Patent classifications
B01J2219/0263
Fluidized bed reactor and a process using same to produce high purity granular polysilicon
The present invention relates to a fluidized bed reactor, comprising a reaction tube, a distributor and a heating device, the reaction tube and the distributor at the bottom of the reaction tube composing a closed space, the distributor comprising a gas inlet and a product outlet, and the reaction tube comprising a tail gas outlet and a seed inlet at the top or upper part respectively, characterized in that the reaction tube comprises a reaction inner tube and a reaction outer tube, and the heating device is an induction heating device placed within a hollow cavity formed between the external wall of the reaction inner tube and the internal wall of the reaction outer tube, wherein the hollow cavity is filled with hydrogen, nitrogen or inert gas for protection, and is able to maintain a pressure of about 0.01 to about 5 MPa; and also to a process of producing high purity granular polysilicon using the reactor. The fluidized bed reactor according to the present invention uses induction heating to heat directly the silicon particles inside the reaction chamber, such that the temperature of the reaction tube is lower than that inside the reaction chamber, which accordingly avoids deposition on the tube wall and results in more uniform heating, and thus is useful for large diameter fluidized bed reactors with much increased output for a single reactor.
PROCESS FOR MAKING A LITHIATED TRANSITION METAL OXIDE
Process for manufacturing a lithiated transition metal oxide, said process comprising the steps of (a) mixing at least one lithium salt and a precursor selected from transition metal oxides, transition metal oxyhydroxides, transition metal hydroxides, and transition metal carbonates, (b) pre-calcining the mixture obtained in step (a) at a temperature in the range of from 300 to 700° C., and (c) calcining the pre-calcined mixture according to step (b) in a multi-stage fluidized bed reactor at a temperature in the range of from 550° C. to 950° C., wherein the temperatures in step (b) and (c) are selected in a way that step (c) is being performed at a temperature higher than that of step (b).
Pressurized Fluid Mixing Device
A pressurized fluid mixing device is disclosed, including an inner casing and an outer casing. A first channel is arranged in the inner casing and includes one or more unit channels, adjacent unit channels of which are communicated with each other, flow blocking members are fixed on the unit channels, the inner casing is provided with one or more first inlets and one or more first outlets, a second channel is arranged in the outer casing, the outer casing is provided with one or more second inlets and one or more second outlets, and the inner casing is fixed on the second channel.
Continuous tubular reactor and method of operating the same
A continuous tubular reactor includes a rotary reaction tube having a reactant inlet and a product outlet, and including a ceramic; a heating device disposed outside the rotary reaction tube; and an angle adjuster adjusting an angle of a rotation axis of the rotary reaction tube. The angle of the rotation axis is 75° or less with respect to a horizontal surface.
MANUFACTURING APPARATUS OF CARBIDE
A manufacturing apparatus of carbide of the present disclosure includes a tank, a lid, a molten salt crucible, an electrode assembly, an air intake device and a heating device. The lid is connected to the tank to jointly delimit a compartment. The molten salt crucible is disposed in the compartment for containing a salt. The electrode assembly includes a working electrode and a counter electrode. An end of the working electrode and an end of the counter electrode both contact the salt in the molten salt crucible, and the end of the working electrode contacting the salt is for fixing a reactant tablet. The air intake device is configured to exchange the air in the compartment. The heating device is configured to heat the compartment.
MATERIALS SYSTEMS FOR INHIBITING PENETRATION OF MOLTEN SALTS, METHODS THEREFOR, AND DEVICES PROVIDED THEREWITH
Materials systems resistant to penetration of molten salts and may be present within a molten-salt-facing wall of a device for containing a molten salt bath at an elevated temperature, and molten-salt-facing walls and devices formed by such materials systems. A first layer of such a system defines an outer surface for direct contact with the molten salt bath, and resists erosion and corrosion and is penetrable by the molten salt at the elevated temperature. A second layer is located adjacent to the first layer and exhibits little or no wetting by the molten salt so that at least a portion of a thickness of the second layer is not penetrable by the molten salt. A third layer is located adjacent to the second layer and is porous and exhibits a low thermal conductivity at the elevated temperature.
QUANTUM DOT MANUFACTURING VESSEL AND QUANTUM DOT MANUFACTURING METHOD USING THE SAME
A quantum dot synthesizing vessel includes an accommodation part which accommodates a reaction mixture therein, and an outer part which includes a microwave absorbing material and covers the accommodation part, where a plurality of openings exposing at least a portion of the accommodation part is defined in the outer part.
IMPROVED HEAT EXCHANGE FLOW REACTOR
A flow reactor includes a flow reactor module having a heat exchange fluid enclosure with an inner surface sealed against a surface of a process fluid module, the inner surface having two or more raised ridges crosswise to a heat exchange flow direction from an inflow port or location to an outflow port or location and having a gap of greater than 0.1 mm between the two or more raised ridges and the surface of the process module.
Analytical device for constituents of a sample
An analytical device for determining a measured variable dependent on the concentration of one or more constituents of a sample includes a decomposition reactor surrounded by an insulating tube, a heating apparatus, an oxygen production system including at least one oxygen permeable membrane, a housing, and a feed gas guiding system for supplying a feed gas to the at least one membrane of the oxygen production system. The feed gas guiding system includes a reaction space surrounding the at least one membrane and is connected with an inflow duct open to the environment such that at least two partitions are arranged coaxially within the insulating tube and surrounding the decomposition reactor, where the partitions subdivide an intermediate space arranged between the decomposition reactor and the insulating tube into annular chambers forming the feed gas guiding system, where the annular chambers are connected with one another by overflow openings.
Recombinator
A recombinator for the catalytic recombination of hydrogen and oxygen generated in energy converters, in particular accumulators, to form water, comprising a housing in which a volume space is formed, into which the gases can flow via an opening and in which a recombination device is arranged that comprises a portion for a catalyst material and a portion for an absorption material, wherein the flow path of the gases to be recombined extends through the portion comprising the absorption material into the portion comprising the catalyst material, wherein a distance space is formed between the portion comprising the absorption material and the portion comprising the catalyst material, wherein the catalyst material is configured as a catalyst bar, the catalyst bar is arranged in a first gas-permeable tube and the distance space is formed in a gap space between the inner walling of the first gas-permeable tube and the outer wall of the catalyst bar.