A contact tray for use in a mass transfer column and having a tray deck for receiving a liquid stream and a plurality of valves distributed across the tray deck through which vapor ascends for interacting with the liquid stream. Each valve has an opening in the tray deck in the form of a central segment and extensions that extend outwardly from opposite ends of the central segment. The valves each include a valve body with a valve cover positioned in covering relationship above and extending outwardly beyond the opening and legs that are attached to the valve cover at recesses located at opposite ends of the valve cover. The legs extend downwardly through the extensions in the opening and include stops in portions of the legs positioned below the tray deck to permit limited vertical movement of the legs to allow the valve body to move between open and closed positions in response to ascending vapor pressure against an undersurface of the valve cover. Deflectors are positioned at opposite sides of the legs to restrict vapor passage around the legs.

A mass transfer assembly has at least one dividing wall, zones of mass transfer structures on opposite sides of the dividing wall, and a vapor flow restrictor that is operable to vary the split of vapor ascending through the zones of mass transfer structures on the opposite sides of the dividing wall.

Distillation trays having improved efficiency and capacity are described. The improvement is accomplished with unique downcomer spout arrangements and bubble promoters which provide equal liquid distribution to all areas of the tray. The ratio of the open area of a contacting zone including part of a bubble promoter and associated deck zone over the open area of the downcomer spout zone on the adjacent tray for distributing liquid to the zone is essentially the same across the tray.

A contact tray has a tray deck for receiving a liquid stream and a plurality of valves distributed across the tray deck through which vapor ascends for interacting with the liquid stream. Each valve includes an opening in the tray deck, wall segments that extend upwardly along opposite sides of the opening, and a valve body. The valve body has a trapezoidal valve cover positioned in covering relationship above and extending outwardly beyond the opening and legs that are attached to the valve cover at recesses located at opposite ends of the valve cover. A vent is positioned in one of the legs.

A tray for a mass-transfer column may allow contact between liquid and gas phases. The tray may include a tray inlet via which the tray is supplied with a liquid phase, a tray outlet via which the liquid phase flows out from the tray, first guide mechanism for guiding the liquid phase where the first guide mechanism forms a first flow path along which the liquid phase flows from the tray inlet to the tray outlet, an inlet for a temperature-control fluid, an outlet for the temperature-control fluid, and second guide mechanism for guiding the temperature-control fluid for heat exchange with the liquid phase. The second guide mechanism forms a second flow path that overlaps with the first flow path and leads from the inlet to the outlet. The temperature-control fluid flows along the second flow path in a direction opposite the flow direction of the liquid phase.

A process for the preparation of an alkylene glycol from an alkene comprising steps of: a) supplying a gas composition to an alkylene oxide absorber through a gas inlet, the absorber comprising an absorption section and a sump, and allowing the gas composition to pass upwards; b) supplying a lean absorbent to the top of the absorption section and allowing the lean absorbent to pass downwards; c) intimately contacting the gas composition with lean absorbent in the absorption section in the presence of one or more catalysts that promote carboxylation and hydrolysis; and d) withdrawing fat absorbent from the absorption section and passing the fat absorbent and any liquid condensate through the sump, wherein the sump comprises one or more baffles that define a flow pathway from a sump inlet to a sump outlet between the one or more baffles.

A fractionation column can be used to separate a liquid containing multiple components into its constituent components based on vapor pressure. While the fractionation column may be designed for certain operational performance, the operational characteristics may change, for example, due to changed flow rates through the column and/or fouling in the column. In some examples, a fractionation column is described that includes a fractionation tray formed of multiple tray decks that move relative to each other. The tray decks can have apertures that move relative to each other between a position in which there is a comparatively large amount of open area through the fractionation tray to a position in which there is a comparatively small amount of open area through the fractionation tray. Movement of the trays can control turndown and/or clear fouling buildup on the tray surface.

A double liquid distribution device (1) suitable for use in in a fractionating or wash column (10) including a high collector tray (2) connected to a manifold support (7) via at least two longitudinal liquid downflow ducts (5, 6), the manifold support (7) supporting at least two series of transverse tubular manifolds (8, 8a 8b) and serving to feed liquid respectively to the first series of manifolds (8a) via a first longitudinal duct (5) and to the second series of manifolds (8b) via a second longitudinal duct (6), each manifold (8, 8a 8b) including distribution orifices (8c) in its under face that are suitable for distributing the liquid onto the top face of the packing bed (9). The two longitudinal liquid downflow ducts (5, 6) are connected together in a low portion (5b, 6b) by a communication device (11) fitted with a valve (12) having controlled opening that is suitable for allowing the liquid to be transferred between the two longitudinal ducts in a controlled manner.

A method for producing an epoxyalkane includes the step of separating a stream containing an epoxyalkane and an extracting agent in a separation column having a column kettle reboiler. A part of a stream in the column kettle of the separation column enters an extracting agent purifier and is treated to obtain a gas phase light fraction that returns to the separation column and a liquid phase heavy fraction that is subjected to a post-treatment. The method can be used in the industrial production of an epoxyalkane.

The present disclosure relates to an apparatus for removing residual monomers and, more specifically, to an apparatus for removing residual monomers, the apparatus being capable of preventing, during the removal of volatile materials by supplying a gas to a flowing distillation material, the formation of dead zones in which the distillation material does not flow or the flow rate thereof decreases. The apparatus for removing residual monomers, of the present disclosure, comprises: a main body capable of supplying a gas to a distillation material accommodated therein; distillation material supply part which is provided at the upper part of the main body and through which the distillation material is injected; a gas inflow part which is provided at the lower part of the main body and through which the gas is injected; a discharge part which is provided at the upper part of the main body, and which discharges volatile materials separated, by means of the gas, from the distillation material; a recovery part, which is provided at the lower part of the main body and recovers the distillation material from which the volatile materials have been removed; a plurality of trays which are provided inside the main body, and each of which has through-holes and a spiral channel; and a downcomer which is provided between the trays, and which is a moving passage through which the distillation material moves downward from the upper part of the main body.