B22F1/145

METHOD OF PRODUCING PHOSPHATE-COATED SmFeN-BASED ANISOTROPIC MAGNETIC POWDER AND PHOSPHATE-COATED SmFeN-BASED ANISOTROPIC MAGNETIC POWDER

A method of producing a phosphate-coated SmFeN-based anisotropic magnetic powder, the method including performing a phosphate treatment including adding an inorganic acid to a slurry containing a raw material SmFeN-based anisotropic magnetic powder, water, a phosphate compound, and a rare earth compound so that the slurry is adjusted to have a pH of at least 1 and not higher than 4.5 to obtain a phosphate-coated SmFeN-based anisotropic magnetic powder having a surface coated with a phosphate.

HIGH-STRENGTH AND HIGH-PLASTICITY TITANIUM MATRIX COMPOSITE AND PREPARATION METHOD THEREOF

The present invention provides a high-strength and high-plasticity titanium matrix composite and a preparation method thereof. The preparation method includes: preparing high-oxygen hydride-dehydride titanium powder using a high-temperature rotary ball grinding treatment process, in which the prepared hydride-dehydride titanium powder has a particle size of 10-40 μm, and has an oxygen content of 0.8-1.5 wt. %; preparing high-purity ultra-fine oxygen adsorbent powder using a wet grinding method of high-energy vibration ball grinding treatment process; in which a purity of the oxygen adsorbent powder is ≥99.9%, and a particle size of the oxygen adsorbent powder is ≤8 μm; mixing the high-oxygen hydride-dehydride titanium powder with the oxygen adsorbent powder in a protective atmosphere, and then press-forming the powder obtained after mixing to obtain a raw material blank; and performing atmosphere protective sintering treatment on the raw material blank to obtain a titanium matrix composite. The method prepares a titanium matrix composite reinforced by in-situ self-generating multi-scale Ca—Ti—O, TiC, TiB particles. The microstructure and grains are effectively refined, and the strength and plasticity of the material are significantly improved.

Method for manufacturing magnetic alloy powder having certain element distributions in thickness direction
11680306 · 2023-06-20 · ·

A method for manufacturing magnetic alloy powder constituted by magnetic grains whose alloy phase is coated with an oxide film, includes: providing a material powder for magnetic alloy whose Fe content is 96.5 to 99 percent by mass and which also contains Si and at least one of non-Si elements (element M) that oxidize more easily than Fe; and heat-treating the material powder and thus forming an oxide film on a surface of each grain constituting the material powder, to obtain a magnetic alloy powder, wherein a content of Fe in the alloy phase is higher than in the material powder; and at a location in the oxide film where its content of Si is in element distributions in a film thickness direction is highest, the content of Si is higher than a content of Fe, and also higher than its content of element M, at the location.

Control of nanostructure and activity by alloying and/or segregation

A method for synthesis of PtNi smooth surface core/shell particles or Nano cages and porous nanocages from segregated nanoparticles.

Control of nanostructure and activity by alloying and/or segregation

A method for synthesis of PtNi smooth surface core/shell particles or Nano cages and porous nanocages from segregated nanoparticles.

Core-shell nanoparticles comprising same element of different isotopes

A core-shell nanoparticle is provided that includes a core comprising a first isotope of an element; an isolation layer surrounding the core; and a shell layer surrounding the isolation layer, wherein the shell layer comprises a second isotope of the element, with the first isotope being different than the second isotope. Methods are also provided for forming such core-shell nanoparticles.

Anisotropic magnetic powders and method of producing the same
11676748 · 2023-06-13 · ·

A method of producing anisotropic magnetic powders comprising obtaining a precipitate containing an element R, iron and lanthanum from a solution including R, iron and lanthanum, wherein R is at least one selected from the group consisting of Sc, Y, Pr, Nd, Pm, Sm, Gd, Tb, Dy, Ho, Er, Tm and Lu; obtaining an oxide containing R, iron and lanthanum from the precipitate; treating the oxide with a reducing gas to obtain a partial oxide; obtaining alloy particles by reduction diffusion of the partial oxide at a temperature in the range of 920° C. to 1200° C.; and nitriding the alloy particles to produce an anisotropic magnetic powder represented by the following general formula: R.sub.v-xFe.sub.(100-v-w-z)N.sub.wLa.sub.xW.sub.z, where 3≤v−x≤30, 5≤w≤15, 0.08≤x≤0.3, and 0≤z≤2.5.

Anisotropic magnetic powders and method of producing the same
11676748 · 2023-06-13 · ·

A method of producing anisotropic magnetic powders comprising obtaining a precipitate containing an element R, iron and lanthanum from a solution including R, iron and lanthanum, wherein R is at least one selected from the group consisting of Sc, Y, Pr, Nd, Pm, Sm, Gd, Tb, Dy, Ho, Er, Tm and Lu; obtaining an oxide containing R, iron and lanthanum from the precipitate; treating the oxide with a reducing gas to obtain a partial oxide; obtaining alloy particles by reduction diffusion of the partial oxide at a temperature in the range of 920° C. to 1200° C.; and nitriding the alloy particles to produce an anisotropic magnetic powder represented by the following general formula: R.sub.v-xFe.sub.(100-v-w-z)N.sub.wLa.sub.xW.sub.z, where 3≤v−x≤30, 5≤w≤15, 0.08≤x≤0.3, and 0≤z≤2.5.

POWDER PROCESSING SYSTEM AND METHOD FOR POWDER HEAT TREATMENT

A method for heat treating metal alloy powder includes (a) introducing metal alloy powder to a chamber having a floor and a sidewall; (b) flowing a fluidizing gas through the floor and into the chamber to fluidize the metal alloy powder in the chamber; (c) flowing an additional gas through the sidewall into the chamber; and (d) heating the chamber to heat treat the metal alloy powder in the chamber. A system for heat treating metal alloy powder includes an inner chamber having a porous floor and a porous sidewall; an outer chamber, the inner chamber being inside of the outer chamber and defining an annular space between the outer chamber and the inner chamber, wherein the outer chamber and the inner chamber are inside a furnace; a source of fluidizing gas connected to the porous floor through the annular space; and a source of additional gas communicated with the porous sidewall through the annular space.

RARE EARTH ALUMINUM ALLOY POWDER APPLICABLE FOR ADDITIVE MANUFACTURING AND PREPARATION METHOD THEREOF

A method for preparing a rare earth aluminum alloy powder applicable for additive manufacturing includes: heating and melting aluminum ingots into an aluminum melt; adding required alloy elements to the aluminum melt to obtain an alloy melt in which the alloy elements are present in the following preset percentages by weight: 1.00% to 10.00% of Ce, 0.05% to 8.00% of Mg, 0.10% to 7.50% of Y, 0.10% to 2.50% of Zr, less than 0.1% of impurities, and the balance aluminum; leading out the alloy melt through a fluid guiding pipe, and impacting the alloy melt with a high-pressure gas flow so that the alloy melt is atomized into fine droplets under an action of surface tension, and solidified into spherical alloy powder; and collecting the spherical alloy powder in a vacuum collector, and screening and drying the spherical alloy powder to obtain the rare earth aluminum alloy powder.