The present invention relates, in general, to the purification of boron trichloride (BCl.sub.3). More particularly, the invention relates to a process for minimizing silicon tetrachloride (SiCl.sub.4) formation in BCl.sub.3 production and/or the removal of SiCl.sub.4 in BCl.sub.3 product stream by preventing/minimizing the silicon source in the reaction chambers. In addition, a hydride material may be used to convert any SiCl.sub.4 present to SiH.sub.4 which is easier to remove. Lastly freeze separation would replace fractional distillation to remove SiCl.sub.4 from BCl.sub.3 that has been partially purified to remove light boilers.

An industrial microwave ultrasonic reactor has an inner wall liner. A microwave generation device is formed by microwave units distributed on an outer sidewall, or by a microwave pipe disposed outside the reactor and microwave units distributed on the microwave pipe. One end of the microwave pipe communicates with the bottom of the reactor via a connection pipe I, and the other end communicates with the top via a return pipe. A shield is disposed outside the microwave generation device to separate the microwave units from the outside, and a heat removal device is disposed outside the shield. An ultrasonic wave generation device is formed by 10 to 30 sets of ultrasonic pulse units disposed at intervals along the outer sidewall. Each set has 10 to 50 members distributed along the circumferential direction of the reactor. A stirring shaft is fixed below a stirring motor and extends into the reactor.

An apparatus for producing a mixed solution, comprising a mixing vessel for preparing an aqueous mixed solution containing a dicarboxylic acid and a Nb compound and a filter for the aqueous mixed solution connected to the mixing vessel via a pipe, the mixing vessel being anticorrosive and equipped with a stirring unit, a heating unit and a cooling unit for the aqueous mixed solution, wherein the aqueous mixed solution prepared in the mixing vessel is fed to the filter via the pipe and filtered in the filter under increased pressure.

A glass lined reaction tank for chemical and pharmaceutical industries and a manufacturing method thereof. One-step molding technical standards for manufacturing iron blanks of the glass lined reaction tanks are deeply developed, an overall structure of a flanged big flange of a tank body and a tank cover matching with the tank body are innovated, and nominal pressure of the big flange and the sealing performance of a tank mouth are perfectly improved. By using a new structurally-combined precise controlled internal heating type electric furnace and an intelligent temperature program control/adjustment/recording instrument, heating temperature of an overall glass lining layer on an inner wall of the tank body is more accurately controlled to be the same, and a synchronous, integral and controlled sintering core technique is realized.

A flow reactor can promote a reaction under appropriate temperature management, can precent reaction fluid or generated gas from being trapped in a heat transmission part, can be disassembled for easy cleaning, and to which a coating or lining can be applied. This flow reactor is provided with two flow paths, a reaction flow path and a second flow path, in a space formed between an inner cylinder and an outer cylinder that are concentric. A spiral heat transmission body is disposed between the inner cylinder and the outer cylinder, and the spiral heat transmission body has a substantially triangular cross-sectional shape in an axial cross-sectional view. The spiral heat transmission body partitions the space into the reaction flow path and the second flow path, and heat is exchanged via the spiral heat transmission body between a reaction fluid F1 flowing through the reaction flow path and a heat medium F2 flowing through the second flow path.