99.5% by weight of titanium sponge. The invention further discloses a method of preparing such composite powder, where the element boron is introduced to the titanium powder through rapid solidification, which significantly improves the solid solubility of boron in Ti, enabling the introduction of part of the boron into the titanium matrix to form supersaturated solid solutions. The reinforcement phase TiB in the boron-containing titanium-based composite powder prepared herein can be precisely controlled in grain size ranging from the nanometer scale to the micrometer scale through temperature or energy density, thereby preparing the titanium-based composite materials with different sizes of reinforcement phases to meet different mechanical requirements.

Mechanically alloyed powder feedstock

Disclosed herein are embodiments of mechanically alloyed powder feedstock and methods for spheroidizing them using microwave plasma processing. The spheroidized powder can be used in metal injection molding processes, hot isostatic processing, and additive manufacturing. In some embodiments, mechanical milling, such as ball milling, can be used to prepare high entropy alloys for microwave plasma processing.