Patent classifications
B01J19/243
Polymerisation unit and polymerisation process
The present invention relates to processes and apparatus useful for (fast) ionic polymerisation of liquid monomer(s) containing reaction mixture for the production of the corresponding polymer(s).
Continuous flow carboxylation reaction
The present invention is related to a two-step carboxylation reaction of an aryl group using continuous flow reaction conditions. This process permits large scale synthesis of useful reaction products in high yield.
FLOW TYPE REACTION DEVICE
An object of the present invention is to provide a flow type reaction device which is capable of maintaining reaction efficiency and productivity which are sufficient for practical use for a long time, and reducing the size and cost of the reaction device, and the present invention provides a flow type reaction device (1) for continuously reacting two or more kinds of raw materials, including a mixing section (10) which is configured to mix two or more kinds of the raw materials, and a reaction section (20) which is provided on a secondary side with respect to the mixing section (10), and configured to obtain a product by reacting two or more kinds of the raw materials, the mixing section (10) includes a mixing device (13) which is configured to mix two or more kinds of the raw materials, and two or more supply pipes (L11, L12) which are configured to supply each of two or more kinds of the raw materials to the mixing device (13), the supply pipes (L11, L12) are respectively connected to the mixing device (13), and at least one of the supply pipes (L11) has, in the vicinity of a connection portion of the supply pipe (L11) with the mixing device (13), a suppression mechanism which is configured to suppress movement of a fluid from the mixing device (13) to the supply pipe (L11).
DEPOSITION APPARATUS CAPABLE OF APPLYING POWDER PARTICLES, AND METHOD FOR APPLYING POWDER PARTICLES
An ALD or digital CVD apparatus and method for microparticles are proposed. The apparatus and the method use an impact, which is caused by the pulsed introduction of a precursor or a purging gas to be introduced into a reactor, without additional vibration or rotation of the reactor, so as to inhibit the agglomeration of particles to be applied to a surface and enable dispersion to be maximized, thereby enabling each particle to be uniformly applied, and simultaneously preventing the loss, in the reactor during processing, of powder to be coated without an additional separate filter or filler. A deposition reactor has a structure in which at least two overlapping reactors are provided. A reactant or a purging gas directly flows into an inner reactor in which a chemical reaction occurs. A purging step is simultaneously carried out in inner and outer reactors.
RING-OPENING POLYMERIZATIONS USING A FLOW REACTOR
Techniques regarding the synthesis of polyesters and/or polycarbonates through one or more ring-opening polymerizations conducted within a flow reactor and facilitated by a urea anion catalyst and/or a thiourea catalyst are provided. For example, one or more embodiments can comprise a method, which can comprise polymerizing, via a ring-opening polymerization within a flow reactor, a cyclic monomer in the presence an organocatalyst comprising a urea anion.
CONTINUOUS FLOW CATALYTIC REACTOR, ASSEMBLING METHOD THEREFOR AND APPLICATION THEREOF
A continuous flow catalytic reactor, an assembling method therefor and an application thereof includes a reaction vessel, a filler packaged in the reaction vessel and a charged catalytic component; the charged catalytic component is fixed to the filler under an action of a direct-current electric field. The continuous flow catalytic reactor may be applied to continuous flow reactions such as a monosaccharide epimerization reaction. A monosaccharide epimerization reaction method includes: providing the continuous flow catalytic reactor; electrically connecting the continuous flow catalytic reactor with a direct-current power supply, thereby to forming the direct-current electric field by electrically connecting the continuous flow catalytic reactor with the direct-current power supply; and heating a reactor container to a target temperature, and inputting a monosaccharide solution from a liquid flow inlet of the reaction vessel and then collecting a solution containing a target product from a liquid flow outlet of the reaction vessel.
METHOD AND DEVICE FOR TREATMENT OF LIQUID HYDROCARBONS
Disclosed is a method and a device for purification and desulfurization of liquid hydrocarbons, which, compared to sodium dispersion desulfurizing processes like already been disclosed, open up additional fields of application and greatly improves economy and achievable results.
Torrefaction process
A method of converting cellulosic feedstock to bio coal. The cellulosic feedstock in a carrier of process fluid is introduced within a conduit having substantially linear portions connected by curved portions creating a serpentine structure. The substantially linear portions are surrounded by tubular sleeves creating annular spaces between the tubular sleeves and substantially linear portions for carrying a high temperature fluid for transferring thermal energy to the cellulosic feedstock and process fluid. The cellulosic feedstock is maintained in an oxygen-free environment. The method is continuous as the cellulosic feedstock in process fluid is subjected to a plurality of mixing elements characterized as having no edges perpendicular to the longitudinal axes of the plurality of substantially linear segments and which are sized and positioned within the plurality of substantially linear segments such no mixing elements are in contact with one another resulting in an open region of travel for fluids passing from the conduit inlet to conduit outlet.
PROCESS FOR THE PREPARATION OF ETHYLENE HOMOPOLYMERS OR COPOLYMERS
A process for the preparation of ethylene homopolymers or copolymers in a facility having a high-pressure tubular reactor and a preheater, wherein a reaction fluid introduced into the reactor at a reactor inlet is heated in the preheater and the average velocity of the reaction fluid in the preheater is lower than the average velocity of the reaction fluid in the tubular reactor and the ratio of the average velocity in the tubular reactor to the average velocity of the reaction fluid in the preheater is in the range from 1.5 to 5.
METHOD FOR MANUFACTURING POLYMER AND FLOW-TYPE REACTION SYSTEM FOR MANUFACTURING POLYMER
The present invention provides a method for manufacturing a polymer by a flow-type reaction.
The method includes introducing a liquid A of an anionic polymerizable monomer, a liquid B of an anionic polymerization initiator, and a polymerization terminator into different flow paths, allowing the liquids to flow in the flow paths, allowing the liquid A and the liquid B to join together, subjecting the monomer to anionic polymerization while the liquids having joined together are flowing to downstream in a reaction flow path, and allowing a solution, which is obtained by the polymerization reaction and flows in the reaction flow path, and the polymerization terminator to join together so as to terminate the polymerization reaction and to obtain a polymer having a number-average molecular weight of 5,000 to 200,000.
A static mixer is disposed in the reaction flow path, and a polymer having a number-average molecular weight equal to or greater than 2,000 is introduced into an inlet port of the mixer. The present invention also provides a flow-type reaction system suitable for performing the manufacturing method.