B01J13/12

Method for Generating Solid Capsules
20240050914 · 2024-02-15 ·

A method for generating capsules includes: a. providing in a first chamber a dispersed phase, the dispersed phase including a solution including a first solvent and a matrix-forming agent, the matrix-forming agent is a solid in its pure state and the first solvent and the matrix-forming agent are configured such that the matrix-forming agent is soluble in the first solvent; and b. providing in a second chamber a continuous phase, the continuous phase including a second solvent. The first and second chambers are fluidic connected by channel(s). The method further includes: c. guiding the dispersed phase from the first chamber through the channel(s) into the second chamber to form an emulsion or a dispersion including a plurality of droplets of the dispersed phase, in the continuous phase; and d. removing the first solvent from the droplets of the dispersed phase and solidifying the matrix-forming agent to form a capsule.

Solvent removing apparatus and method of manufacturing microsphere using the same
11944949 · 2024-04-02 · ·

A solvent removing apparatus includes a container containing an emulsion comprising a first raw material of a continuous phase and a second raw material of a dispersed phase, an impeller rotating in the container to stir the emulsion, and a foam breaker spaced apart from the impeller on an upper portion of the impeller, positioned below a surface of the emulsion to be submerged in the emulsion when the emulsion is calm, and rotating to reduce foam generated during stirring of the emulsion.

Solvent removing apparatus and method of manufacturing microsphere using the same
11944949 · 2024-04-02 · ·

A solvent removing apparatus includes a container containing an emulsion comprising a first raw material of a continuous phase and a second raw material of a dispersed phase, an impeller rotating in the container to stir the emulsion, and a foam breaker spaced apart from the impeller on an upper portion of the impeller, positioned below a surface of the emulsion to be submerged in the emulsion when the emulsion is calm, and rotating to reduce foam generated during stirring of the emulsion.

POROUS MICROSPHERE AND METHOD FOR PREPARING THE SAME

A porous microsphere and a method for preparing the same includes the following steps. A copolymer having a vinylbenzyl chloride unit and a vinylbenzyl alcohol unit is dissolved in an organic solvent, and inorganic particles are dispersed in the organic solvent to form a mixed suspension. An aqueous solution containing a surfactant is provided. The mixed suspension is emulsified in the aqueous solution to form an emulsion. The emulsion is heated to evaporate the organic solvent to obtain inorganic-composite porous microspheres suspended in water. The copolymer in the formed porous microspheres can be further carbonized or removed to produce inorganic-based porous microspheres containing carbon or not containing carbon.

Method for preparing high sensitivity temperature sensitive reversible color-changing microcapsule

The disclosure belongs to the technical field of material science, and particularly relates to a method for preparing a high sensitivity temperature sensitive reversible color-changing microcapsule. According to the method, a series of novel fluorane dyes are designed and synthesized, the color-changing performance can be achieved without a color developing agent, the fluorane dyes are compounded with a phase change material according to a certain proportion, a series of two-component reversible temperature sensitive color-changing dyes are prepared, and then a two-component reversible thermochromic microcapsule with good color performance and color-changing response performance is prepared by adopting a solvent evaporation method. The two-component reversible thermochromic microcapsule provided by the disclosure can effectively alleviate the color lag phenomenon of a traditional three-component thermochromic capsule.

Microcapsules comprising black pigments

Monolayered microcapsules comprising a black pigment and cosmetic formulations comprising them are provided for use particularly in mascara and eye liner formulations. The black pigment may be carbon black, black iron oxide, or both.

Microcapsules comprising black pigments

Monolayered microcapsules comprising a black pigment and cosmetic formulations comprising them are provided for use particularly in mascara and eye liner formulations. The black pigment may be carbon black, black iron oxide, or both.

Fibrous support comprising particles containing a partially water-soluble active agent, particles, and methods for producing said particles

The invention relates to a support consisting of natural and/or synthetic fibers which particles are held, which are preferably water-soluble, comprising at least one active agent, said particles at least partially releasing the active agent(s) under the effect of an external stress, characterized in the active agent has a water-solubility of between 0.1 and 60 wt. %, preferably between 0.1 and 30 wt. %.

Oxidized cellulose microspheres
10426730 · 2019-10-01 · ·

A process for forming microspheres is disclosed. The process includes contacting a solvent with a modified cellulose to form a solution; contacting the modified cellulose solution with at least one bioactive agent to form a discontinuous phase liquid; contacting the discontinuous phase liquid with a continuous phase liquid to form an emulsion; and contacting the emulsion with a third phase liquid to extract the solvent from the emulsion, thereby forming a plurality of modified cellulose microspheres.

Oxidized cellulose microspheres
10426730 · 2019-10-01 · ·

A process for forming microspheres is disclosed. The process includes contacting a solvent with a modified cellulose to form a solution; contacting the modified cellulose solution with at least one bioactive agent to form a discontinuous phase liquid; contacting the discontinuous phase liquid with a continuous phase liquid to form an emulsion; and contacting the emulsion with a third phase liquid to extract the solvent from the emulsion, thereby forming a plurality of modified cellulose microspheres.