B01D11/0434

Rubber and By-Product Extraction Systems and Methods
20200172637 · 2020-06-04 ·

Systems and methods for extracting useful by-products and natural rubber from non-Hevea rubber bearing plants are disclosed.

Rubber and by-product extraction systems and methods
10584185 · 2020-03-10 · ·

Systems and methods for extracting useful by-products and natural rubber from non-Hevea rubber bearing plants are disclosed.

METHOD FOR RECOVERING LITHIUM BIS(FLUOROSULFONYL)IMIDE

A method for recovering lithium bis(fluorosulfonyl)imide is provided in the present application. The method of the present application may comprise: mixing a slag from lithium bis(fluorosulfonyl)imide production process with a solvent of carbonate ester, to obtain a mixed material; subjecting the mixed material to solid-liquid separation, to obtain a discharged liquid and a solid slag; monitoring the chromaticity of the discharged liquid and comparing the chromaticity of the discharged liquid with a chromaticity reference; recycling the discharged liquid to the mixed material, if the chromaticity of the discharged liquid is higher than the chromaticity reference; and recycling the discharged liquid to lithium bis(fluorosulfonyl)imide production process, if the chromaticity of the discharged liquid is lower than or equal to the chromaticity reference.

LIQUID-LIQUID EXTRACTION OF DMF

The present invention relates to a method for the chlorination of a sucrose-6-acylate to produce a 4,1,6-trichloro-4,1,6-trideoxy-galactosucrose-6-acylate wherein said method includes steps of: (i) combining the sucrose-6-acylate with a chlorinating agent in a reaction vehicle comprising a tertiary amide to afford a mixture; (ii) heating said mixture for a heating period in order to provide chlorination of sucrose-6-acylate at the 4, 1 and 6 positions thereof; and (iii) quenching the product stream of (ii) to produce a 4,1,6-trichloro-4,1,6-trideoxy-galactosucrose-6-acylate;
wherein before said quenching, a portion of said tertiary amide is removed by extraction into a solvent in which said tertiary amide is at least partially soluble.

Liquid-liquid extraction of DMF

The present invention relates to a method for the chlorination of a sucrose-6-acylate to produce a 4,1,6-trichloro-4,1,6-trideoxy-galactosucrose-6-acylate wherein said method includes steps of: (i) combining the sucrose-6-acylate with a chlorinating agent in a reaction vehicle comprising a tertiary amide to afford a mixture; (ii) heating said mixture for a heating period in order to provide chlorination of sucrose-6-acylate at the 4, 1 and 6 positions thereof; and (iii) quenching the product stream of (ii) to produce a 4,1,6-trichloro-4,1,6-trideoxy-galactosucrose-6-acylate;
wherein before said quenching, a portion of said tertiary amide is removed by extraction into a solvent in which said tertiary amide is at least partially soluble.

Static Internal, Use of One or More Static Internal, Agitated Liquid-Liquid Contactor and use of an Agitated Liquid-Liquid Contactor
20190232192 · 2019-08-01 · ·

A static internal (1) embodied so as to be suitable for improving a contact, heat transfer or mass transfer between the liquids in an agitated liquid-liquid contactor (3) lacking calming sections and having an metallic agitated internal (2). The surface energy of the static internal (1) is <40, preferably <30, more preferably <25, most preferably <20 mN/m.

Method of recovering (meth)acrylic acid

The present invention relates to a method of recovering (meth)acrylic acid and an apparatus used for the recovery method. The recovery method according to the present invention discharges each (meth)acrylic acid aqueous solution of different concentrations at a (meth)acrylic acid absorption tower, and uses an extraction solvent of a specific ratio in the step of extracting (meth)acrylic acid, thus enabling the operation of a continuous process of recovering (meth)acrylic acid that can secure a high (meth)acrylic acid recovery rate, and can simultaneously significantly reduce purification energy cost.

METHODS AND SYSTEMS FOR THE MANUFACTURE OF AN AROMATIC PHTHALIC BISIMIDE AND A POLYETHERIMIDE

A method for producing an aromatic bisimide includes reacting a dialkali metal salt of a dihydroxy aromatic compound with a reactive substituted phthalimide under conditions effective to form a product mixture, introducing the product mixture to a liquid-liquid extraction column including an aqueous alkali metal hydroxide solution, and recovering from the liquid-liquid extraction column a purified aromatic bisimide having less than 500 ppm of residual dialkali metal salt of the dihydroxy aromatic compound, the corresponding dihydroxy aromatic compound, the corresponding mono-substituted salt of the dihydroxy aromatic compound, or a combination including at least one of the foregoing. A method for the manufacture of a polyetherimide from an aromatic bisimide prepared by the above method is also disclosed. A polyetherimide having less than 100 ppb of residual bisphenol A and an article made therefrom are also described.

Combined Solids-Producing Direct-Contact Exchange and Separations
20190099693 · 2019-04-04 ·

A method for separating a dissolved product from a liquid is disclosed. A carrier liquid is cooled in a direct-contact exchanger, the direct-contact exchanger using a liquid coolant to cool the carrier liquid. The carrier liquid comprises a dissolved product. The carrier liquid and the liquid coolant are substantially immiscible. A portion of the dissolved product is condensed, frozen, deposited, desublimated, or a combination thereof out of the carrier liquid as a solid product at a liquid-liquid interface between the liquid coolant and the carrier liquid. The solid product is entrained in the carrier liquid, the liquid coolant, or a combination thereof. The solid product is separated from the carrier liquid, the liquid coolant, or a combination thereof.

A METHOD OF RECOVERING (METH)ACRYLIC ACID
20190083923 · 2019-03-21 · ·

The present invention relates to a method of recovering (meth)acrylic acid and an apparatus used for the recovery method. The recovery method according to the present invention discharges each (meth)acrylic acid aqueous solution of different concentrations at a (meth)acrylic acid absorption tower, and uses an extraction solvent of a specific ratio in the step of extracting (meth)acrylic acid, thus enabling the operation of a continuous process of recovering (meth)acrylic acid that can secure a high (meth)acrylic acid recovery rate, and can simultaneously significantly reduce purification energy cost.