The present disclosure provides a preparation method of a metal powder material. An alloy sheet composed of a matrix phase and a dispersive phase with different chemical reactivities is prepared by the rapid solidification technique of alloy melt. Metal powder is prepared by the reaction of the alloy sheet and an acid solution. Please refer to the description for the detailed preparation method. This method is simple in operation, can be used to prepare many kinds of metal powder materials of different shapes and at the nanometer scale, the submicron scale and the micron scale, and has a good application prospect in the fields of catalysis, powder metallurgy and 3D printing.

Herein disclosed is a method of making a fuel cell including forming an anode, a cathode, and an electrolyte using an additive manufacturing machine. The electrolyte is between the anode and the cathode. Preferably, electrical current flow is perpendicular to the electrolyte in the lateral direction when the fuel cell is in use. Preferably, the method comprises making an interconnect, a barrier layer, and a catalyst layer using the additive manufacturing machine.

Articles are manufactured using self-propagating high-temperature synthesis (SHS) reactions. Particulates including reactants can be blended to form a particulate blend. The particulate blend can be preformed. The preform article can be heated to a pre-heat temperature being below an auto-activation temperature and above a minimum compression activated synthesis temperature. Compressive stress can be exerted on the preform article at the pre-heat temperature to initiate the SHS reaction between the reactants and thereby form a product metallic compound. At approximately peak temperature, a flow stress of the product metallic compound can be exceeded to substantially reduce porosity and thereby form a shaped substantially dense article.

A method for preparing an oxygen-free passivated titanium or titanium-alloy powder product by means of gas-solid fluidization is provided. The new method includes placing the metal halide and the titanium powder which meet formula requirements into a gasifier and a fluidized bed reactor respectively; heating the gasifier to gasify the metal halide, and introducing dry argon and halide gas into the fluidized bed reactor; opening the fluidized bed, heating the fluidized bed, fluidizing the titanium powder after the introduction of the argon and the metal halide gas, and cooling the product to obtain the titanium powder subjected to oxygen-free passivation using metal chloride; molding the oxygen-free passivated titanium powder into a green body with powder metallurgy technology; and sintering the green body in vacuum or argon atmosphere according to the molding technology, and after temperature rise treatment, performing a densification sintering operation to obtain a high-performance titanium product component.

A nanocomposite metal material includes a carrier formed of Zr and two-element metal particles supported on the carrier. The two-element metal is formed of Cu and Ni, and a degree of oxidation of the carrier is more than 31% and 100% or less. In a case where the nanocomposite metal material is disposed in a reaction furnace of a thermal reactor, the inside of the reaction furnace is brought into a vacuum state, and the inside of the reaction furnace is heated to a temperature range of 250° C. or higher and 350° C. or lower with a heating mechanism included in the thermal reactor while supplying at least one of hydrogen gas and deuterium gas into the reaction furnace, excessive heat of the nanocomposite metal material is 100 W/kg or more.

A composite for a porous transport layer may include a particulate substrate including at least one selected from a group consisting of an oxide of a first metal and a second metal, and nanoparticles of a third metal formed on a surface of the particulate substrate, a sintered body thereof, and a method for preparing the same.

Processes are provided for producing a titanium alloy material, such as Ti—Al alloys. In one embodiment, the process includes: heating an input mixture to a preheat temperature with the input mixture including aluminum, optionally, AlCl.sub.3, and, optionally ally, one or more alloying element halide; introducing TiCl.sub.4 to the input mixture at the first reaction temperature such that substantially all of the Ti.sup.4+ in the TiCl.sub.4 is reduced to Ti.sup.3+; thereafter, heating to a second reaction temperature such that substantially all of the Ti.sup.3+ is reduced to Ti.sup.2+ to form an intermediate mixture (e.g., a Ti.sup.2+ salt); and introducing the intermediate mixture into a reaction chamber at a disproportionation temperature reaction to form the titanium alloy material from the Ti.sup.2+ via a disproportionation reaction.

A method for densifying a material includes arranging the material in a cavity of a mold and applying pressure to the material in the mold. While applying pressure to the material in the mold, a magnetic field is applied to the material in the mold to cause the material to transform between a first allotrope phase and a second allotrope phase. Applying the magnetic field to the material includes magnetic cycling, which includes one or more iterations of adjusting the magnetic field to a first strength, and then adjusting the magnetic field to a second strength. The method includes determining a density of the material during the magnetic cycling and, responsive to determination that the determined density reaches a threshold density, stopping the magnetic cycling.

A method for manufacturing a porous metal body according to the present invention includes: a surface oxidizing step of heating a titanium-containing powder in an atmosphere containing oxygen at a temperature of 250° C. or more for 30 minutes or more to provide a surface-oxidized powder; and a sintering step of depositing the surface-oxidized powder in a dry process, and sintering the surface-oxidized powder by heating it in a reduced pressure atmosphere or an inert atmosphere at a temperature of 950° C. or more.

A spherical Ti-based powder and a manufacturing method therefor are provided. The spherical Ti-based powder has a 50% particle size (D50) of 1 to 250 μm in a cumulative particle size distribution based on volume, in which a total amount of oxygen and hydrogen is less than 3000 ppm by mass, an area defect rate in a cross-section of the spherical Ti-based powder is less than 0.100%, and an area circularity of the spherical Ti-based powder in a secondary projection image is 0.90 or more. The spherical Ti-based powder can be obtained by subjecting a pulverized Ti-based powder to a fusion and solidification treatment using a thermal plasma in which a flow rate of hydrogen gas as a working gas is adjusted to less than 0.3 l/min.