B01J2219/0218

Method and apparatus for preparing transition metal lithium oxide

The present disclosure provides a method for preparing a transition metal lithium oxide, comprising steps of: A) mixing a lithium salt and a transition metal compound, and performing a pretreatment to obtain a precursor; wherein the pretreatment temperature is 100-300° C.; and the pretreatment time is 1-10 h; B) precalcining the precursor to obtain an intermediate; and C) continuously feeding the intermediate into a feed port of a moving bed reactor, and calcining, to obtain a transition metal lithium oxide. In the present disclosure, a pretreatment process is performed before the precalcination, and the pretreatment temperature and time are further limited, thereby solving the problem of material hardening during the calcination process of battery materials. In conjunction with using a moving bed reactor, the gas phase and the solid phase are sufficiently contacted, and at the same time the thickness of the filler is increased, the productivity is enhanced and the oxygen consumption is largely decreased at the same time. The present disclosure further provides an apparatus for preparing a transition metal lithium oxide.

Universal Chemical Processor with Radioisotope Source
20230128332 · 2023-04-27 ·

A universal chemical processor (UCP) including a reactor vessel having a central longitudinal axis and main chamber comprises a first inlet port for a main feedstock, a second inlet port for a fluidizing medium and a third inlet port for one or more reactants. The UCP also includes a reactive radioactive chemical processor (R.sup.2CP) that contains a radioactive element positioned extending along the longitudinal axis in the main chamber. In operation, a fluidized bed can be supported in the main chamber when a fluidizing medium and feedstock are supplied to the main chamber through the first and second inlet ports and the radioactive element of the R.sup.2CP emits ionizing radiation that is capable of ionizing feedstock and reactants, inducing chemical reactions, and sterilizing and decomposing any organic materials within a radiation zone.

Combustion chamber hot face refractory lining

A refractory lining in a combustion chamber operating in a reducing atmosphere. The lining includes at least one or more Zirconia (Zr)-based refractory lining members comprising one or more Zr-based parts. The Zr-based parts comprise at least 90 wt. %, preferably at least 95 wt. %, of monoclinic ZrO.sub.2 and/or partially stabilized ZrO.sub.2 and/or fully stabilized ZrO.sub.2, wherein the total content of tetragonal and cubic ZrO.sub.2 amounts to at least 20 wt. %, preferably more than 35 wt. %, as well as Zr based refractory lining members and methods for manufacturing the Zr based refractory lining members.

CERAMIC COATING ON METAL PARTS TO REDUCE DEPOSIT OF METALLIC TRANSITION METALS IN HYDROGENATION REACTIONS

The present invention relates to a method of reducing the deposit of metallic transition metal, particularly palladium, on a metal part in hydrogenation reactions using hydrogen and a heterogenous supported palladium catalyst. These metallic transition metal deposit, particularly palladium deposits, are particularly formed at areas which are exposed to high velocity and shear forces of the hydrogenation mixture comprising the transition metal catalyst, particularly palladium catalyst. They are significantly reduced or even avoided when the surface of the respective metal parts are coated by a plasma sprayed ceramic coating.

X-SHAPED REFRACTORY ANCHOR DEVICE AND SYSTEM

Refractory anchoring devices include a main body and a mounting feature for mounting to a thermal vessel. The main body includes four anchor branch segments angled with respect to each other to form an X shape with four unenclosed cell openings, including two opposite triangular side openings and two opposite triangular end openings. In some embodiments, the main body further includes extension segments extending from and angled relative to respective branch segments to define two of the opposite openings as semi-hexagonal. Some embodiments include reinforcement segments extending from branch segments into openings, voids extending through branch segments, two anchor strips inter-engaged to form the four branch segments, and/or a single stud-welding stud for the mounting feature. Refractory anchoring systems and methods include an array of the refractory anchoring devices arranged and mounted so that the unenclosed openings of adjacent anchoring devices cooperatively form substantially hexagonal and rhombus shaped cells.

X-SHAPED REFRACTORY ANCHOR DEVICE AND SYSTEM

Refractory anchoring devices include a main body and a mounting feature for mounting to a thermal vessel. The main body includes four anchor branch segments angled with respect to each other to form an X shape with four unenclosed cell openings, including two opposite triangular side openings and two opposite triangular end openings. In some embodiments, the main body further includes extension segments extending from and angled relative to respective branch segments to define two of the opposite openings as semi-hexagonal. Some embodiments include reinforcement segments extending from branch segments into openings, voids extending through branch segments, two anchor strips inter-engaged to form the four branch segments, and/or a single stud-welding stud for the mounting feature. Refractory anchoring systems and methods include an array of the refractory anchoring devices arranged and mounted so that the unenclosed openings of adjacent anchoring devices cooperatively form substantially hexagonal and rhombus shaped cells.

Process for the positioning of a corrosion-resistant coating on a wall of an item of equipment of a FCC unit
11266967 · 2022-03-08 · ·

The invention relates to a process for the positioning of a corrosion-resistant coating on an internal or external metal wall (20) of a fluid catalytic cracking unit chamber, comprising: (i) the shaping of a metal anchoring structure (10) formed from a plurality of strips (12) assembled in pairs by joining assembly portions (121, 122) so as to form a plurality of cells (14), the anchoring structure comprising a plurality of fastening tabs (16) integral with strip portions other than assembly portions, (ii) the fastening of said anchoring structure (10) by welding the free edge (18) of a part at least of the fastening tabs to the metal wall (20), defining a space between a longitudinal edge (12b) of an anchoring structure and the metal wall, (iii) the insertion of a composite material into the cells (14) from the metal wall (20) and at least up to the upper longitudinal edge (12a) of each strip.

METHOD AND APPARATUS FOR PREPARING TRANSITION METAL LITHIUM OXIDE

The present disclosure provides a method for preparing a transition metal lithium oxide, comprising steps of: A) mixing a lithium salt and a transition metal compound, and performing a pretreatment to obtain a precursor; wherein the pretreatment temperature is 100-300° C.; and the pretreatment time is 1-10 h; B) precalcining the precursor to obtain an intermediate; and C) continuously feeding the intermediate into a feed port of a moving bed reactor, and calcining, to obtain a transition metal lithium oxide. In the present disclosure, a pretreatment process is performed before the precalcination, and the pretreatment temperature and time are further limited, thereby solving the problem of material hardening during the calcination process of battery materials. In conjunction with using a moving bed reactor, the gas phase and the solid phase are sufficiently contacted, and at the same time the thickness of the filler is increased, the productivity is enhanced and the oxygen consumption is largely decreased at the same time. The present disclosure further provides an apparatus for preparing a transition metal lithium oxide.

Anchoring mesh for an anti-erosion coating
11065596 · 2021-07-20 · ·

The invention relates to a metal anchoring mesh intended to be secured to a metal wall of a chamber of a fluid catalytic cracking unit, in order to form cells (64). Said metal anchoring mesh comprises a plurality of wavy elementary parts (12, 14) connected successively together, forming cylindrical surfaces that are able to respectively define said cells, said cylindrical surfaces each having a central axis of symmetry A, the wavy elementary parts (12,14) each having protruding tongues (42′, 44′), said protruding tongues being able to extend respectively inside said cells (64). Said tongues (42′, 44′) extend along a length less than a quarter of the distance d that extends between said cylindrical surface and said central axis of symmetry A of said cylindrical surface.

COMBUSTION CHAMBER HOT FACE REFRACTORY LINING

A refractory lining in a combustion chamber operating in a reducing atmosphere. The lining includes at least one or more Zirconia (Zr)-based refractory lining members comprising one or more Zr-based parts. The Zr-based parts comprise at least 90 wt. %, preferably at least 95 wt. %, of monoclinic ZrO.sub.2 and/or partially stabilized ZrO.sub.2 and/or fully stabilized ZrO.sub.2, wherein the total content of tetragonal and cubic ZrO.sub.2 amounts to at least 20 wt. %, preferably more than 35 wt. %, as well as Zr based refractory lining members and methods for manufacturing the Zr based refractory lining members.