B01D17/047

Treatment of contaminated oil produced by oil and gas wells

A method of treating a contaminated oil comprising preparing a brine solution, adding ozone to the brine solution to produce ozonated brine solution, adding a volume of ozonated brine solution to a volume of the contaminated oil, mixing the volumes of contaminated oil and ozonated brine solution with coagulant and surfactant at a shear rate sufficiently high so as to cause formation of an emulsion of the contaminated oil and the brine solution, stopping the mixing, thereby causing the emulsion to separate into an aqueous brine liquid phase and an oil liquid phase, separating the brine liquid phase from the oil liquid phase, and separating at least one contaminant from the oil liquid phase to produce a volume of purified oil.

IONIC LIQUIDS FORMULATION AS AN ENVIRONMENTALLY FRIENDLY OIL DISPERSANT

Disclosed herein is an oil dispersant composition that contains an acyl amino acid ionic liquid, a dicationic ionic liquid, a fruit acid ionic liquid, a polyacid ionic liquid, and an ethoxylate oleyl ether ionic liquid. The composition may also be diluted with water. The composition is useful for dispersing an oil spill in a body of water, while being less toxic to the aquatic environment and also acting to stimulate bacterial growth in said aquatic environment.

Separation of components from whole stillage
09730463 · 2017-08-15 ·

A multi stage process for separating oil, protein, fiber and clean water from a stream containing whole stillage byproduct from ethanol production is disclosed. In a first step, fibers are separated in a two-step process that includes a plate separator and a press. In a subsequent step, the liquid stream separated from the fibers and contains oil, protein and water is treated with a composition that causes the protein to gel. The liquid stream is then processed in a phase separator that drains the oil by gravity, removes the water by an impeller under pressure and removes the solidified protein using a scroll.

Copper mesh coated with manganese molybdate and application thereof in the separation of oil-water emulsion and degradation of organic pollutants in water
11452991 · 2022-09-27 · ·

The invention aims to provide a copper mesh coated with manganese molybdate and application thereof in the separation of oil-water emulsion and degradation of organic pollutants in water. A large amount of nano-scale manganese molybdates are grown on the surface of a copper mesh through a two-step hydrothermal method. Thereby, a multifunctional composite material is prepared, which can effectively separate oil-water emulsion and degrade organic pollutants in water. The copper mesh has good recyclability. Most of all, the product is suitable for industrial production to achieve the purpose of treating water pollution.

Polysaccharide microgels for cleaning water of petroleum and petroleum products and method for using same (variants)

The group of inventions relates to the field of organic chemistry and can be used for cleaning water, industrial and domestic waste water or waste water sediment, and for the containment and recovery of petroleum and petroleum product spills in large bodies of water, rivers, lakes and seas. In the claimed group of inventions, aqueous solutions of polysaccharide microgels, having a molecular mass of 20000-200000 daltons and a particle size of 50-600 nm, are used as a substance for cleaning water of petroleum and petroleum products. Moreover, low concentrations of polysaccharide microgels in water, ranging from 0.1 to 20 g/l, are used. Said solutions are used as a surface modifier for a filter used in separating water-oil emulsions, as a sorbent for the containment and recovery of oil spills in an aqueous medium, and also as a coagulant for the cleaning of water polluted by petroleum and petroleum products. The technical result is in making it possible to recover a commercial product, recovered during the process of cleaning water of petroleum or petroleum products, and to recover the starting substance for the reuse thereof, while simultaneously simplifying the slurry utilization process.

Demulsifying additive for separation of oil and water

A demulsifying additive comprising a branched aliphatic compound may be introduced to a stream containing mixtures of or emulsions of oil and water in an effective amount to separate water from the oil in the stream, such as separating oil from emulsified oil-in-water and/or separating water from emulsified water-in-oil in a production fluid. The branched aliphatic compound may be grafted with a polyether via a crosslinking reaction. Alternatively, branched aliphatic compounds may be crosslinked together.

Oil extraction method and composition for use in the method
09816050 · 2017-11-14 ·

A demulsifying composition is disclosed for aiding extraction of an emulsified oil from an oil and water emulsion. The composition includes one or more non-ionic surfactants having a HLB value of 6 or greater, wherein the non-ionic surfactant is selected from the group consisting of alkoxylated plant oils, alkoxylated plant fats, alkoxylated animal oils, alkoxylated animal fats, alkyl polyglucosides, alkoxylated glycerols, and mixtures thereof. The composition may include silicon containing particles. A method for recovering oil from a corn to ethanol process is also disclosed. The method includes the steps of adding the composition to a process stream of the corn to ethanol process, and extracting oil from the process stream.

Purification of oil
11247147 · 2022-02-15 · ·

A system (1; 101) and a method for purification of oil, said system comprising:—at least one feed tank (3) comprising oil to be purified;—a separation aid dosing device(13);—at least one basic sedimentation tank (21a, 21b) comprising at least one inlet (23a, 23b) connected to the feed tank (3) and to the separation aid dosing device (13) for receiving oil to be purified and separation aid, said at least one basic sedimentation tank (21a, 21b) further comprising at least one sludge phase outlet (41a, 41b) provided in a bottom part (37a, 37b) of the basic sedimentation tank and at least one oil phase outlet (39a, 39b);—at least one advanced sedimentation tank (121) comprising at least one sludge phase inlet (122) connected to the at least one sludge phase outlet (41a, 41b) of the at least one basic sedimentation tank (21a, 21b), said advanced sedimentation tank (121) further comprising at least one sludge phase outlet (141; 141a, 141b) connected to a sludge tank (143) and at least one oil phase outlet (139a, 139b; 39), wherein said advanced sedimentation tank (121) further comprises at least one sensor (55; 55a, 55b, 55c) for detecting the presence of an oil phase or a sludge phase.

METHOD AND DEVICES FOR DE-EMULSIFYING AND COMPLEXING ORGANIC COMPOUNDS IN EMULSIONS
20170260072 · 2017-09-14 · ·

The invention relates to a method for aggregating and separating an organic material mixture which is provided in a dissolved form in an aqueous emulsion. The method is characterized by the following steps: a) providing an aqueous emulsion with organic compounds which are provided in the emulsion in a dissolved form, said organic compounds being carboxylic acids, phospholipids, glycolipids, glyceroglycolipids, phenols, sterols, chlorophyll, and/or sinapines, b) mixing the emulsion from step a) with an aqueous solution containing copper(II) ions and/or calcium ions until an aggregate formation is achieved, and c) separating the aggregates from step b) by means of a sedimentation, filtration, or centrifugation process after achieving an aggregated phase of the organic compounds from step b).

N-vinylpyrrolidone-based cationic copolymer for separating an oil-in-water emulsion

Embodiments of the present disclosure include a method of separating an oil-in-water emulsion formed during crude oil production into a water phase and an oil phase that includes adding 1 part-per-million (ppm) to 10000 ppm of an N-vinylpyrrolidone based cationic copolymer to the oil-in-water emulsion, based on the total volume of the oil-in-water emulsion, to form a water phase and an oil phase, and separating the water phase from the oil phase.