A distillation and dehydration system is provided that produces an anhydrous organic solvent. The provided system includes vapor recompression (e.g., a mechanical or thermal vapor recompression unit) to recover heat from a rectification-distillation section (e.g., a rectifier/stripper column). The addition of vapor recompression enables further heat recovery within a stream by increasing the condensation temperature and pressure of that stream and later using its latent heat by condensing it.

The duty of internal heat exchange can be flexibly adjusted without impairing energy saving performance of a HIDiC. A method of adjusting the duty of heat exchange in a heat exchange structure of a HIDiC includes totally condensing a portion of the vapor fed to a heat exchange structure in a heat exchange structure; and providing a liquid control valve downstream of the heat exchange structure on the first line, without providing a control valve on a vapor-flowing part of first and second lines of the HIDiC, and adjusting a flow rate of a portion of the compressor outlet vapor flowing into the heat exchange structure by using the control valve, while compensating for a pressure loss needed for the control valve by using a liquid head of a condensate, and/or by using pressurization by a pump.

The present invention relates to a facility for purifying recovered NMP from lithium-ion battery production, comprising a first column for separating low-boiling impurities, comprising a supply, in its central part, for the recovered NMP, and which can be heated by means of a first evaporator for supplying thermal energy; and a second column for separating high-boiling impurities, a connection line from a lower part of the first column to a lower part of the second column being provided. In this case, according to the invention, the second column can be heated by means of a second evaporator comprising an inlet and an outlet for purified NMP, and the second column is assigned a compressor portion which extends from a head of the second column to the inlet of the second evaporator and comprises a mechanical vapor compressor for inputting energy to the vapor of the second column. The present invention furthermore relates to a method for operating a facility of this kind.

A process for recovering heat from the separation of hydrocarbons. The overhead vapor stream from a fractionation column is passed to a two stage heat pump compressor. The first stage of compression is used to reboil the fractionation column. The second stage is compressed and cooled passed to a separation zone. The liquid in the separation zone may be passed back to the fractionation column as secondary reflux, and/or recovered as liquid product. Heat may also be removed from the second stage. A suction drum on the first stage may be used to protect the heat pump compressor from any droplets in the overhead stream.

A unique adaptive method of Mechanical Vapor Re-compression (MVR) to dehydrate abrasive sludge to a dry, sterile state that is nearly moisture free while maintaining extremely high process efficiencies by adaptively tuning the system parameters related to the varying specific plus latent heats of the input feedstream. This Adaptive MVR (AMVR) process is supported by the effective use of a unique method and apparatus for the optimization of the conductive heating process as applied to a range of sludge consistencies.

A system for purifying incoming fluid is modular and includes a heat exchanger module, an evaporator-condenser module and a compressor. The system components are arranged in a stacked configuration to facilitate gravitational flow of the purified fluid such that the purified fluid drains passively for collection. A system for preparation of ready-to-use treatment fluid includes the modular fluid purification system, a preparation station and a coupling device. The components are configured to be retained in a portable carrier that is manually operable for improved access to and mobility of the components. A coupling device can connect the flow channels of several components and can be used in preparing ready-to-use dialysate. A system prepares a receptacle and a ready-to-use treatment fluid in the receptacle.

A process for purifying a crude composition comprising rectifying the crude composition in a rectification plant. The rectification plant comprises a rectification column including: a first overhead condenser for condensing a head fraction, and a reboiler for evaporating a bottom fraction. A difference between a temperature of the head fraction and a temperature of the bottom fraction is less than or equal to 20? C. A heat pump is provided between the first overhead condenser and the reboiler. The heat pump is an indirect heat pump that is operated with water or methanol as a refrigerant, and the indirect heat pump includes an expansion valve and a compressor. The heat pump comprises a second condenser located upstream of the compressor.

The device is designed for production of light, highly pure water with a high content of light molecules .sup.1H.sub.2 .sup.16O.

The technical results are productivity increasIIITII of the device and a reduction in energy costs per unit of the finished product.

The device is equipped with a heat pump, the distillation column consists of two coaxial tubes of diameter D1 and D2 with a layer of random packing located in the gap between them, where (D1D2)/2<300 mm, and the liquid distributor at the top of the column has at least 800 irrigation points per square meter of the cross-sectional area of the packing part of the column.

A system and method for producing substantially anhydrous ethanol, methanol or other volatile chemicals includes: (a) a first distillation stripping column or column set with overhead vapors compressed using mechanical vapor recompression to strip off a weak ethanol overheads; (b) a second distillation rectifying column having a higher operating temperature than the stripping column; (c) a dehydration means in fluid communication with the rectifying column; (d) reboiler for the stripping column which partially condenses the vapor from the mechanical vapor recompression, (e) a trim condenser which completes the condensing of the vapor/liquid mix of the reboiler, (f) a heat recovery circuit which condenses the rectifying column overheads and molecular sieve dry ethanol condenser and (g) a heat exchange to transfer the recovered heat of (f) to the first distillation stripping column reboiler feed.

A distillation and dehydration system is provided that produces an anhydrous organic solvent. The provided system includes vapor recompression (e.g., a mechanical or thermal vapor recompression unit) to recover heat from a rectification-distillation section (e.g., a rectifier/stripper column). The addition of vapor recompression enables further heat recovery within a stream by increasing the condensation temperature and pressure of that stream and later using its latent heat by condensing it.