B01J2219/00166

Method for continuous polymerization of modified diene elastomer with lithium amide initiator

A process for the continuous synthesis of a modified diene elastomer comprising at least one silicon atom directly connected to the elastomer chain is provided. The process comprises polymerization by n reactors r1 to rn, considered to be continuous stirred-tank reactors equipped with an internal stirring system and arranged in series, n varying from 2 to 15. The reactor r1 is fed by an input solution comprising a solvent, one or more monomer(s), an anionic polymerization initiator chosen from lithium amides and a polar agent. The temperature of each reactor varies from 20° C. to 150° C. and is greater than or equal to the temperature of the reactor which immediately precedes it. The living diene elastomer obtained exhibits a polydispersity index varying from 1.1 to 1.7. The process further comprises modification of the living diene elastomer obtained in the preceding stage by a functionalization, coupling or star-branching agent.

SYSTEM, DEVICE AND METHOD FOR HYDROGEN PRODUCTION
20210371276 · 2021-12-02 ·

A system including a gas production device including (a) a solid containing compartment configured to contain a solid, (b) at least one fluid channel with an inlet and an outlet comprising an opening along at least a portion of its length, the opening facing the solid, (c) a solution compartment configured to contain a solution, the solution compartment: (1) being in fluid communication with the fluid channel inlet and outlet, (2) located along a fluid pathway in between the fluid channel outlet and inlet, and (3) at least one hydrogen gas outlet, (d) a fluid flow driver in fluid communication with the fluid pathway, and (e) a fluid flow rate regulator connected to the fluid flow driver. Disclosed is also a method for producing a gas (e.g., hydrogen).

CONTINUOUS PRODUCTION OF POLYURETHANE PREPOLYMERS

Described herein is a continuous process for producing polyurethane prepolymers in a residence time reactor with plug flow. Also described herein is a method of using these prepolymers for producing polyurethanes.

Micro-electrolysis reactor for ultra fast, oxidant free, C—C coupling reaction and synthesis of daclatasvir analogs thereof

The present invention relates to a continuous micro-electro-flow reactor system for ultra-fast, oxidant free, C—C coupling reaction for making symmetrical biaryls and analogs thereof. This invention further relates to the said process for preparation of antiviral drug, daclatasvir of general formula I.

Reactor System for the Production of High Value Chemical Products
20230271157 · 2023-08-31 ·

The invention is directed to a chemical reactor (100) having (a) two or more gas reactor elements (12) with each gas reactor element (12) having (i) a first reaction chamber (38), and (ii) a feed assembly unit (36), (b) a second reaction chamber (20) coupled with each of the two or more gas reactor elements (12) and configured to independently receive two or more product streams from the two or more gas reactor elements (12); and optionally, (c) a gas converging section (40) located downstream to the second reaction chamber (20). The invention is further directed to a method of producing chemical products using the chemical reactor (100) of the present invention.

Continuous flow processes for making bicyclic compounds

Processes for making bicyclic compounds and precursors thereof, and particularly for making [1.1.1]propellane and bicyclo[1.1.1]pentane and derivatives thereof, utilize continuous flow reaction methods and conditions. A continuous process for making [1.1.1]propellane can be conducted under reaction conditions that advantageously minimize clogging of a continuous flow reactor. A continuous flow process can be used to make precursors of [1.1.1]propellane.

Fluidized Bed Reactor Apparatus and a Method for Processing Organic Material Using a Fluidized Bed Reactor Apparatus
20220152569 · 2022-05-19 ·

Fluidized bed reactor apparatus, comprising a cylindrical reactor chamber (10), and a rotating shaft (14) equipped with radially extending fluidization units (16) disposed in the reactor chamber (10), said rotating shaft (14) being connected to a drive unit (42). The apparatus further comprising means for feeding fluidizing bed material into the rector chamber (10), creating a fluidized bed (28) in the reactor chamber (10), means for feeding organic material that shall be processed into the fluidized bed (28) in the reactor chamber (10), and one or more outlets (22,24) for discharge of material, gases and vapors, wherein the process in the reactor chamber (10) is controlled by a control system (40) connected to at least the drive unit (42). The invention also relates to a method for processing organic material using a fluidized bed reactor apparatus.

SAFE PYROLYTIC EXTRACTION OF DISINFECTING AGENTS FROM OILS
20220151243 · 2022-05-19 ·

Described herein are methods for producing multiple disinfecting agents from oils and reactors for producing multiple disinfecting agents from oils.

METHODS AND REACTORS FOR PRODUCING MULTIPLE DISINFECTING AGENTS FROM OILS
20220151239 · 2022-05-19 ·

Described herein are methods for producing multiple disinfecting agents from oils, including waste oils, and reactors for producing multiple disinfecting agents from the oils.

CONTINUOUS SYNTHESIS OF UPCONVERTING NANOPARTICLES
20230242412 · 2023-08-03 ·

Synthesizing upconverting nanoparticles includes heating a precursor solution comprising one or more rare earth salts, an alkali metal salt or alkaline earth salt, and a solvent comprising a plasticizer in a microwave reactor to yield a product mixture, and cooling the product mixture to yield the upconverting nanoparticles. Core-shell upconverting nanoparticles are synthesized by combining the upconverting nanoparticles with a precursor solution comprising one or more rare earth salts, an alkali metal salt or alkaline earth salt, and a solvent comprising a plasticizer to yield a nanoparticle mixture, heating the nanoparticle mixture in a microwave reactor to yield a product mixture, and cooling the product mixture to yield the core-shell upconverting nanoparticles.