Patent classifications
B01J2203/0625
METHOD FOR PREPARING HIGH-PRESSURE STATE MATERIAL CAPABLE OF BEING DETACHED FROM HIGH-PRESSURE DEVICE
The present invention relates to the field of materials, in particular to a method for preparing a high-pressure state material that can be detached from a high-pressure device. The method comprising: placing a carbon material and a target material into a high-pressure device, and subjecting the resultant to high-temperature and high-pressure treatment to obtain a diamond high-pressure chamber containing a high-pressure state material inside. The present invention enables the high-pressure state material (including the substance and its pressure state) to be preserved inside the diamond high-pressure chamber by mixing the carbon material and the target material and placing into the sample chamber of a conventional high-pressure device, and then transforming the carbon material into diamond using the high-temperature and high-pressure treatment. The diamond high-pressure chamber can be separated from the conventional high-pressure device and maintain the high-pressure state inside, thus allowing the high-pressure material to be studied and applied in an atmospheric pressure environment.
Method for obtaining synthetic diamonds from saccharose and an equipment for carrying out said method
The invention relates to a method for obtaining synthetic diamonds from sucrose, and to a device for carrying out said method, the method comprising: introducing sucrose or a solution of water and sucrose into a hermetic capsule without air, which is surrounded by an external container that keeps the volume of the capsule constant during the entire process; increasing the pressure inside the capsule by breaking down the sucrose inside the capsule, either by increasing the temperature or by combining the sucrose with sulfuric acid, until the carbon resulting from said pressure conditions of the capsule is transformed into diamond; and controlling the pressure generated inside the capsule, using containing means that apply pressure externally around the container of the capsule. In addition, extra carbon is added, increasing the dimensions of the diamond.
POLYCRYSTALLINE DIAMOND STRUCTURE
A polycrystalline diamond structure comprises a first region and a second region adjacent the first region, the second region being bonded to the first region by intergrowth of diamond grains. The first region comprises a plurality of alternating strata or layers, each or one or more strata or layers in the first region having a thickness in the range of around 5 to 300 microns. The polycrystalline diamond (PCD) structure has a diamond content of at most about 95 percent of the volume of the PCD material, a binder content of at least about 5 percent of the volume of the PCD material, and one or more of the layers or strata in the first region comprise and/or the second region comprises diamond grains having a mean diamond grain contiguity of greater than about 60 percent and a standard deviation of less than about 2.2 percent. There is also disclosed a method of making such a polycrystalline diamond structure.
METHODS FOR FORMING POLYCRYSTALLINE MATERIALS INCLUDING PROVIDING MATERIAL WITH SUPERABRASIVE GRAINS PRIOR TO HPHT PROCESSING
Grains of superabrasive material may be infiltrated with a molten metal alloy at a relatively low temperature, and the molten metal alloy may be solidified within interstitial spaces between the grains of superabrasive material to form a solid metal alloy having the grains of superabrasive material embedded therein. The solid metal alloy with the grains of superabrasive material embedded therein may be subjected to a high pressure and high temperature process to form a polycrystalline superabrasive material. A polycrystalline superabrasive material also may be formed by depositing material on surfaces of grains of superabrasive material in a chemical vapor infiltration process to form a porous body, which then may be subjected to a high pressure and high temperature process. Polycrystalline compacts and cutting elements including such compacts may be formed using such methods.
Cutting elements and earth-boring tools including a polycrystalline diamond material
Methods of forming polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure and a temperature sufficient to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool include a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.
Methods for forming polycrystalline materials including providing material with superabrasive grains prior to HPHT processing
Grains of superabrasive material may be infiltrated with a molten metal alloy at a relatively low temperature, and the molten metal alloy may be solidified within interstitial spaces between the grains of superabrasive material to form a solid metal alloy having the grains of superabrasive material embedded therein. The solid metal alloy with the grains of superabrasive material embedded therein may be subjected to a high pressure and high temperature process to form a polycrystalline superabrasive material. A polycrystalline superabrasive material also may be formed by depositing material on surfaces of grains of superabrasive material in a chemical vapor infiltration process to form a porous body, which then may be subjected to a high pressure and high temperature process. Polycrystalline compacts and cutting elements including such compacts may be formed using such methods.
Method of forming graphene material by graphite exfoliation
A method of producing graphene sheets and plates from graphitic material including (a) mixing graphitic material particles in a liquid medium to form a suspension; (b) compressing the suspension; (c) directing the compressed suspension through a local constriction into an area of reduced pressure to decompress the suspension in less than 210.sup.6 second to a pressure less than 20% of the compression pressure, thereby exfoliating graphene sheets and plates from the graphitic material.
METHOD OF FORMING GRAPHENE MATERIAL BY GRAPHITE EXFOLIATION
A method of producing graphene sheets and plates from graphitic material including (a) mixing graphitic material particles in a liquid medium to form a suspension; (b) compressing the suspension; (c) directing the compressed suspension through a local constriction into an area of reduced pressure to decompress the suspension in less than 210.sup.6 second to a pressure less than 20% of the compression pressure, thereby exfoliating graphene sheets and plates from the graphitic material.
CUTTING ELEMENTS FORMED USING LIQUID HYDROCARBONS AND HYDRATED HYDROCARBONS, AND EARTH-BORING TOOLS COMPRISING SUCH CUTTING ELEMENTS
Methods of forming polycrystalline diamond include encapsulating diamond particles and a hydrocarbon substance in a canister, and subjecting the encapsulated diamond particles and hydrocarbon substance to a pressure and a temperature sufficient to form inter-granular bonds between the diamond particles. Cutting elements for use in an earth-boring tool includes a polycrystalline diamond material formed by such processes. Earth-boring tools include such cutting elements.
Method for preparing high-pressure state material capable of being detached from high-pressure device
The present invention relates to the field of materials, in particular to a method for preparing a high-pressure state material that can be detached from a high-pressure device. The method comprising: placing a carbon material and a target material into a high-pressure device, and subjecting the resultant to high-temperature and high-pressure treatment to obtain a diamond high-pressure chamber containing a high-pressure state material inside. The present invention enables the high-pressure state material (including the substance and its pressure state) to be preserved inside the diamond high-pressure chamber by mixing the carbon material and the target material and placing into the sample chamber of a conventional high-pressure device, and then transforming the carbon material into diamond using the high-temperature and high-pressure treatment. The diamond high-pressure chamber can be separated from the conventional high-pressure device and maintain the high-pressure state inside, thus allowing the high-pressure material to be studied and applied in an atmospheric pressure environment.