The method is: a preparation step in which a magnetic metal source, a nucleating agent, a complexing agent, a reducing agent, and a pH adjusting agent are prepared as starting materials; a crystallization step in which a reaction liquid that includes the starting materials and water is prepared, and a crystallized powder that includes the magnetic metals is made to crystallize in the reaction liquid by a reduction reaction; and a recovery step in which the crystallized powder is recovered from the reaction liquid. The magnetic metal source includes a water-soluble iron salt and a water-soluble nickel salt, the nucleating agent is a water-soluble salt of a metal that is more noble than nickel, and the complexing agent is at least one type of substance selected from the group consisting of a hydroxy carboxylic acid, a salt of a hydroxy carboxylic acid, and a derivative of a hydroxy carboxylic acid.

A method for producing a metal powder provided on the surface thereof with a glassy thin film, wherein a glassy substance is produced in the vicinity of the surface of the metal powder by spray pyrolysis from a solution that contains a thermally decomposable metal compound and a glass precursor that produces a glassy substance that does not form a solid solution with the metal produced from the metal compound by thermal decomposition, so as to form the metal powder provided on the surface thereof with the glassy thin film. The metal includes a base metal as a major component, and the solution contains 5 to 30 mass %, as the mass % with reference to the overall solution, of a reducing agent that is soluble in the solution and exhibits a reducing activity during the aforementioned step of heating.

A method of forming one of a plurality of encapsulated crystalline particles includes feeding a coaxial feed wire downwardly such that a first wire end of the coaxial feed wire is positioned at a heating source. The coaxial feed wire includes a crystalline wire core, and an amorphous shell surrounding the crystalline wire core. The first end of the coaxial feed wire is heated at the heating source, thereby forming a molten pendant drop at the first wire end. The plurality of encapsulated crystalline particles are emitted from the molten pendant drop onto a collector located below the molten pendant drop.

Silicon oxide-coated Fe-based soft magnetic powder having a high insulation capability can be obtained in such a manner that Fe-based soft magnetic powder is dispersed in a mixed solvent of water and an alcohol having a Hansen solubility parameter (SP value) of 11.3 or less, containing 5% by mass or more and 50% by mass or less of water, so as to provide a slurry. Then, a silicon alkoxide and a hydrolysis catalyst for the silicon alkoxide are added to the slurry to coat a silicon oxide thereon. The silicon oxide-coated Fe-based soft magnetic powder is capable of providing a powder compact having a high volume resistivity in molding into a powder compact. A method of producing the same is also disclosed.

The present invention relates to silicon coated metal microparticles in which at least a part of a surface of a metal microparticle composed of at least one of metal elements or metalloid elements is coated with silicon, wherein the silicon coated metal microparticles are a product obtained by a reduction treatment of silicon compound coated precursor microparticles in which at least a part of a surface of a precursor microparticle containing a precursor of the metal microparticles is coated with a silicon compound, or silicon doped precursor microparticles containing a precursor of the metal microparticles. Because it is possible particularly to strictly control a particle diameter of the silicon compound coated metal microparticle by controlling conditions of the reduction treatment, design of a more appropriate composition can become facilitated, compared with a conventional composition, in terms of diversified usages and desired properties of silicon compound coated metal microparticles.

The present invention relates to a method for producing a treated object, comprising the steps of: applying a layer of particles to a target area; applying a liquid binder to a selected portion of the layer in accordance with a cross-section of the object, so that the particles in the selected portion are bonded; repeating the steps of applying a layer of particles and applying a binder for a plurality of layers so that the bonded portions of the adjacent layers are bonded to form an object, wherein at least a part of the particles comprises a meltable polymer. A binder which cures by cross-linking is preferably selected as the binder. The obtained object is at least partially contacted with a liquid heated to ≥T or with a powder bed heated to ≥T in order to obtain the treated object. T represents a temperature of ≥25° C., the liquid does not represent a solvent or a reaction partner for the binder present in the object and the meltable polymer, and the powder bed is different from the particles of the meltable polymer. The invention also relates to a treated object that can be obtained by the method according to the invention.

The present application provides an iron-based amorphous alloy powder, a preparation method therefor and an application thereof. The iron-based amorphous alloy powder comprises a Cu element, and the particle shape of the iron-based amorphous alloy powder is spherical. The preparation method comprises the following steps: (1) smelting a master alloy to obtain iron-based amorphous alloy molten iron, the master alloy comprising a Cu element; and (2) treating the iron-based amorphous alloy molten iron obtained in step (1) by means of water-gas combined atomization to obtain the iron-based amorphous alloy powder.

A three-dimensional shaped article production method according to the invention is a method for producing a three-dimensional shaped article by stacking layers formed in a predetermined pattern, wherein a series of steps including a composition supply step of supplying a composition containing a plurality of particles to a predetermined part, and a bonding step of bonding the particles by irradiation with a laser light is performed repeatedly, and the composition supply step includes a step of forming a first region using a first composition containing first particles as the composition, and a step of forming a second region using a second composition containing second particles which are different from the first particles as the composition, and the bonding of the particles in the first region and the bonding of the particles in the second region are performed by irradiation with laser lights with a different spectrum.

This disclosure concerns building of three-dimensional objects in a fluidized bed of particles. The invention uses the fluidized bed as a medium for building three-dimensional objects by joining individual particles together in a planned pattern to fabricate a product. The fluid-like properties of the fluidized bed permit movement of computer-controlled, mechanically driven probes through the fluidized medium. The probes deliver adhesives or energy to specific points in the fluidized bed. The adhesives bind the particles together. Energy delivered by the probes causes fusion and welding or chemical bonding of the particles. The invention encompasses any shape, size, or composition of particles. Particles may be joined but not limited to adhesion, welding, and chemical bonding. Auxiliary features include use of stationary or mobile forms, changing the pattern of fluidization, use of multiple probes working simultaneously, and introduction of solid objects into the build, etc., to assist in forming the product.

A metal magnetic particle provided with an oxide layer on a surface of an alloy particle containing Fe and Si. The oxide layer has a first oxide layer, a second oxide layer, a third oxide layer, and a fourth oxide layer. Also, in line analysis of element content by using a scanning transmission electron microscope-energy dispersive X-ray spectroscopy, the first oxide layer is a layer where Fe content takes a local maximum value, the second oxide layer is a layer where Fe content takes a local maximum value, the third oxide layer is a layer where Si content takes a local maximum value, and the fourth oxide layer is a layer where Fe content takes a local maximum value.