A high-flux silicon carbide ceramic filter membrane and a preparation method thereof are provided. In the preparation method, a separation layer is directly coated at a time on the basis of a support, that is, after the support is sintered, the separation layer is directly coated and then sintered for carbon removal. In the present disclosure, a sintering process and a coating formula are optimized to prevent fine silicon carbide particles from entering micropores of a support due to capillary filtration and film formation during coating, such that a separation layer with an average pore size of 0.2 m or less can be directly coated on a silicon carbide support with an average pore size of 10 m or more, and fine silicon carbide particles can be effectively prevented from entering micropores of the support during the coating.

A process for making an iron oxide impregnated carbon nanotube membrane. In this template-free and binder-free process, iron oxide nanoparticles are homogeneously dispersed onto the surface of carbon nanotubes by wet impregnation. The amount of iron oxide nanoparticles loaded on the carbon nanotubes range from 0.25-80% by weight per total weight of the doped carbon nanotubes. The iron oxide doped carbon nanotubes are then pressed to form a carbon nanotube disc which is then sintered at high temperatures to form a mixed matrix membrane of iron oxide nanoparticles homogeneously dispersed across a carbon nanotube matrix. Methods of characterizing porosity, hydrophilicity and fouling potential of the carbon nanotube membrane are also described.

A method for fabrication of an hydrogen-permeable membrane, comprising forming an alloy of a target composition and structure from powders by mechanically alloying; and forming a membrane from the alloy of the target composition and structure.

A ceramic membrane including a feed flow inlet, a retentate flow outlet, a permeate flow outlet, a membrane interface portion. The membrane interface portion include a feed flow channel fluidly coupled to the feed flow inlet and to the retentate flow outlet and permeate flow channel fluidly coupled to the retentate flow outlet, wherein the membrane interface portion is operable to allow for fluid communication between the feed flow channels and the permeate flow channels through a membrane portion, and wherein the ceramic membrane has an open porosity of at least 10%. Also provided is a process for preparing the ceramic membrane by additive manufacture.

The invention provides a porous hybrid matrix membrane support having at least one porous mesh layer of mesh densified to form a membrane mesh support and at least one porous filament layer of filaments that are generally non-woven, densified to form a membrane filament support. The filament layer is densified to provide a sufficiently small crevice depth in the membrane filament support that can help protect a membrane layer on the membrane filament support from rupturing. The membrane mesh support and the membrane filament support with micro-smooth surfaces can be integrally joined by diffusion bonding to resist separation across the adjoining surfaces. The combined, diffusion bonded support of both types of layers provide structural support sufficient for high pressures and provide substantial uniform permeability across the face of the structural support.

A metal organic framework glass membrane and a preparation method thereof are provided. The preparation method includes a step of heating a crystalline metal organic framework material to the melting temperature at a rate of 1-15 C./min and then naturally cooling the crystalline metal organic framework material. The crystalline metal organic framework material contains a metal node and a ligand A. The metal node is a zinc ion and/or a cobalt ion and the ligand A is imidazole or phosphoric acid. The metal organic framework glass membrane has a wide range of membrane-forming conditions, and the material thereof can be melted without being decomposed within a control range to form a continuous glass layer with good repeatability.

Provided is a method for manufacturing a micropore filter usable as SCE. Stainless steel particles having particle diameters of 3 to 60 m are subjected to milling in a bead mill using zirconia beads to prepare powder having a flakiness of 0.03 to 0.4. The zirconia adhered to the surface of the powder is removed by pickling. A load of 10 to 15 kN is applied to 0.5 to 1.0 g of the pickled powder, thereby compacting the powder into a columnar compact body. The compact body is kept and fired in a vacuum atmosphere of 10.sup.5 to 10.sup.3 Pa at a temperature of 1000 to 1300 C. for 1 to 3 hours to form a sintered body. The sintered body is pressed into a pipe having an inner diameter of 0.90 to 0.99 times of the outer diameter of the sintered body, and extruded to obtain a micropore filter.

The present invention relates to design and manufacture of multilayer sintered membranes made from metals and inorganic compounds (ceramics, silicate, clay, zeolites, phosphates, etc.). The membranes are designated for separation of water. They comprise at least one layer having nanopores commensurable with the size of water molecules. The membranes comprise: (a) supporting metallic layer having pore size 1-500 microns, (b) metallic interlayer having pore size <2 micron, (c) sublayer with local regular protrusions of the interlayer into the supporting layer to increase service life of the membrane, and (d) one nanoporous ceramic or metallic top layer having pore size in the range of 1-15 angstroms. The invented design and method allow the manufacture of cost-effective multilayer membranes containing nanoporous layer with controlled pore sizes in each layer and optimal morphology of pores that provides selective transport of molecules during filtration and separation of liquids.

There is provided an inorganic hierarchical porous membrane comprising at least two layers, wherein each layer of the at least two layers comprises a different average pore size as compared to another layer of the at least two layers, and wherein the membrane comprises a patterned surface. There is also provided a method of forming the membrane.

A composite nanoporous metal membrane, a method of making same, and a method of using same to filter supercritical CO.sub.2 are provided. The method of making generally includes a) providing a sintered coarse porous layer; b) applying to an outer face of the coarse porous layer second metal particles; c) sintering to form a structure comprising coarse and intermediate layers; d) applying a suspension of third metal particles; e) drying the suspension of third particles; f) pressing the dried layer of third particles; and g) sintering to form a composite nanoporous metal membrane. The composite nanoporous metal membrane generally includes: a) a sintered coarse layer; b) an intermediate layer comprising first metal particles and second metal particles joined in a sintered structure which is sintered to the coarse layer; and c) a fine layer comprising third metal particles joined in a sintered structure which is sintered to the intermediate layer.