B01J2208/0053

EBULLATED BED REACTOR UPGRADED TO PRODUCE SEDIMENT THAT CAUSES LESS EQUIPMENT FOULING

An ebullated bed hydroprocessing system is upgraded and operated at modified conditions using a dual catalyst system to produce less fouling sediment. The less fouling sediment produced by the upgraded ebullated bed reactor reduces the rate of equipment fouling at any given sediment production rate and/or concentration compared to the sediment produced by the ebullated bed reactor prior to upgrading. In some cases, sediment production rate and/or concentration are maintained or increased, after upgrading the ebullated bed reactor, while equipment fouling is reduced. In other cases, sediment production rate and/or concentration are increased, after upgrading the ebullated bed reactor, without increasing equipment fouling. In some cases, sediment production rate and/or concentration are decreased by a given percentage, after upgrading the ebullated bed reactor, and the rate of equipment fouling is decreased by a substantially greater percentage.

Hydrogen generation assemblies and hydrogen purification devices
11364473 · 2022-06-21 · ·

Hydrogen generation assemblies, hydrogen purification devices, and their components, and methods of manufacturing those assemblies, devices, and components are disclosed. In some embodiments, the devices may include an insulation base having insulating material and at least one passage that extends through the insulating material. In some embodiments, the at least one passage may be in fluid communication with a combustion region.

PROCESS AND PLANT FOR PRODUCING METHANOL FROM SUBSTOICHIOMETRIC SYNTHESIS GAS
20220185752 · 2022-06-16 ·

Proposed is a process for producing methanol from synthesis gas by means of multi-stage, for example two-stage, heterogeneously catalyzed methanol synthesis, wherein the methanol product formed in every synthesis stage is separated by condensation and the remaining residual gas is supplied to the downstream synthesis stage or after separation of a purge stream recycled to the first synthesis stage as a recycle stream. According to the invention after each synthesis stage the residual gas streams have separated from them a respective purge stream, from which, using one or more hydrogen recovery apparatuses, hydrogen is separated and recycled to the first synthesis stage. The ratio of the individual purge streams and their total molar flow may optionally be varied to allow better control of the reaction in the individual synthesis stages and to allow reaction to the advancing deactivation of the catalysts present therein.

Method and system for low detection limit EO using pressure, chiller and reactor
20220187201 · 2022-06-16 ·

A gas analysis system and method using a spectrometer, such as a Fourier transform infrared spectrometer, utilizes a reactor, such as a catalytic reactor, for providing interference spectra. The gas is pressurized and chilled to remove water prior to the spectrometer.

Reformer tube having a structured catalyst and improved heat balance

A reformer tube for producing synthesis gas by steam reforming of hydrocarbon-containing feed gases, in which a structured stream reforming catalyst is used, is proposed. According to the invention, a heat exchanger tube is arranged in the interior of the structured catalyst, with the feed gas stream flowing firstly through the structured catalyst and subsequently in countercurrent through the heat exchanger tube. This improves the heat exchange between the synthesis gas product stream and the structured catalyst and the feed gas stream flowing through it, especially in the radial direction.

Micro-interface strengthening reaction system and method for preparing ship fuel

The present invention relates to a micro-interface strengthening reaction system and method for heavy oil hydrogenation preparation of ship fuel, including a liquid phase feed unit, a gas phase feed unit, a micro-interface generator, a fixed-bed reactor and a separation tank. The present invention may reduce the pressure during the reaction by 10-80% while ensuring the efficiency of the reaction by breaking the gas to form micro-sized micro-bubbles and making the micro-bubbles mix with heavy oil to form an emulsion to increase the area between the gas and the liquid phase and to achieve the effect of enhancing mass transfer in a lower preset range. And, the present invention greatly enhances the mass transfer, so that the gas-liquid ratio can be greatly reduced. Also, the method of the present invention has low process severity, high production safety, low product cost per ton, and strong market competitiveness.

PROCESS TO CONDUCT AN ENDOTHERMIC STEAM REFORMING REACTION IN A FLUIDIZED BED REACTOR
20230271831 · 2023-08-31 ·

The disclosure relates to a process to perform an endothermic steam reforming of hydrocarbons, said process comprising the steps of providing a fluidized bed reactor comprising at least two electrodes and a bed comprising particles, wherein the particles are put in a fluidized state to obtain a fluidized bed; heating the fluidized bed to a temperature ranging from 500° C. to 1200° C. by passing an electric current through the fluidized bed to conduct the endothermic reaction. The process is remarkable in that the particles of the bed comprise electrically conductive particles and particles of a catalytic composition, wherein at least 10 wt. % of the particles are electrically conductive particles and have a resistivity ranging from 0.001 to 500 Ohm.Math.cm at 800° C. and in that the step of heating the fluidized bed is performed by passing an electric current through the fluidized bed.

PROCESS TO CONDUCT AN ENDOTHERMIC CATALYTIC CRACKING REACTION IN A FLUIDIZED BED REACTOR
20230271900 · 2023-08-31 ·

The disclosure relates to a process to perform a catalytic cracking reaction of hydrocarbons having at least four carbons, said process comprising the steps of providing a fluidized bed reactor comprising at least two electrodes and a bed comprising particles, wherein the particles are put in a fluidized state to obtain a fluidized bed; heating said bed to a temperature between 500° C. and 850° C. by passing an electric current through the fluidized bed to conduct the reaction. The process is remarkable in that the particles of the bed comprise electrically conductive particles and particles of a catalytic composition, wherein at least 10 wt. % of the particles are electrically conductive particles and have a resistivity from 0.001 to 500 Ohm.cm at 500° C. and in that the step of heating the fluidized bed is performed by passing an electric current through the fluidized bed.

PROCESS TO CONDUCT ENDOTHERMIC DIRECT PYROLYSIS OF METHANE IN A FLUIDIZED BED REACTOR
20230271899 · 2023-08-31 ·

The disclosure relates to a process to perform an endothermic methane pyrolysis reaction, said process comprising the steps of providing at least one fluidized bed reactor comprising at least two electrodes; and a bed comprising particles, wherein the particles are put in a fluidized state by passing upwardly through the said bed a fluid stream, to obtain a fluidized bed; heating the fluidized bed to a temperature ranging from 500° C. to 1200° C. to conduct the endothermic methane pyrolysis reaction; wherein the particles of the bed comprise electrically conductive particles and particles of a catalytic composition; wherein at least 10 wt. % of the particles are electrically conductive particles and have a resistivity ranging from 0.001 Ohm.Math.cm to 500 Ohm.Math.cm at 800° C. and wherein the step of heating the fluidized bed is performed by passing an electric current through the fluidized bed.

Method for improving reaction yield
11338262 · 2022-05-24 · ·

In a catalytic reaction, after a reaction product leaves a catalyst bed, an inert substance with a low temperature is sprayed, and through heat absorption and vaporization processes of the inert substance, the temperature of the reaction product drops rapidly when staying in a catalyst cushion layer at a discharge end of a fixed bed reactor, or in a space formed by the catalyst cushion layer at the discharge end of the fixed bed reactor and a reactor head, or in a space formed by a tube plate at the discharge end of the fixed bed reactor and the reactor head. The residence time of the reaction product is shortened due to the entrance of the inert substance in a gaseous state.