A method including: (a) contacting lime with an extract including a S1 solvent carrying a contaminant load to form a lime treated extract; and (b) reducing the contaminant load by removing solids. Optionally, the method includes washing the lime treated extract with water. Optionally, a pH of the lime treated extract is at least 6.5.

Sample purification systems include a particle extraction assembly having a mixing compartment and a settling compartment. A biological sample is mixed with two liquid phases formulated to effectuate transfer of a biological molecule into a first phase and particulate contaminants into a second phase. The first phase includes a solubilizing salt, the second phase includes an organic molecule, and the mixture can have little or no monoatomic salt or dextran. The molecule-containing first phase can be optionally concentrated without also concentrating the particulate contaminants and introduced into a multi-stage liquid-liquid extractor, by which the biological molecule or molecular contaminants are extracted from the first phase into a third phase, thereby purifying the molecule away from contaminants. The extracted sample can be further purified through a series of processing steps. The system can be run in continuously mode to maintain sterility of the sample.

A process for a reactive separation of organic molecules from biomass includes a reaction step for the biomass, a simultaneous extraction step using a solvent, and a filtration step to recover products, wherein the products comprise ferulic acid and/or coumaric acid. The products are extracted from the biomass in a pressurized stirred batch reactor using a liquid extraction solvent and a base in which the ferulate and the coumarate remain.

In an autoclave apparatus for a high-pressure acid leaching process which advances leaching by stirring heated and pressurized material slurry and sulfuric acid by stirrers in compartments in an autoclave main body of a plurality of compartments, transfers slurry from an upstream side compartment to a downstream one to advance leaching, liquid flow ports for slurry transfer that open and close by doors are provided on the partition walls, the liquid flow ports for slurry transfer are installed at positions where the heights from the lowermost portion the autoclave to the center of gravity are 0.1 to 0.3 times an autoclave diameter and distances from the center lines of the partition walls to the center of gravity are 0.05 to 0.25 times the autoclave diameter, and the liquid flow ports for slurry transfer have shapes which do not reach end portions of the partition walls.

This invention relates to the extraction of psychoactive compounds from fungus for use in medicine. Raw fungus is dried and ground. The solvent used for extraction is methanol or a hydro-methanol mixture, an acidic hydro-methanol mixture, or an alkaline hydro-methanol mixture. The extraction slurry is filtered and pH-adjusted if necessary. The methanol in the solvent is then completely evaporated and water added back, where necessary, to form a concentrated slurry. The concentrated slurry is then standardized to provide a known concentration of the psychoactive alkaloids that have been extracted. The standardized slurry may then be dried to result in a powdered extract with a precisely defined purity of psychoactive compounds.

A process of extraction, quantification and recovery of additives in polypropylene with the stages of washing the plastic material (A), grinding the material (A) to a particle size from 10 to 500 microns, extraction where the material (A) is transferred to a column (1) and then such material successively passes through column (2), column (3) and column (4), respectively, for successive extractions with solvents (I), (II), (III) and (IV), packed column extraction, where the solvent with the additives obtained from each extraction in columns (1), (2), (3) and (4) passes through packed columns (1′), (2′), (3′) and (4′), respectively, crystallization of the additives obtained after each extraction stage in packed columns (1′), (2′), (3′) and (4′) respectively; and quantification of the additives obtained and where the residual material without additives is subjected to pyrolysis.

An object to be decontaminated contaminated with radioactive material is introduced into an acid eluting solvent to dissolve the radioactive material. The radioactive material dissolved is concentrated and separated from the eluting solvent in the present method. The object to be decontaminated comprises contaminated soil and contaminated liquid. One or both of the contaminated soil and the contaminated liquid are collected and introduced into the eluting solvent. The radioactive materials and the object to be decontaminated dissolved in the eluting solvent are separated into solid and liquid. The decontaminated soil separated from the eluting solvent is collected. The eluting solvent used for separating the radioactive material and in which radioactive material is dissolved is concentrated.

A supercritical fluid extraction (SFE) apparatus is provided that is capable of being operated in a continuous and/or steady-state fashion. The SFE apparatus may include an extraction assembly. The extraction assembly may include a first extraction chamber (FEC) to contain a first amount of source material from which a compound is to be extracted, and a second extraction chamber (SEC) to contain a second amount of the source material. The extraction assembly may include a valve to control a flow of a solvent into the FEC or the SEC. The SFE apparatus may include a collection chamber that is mounted substantially perpendicular to the extraction assembly. Other embodiments are described.

An extractor suitable for using a solvent to separate a compound from a solid or semisolid substance containing the compound. The extractor includes a conveying assembly having an inclined conveyor for receiving the substance from a substance inlet and moving the substance through the solvent, an inclined upper surface associated with the first conveyor and an inclined lower surface associated with the first conveyor. The conveyor is configured to move the substance downward through the solvent along the upper surface toward a lower end of the conveyor and upward through the solvent along the lower surface toward an upper end of the conveyor.

A closed rotatable extraction system includes at least two tubes where one tube accepts an extractable material, and the system can be evacuated through a valve in the system. At least one conduit comprises at least one flexible hose, bent ridged pipe, t-pipe, curved pipe, or any combination thereof. At least one valve that when open allows evacuation of the system, and optionally for introduction of a solvent for extraction. When the at least one valve is closed a solvent vapor atmosphere is defined as almost exclusively or exclusively the solvent vapor and has a gas pressure that is about the solvents vapor pressure or less in the closed rotatable extraction system. The closed rotatable extraction system or a portion thereof can involve a first rotation orientation for liquid transfer and a second orientation for a vapor transfer.