A jacketed vessel for temperature control of contents within the vessel is provided. The vessel has a shell and an external jacket through which heating or cooling fluid is circulated. The jacket is formed by a length of conduit arranged in a spiral orientation around the vessel shell. The conduit has a center portion having a concave inner surface and has opposing side portions having convex inner surfaces. Edge sections of each side portion are welded to the exterior surface of the shell to form the jacket. Edge sections of adjacent arcs of conduit may be simultaneously welded to the shell in a single weld pass. The shape of the conduit provides improved heat transfer and pressure drop characteristics, as well as improvements in the vessel manufacturing process.

In various embodiments, a microreactor features a corrosion-resistant microchannel network encased within a thermally conductive matrix material that may define therewithin one or more hollow heat-exchange conduits.

A universal chemical processor (UCP) including a reactor vessel having a central longitudinal axis and main chamber comprises a first inlet port for a main feedstock, a second inlet port for a fluidizing medium and a third inlet port for one or more reactants. The UCP also includes a reactive radioactive chemical processor (R.sup.2CP) that contains a radioactive element positioned extending along the longitudinal axis in the main chamber. In operation, a fluidized bed can be supported in the main chamber when a fluidizing medium and feedstock are supplied to the main chamber through the first and second inlet ports and the radioactive element of the R.sup.2CP emits ionizing radiation that is capable of ionizing feedstock and reactants, inducing chemical reactions, and sterilizing and decomposing any organic materials within a radiation zone.

The present invention relates to a method of reducing the deposit of metallic transition metal, particularly palladium, on a metal part in hydrogenation reactions using hydrogen and a heterogenous supported palladium catalyst. These metallic transition metal deposit, particularly palladium deposits, are particularly formed at areas which are exposed to high velocity and shear forces of the hydrogenation mixture comprising the transition metal catalyst, particularly palladium catalyst. They are significantly reduced or even avoided when the surface of the respective metal parts are coated by a plasma sprayed ceramic coating.

A jacketed vessel for temperature control of contents within the vessel is provided. The vessel has a shell and an external jacket through which heating or cooling fluid is circulated. The jacket is formed by a length of conduit arranged in a spiral orientation around the vessel shell. The conduit has a center portion having a concave inner surface and has opposing side portions having convex inner surfaces. Edge sections of each side portion are welded to the exterior surface of the shell to form the jacket. Edge sections of adjacent arcs of conduit may be simultaneously welded to the shell in a single weld pass. The shape of the conduit provides improved heat transfer and pressure drop characteristics, as well as improvements in the vessel manufacturing process.

According to an embodiment, a method for preparing a sea urchin-shaped zinc oxide (ZnO) nanowire comprises preparing a mixture of a ZnO nano-powder and a graphite powder and irradiating the mixture, in a container, with a microwave.

In various embodiments, a microreactor features a corrosion-resistant microchannel network encased within a thermally conductive matrix material that may define therewithin one or more hollow heat-exchange conduits.

A method for producing a lithium bis(fluorosulfonyl)imide salt F—(SO.sub.2)—NLi—(SO.sub.2)—F, comprising a step comprising a step of chlorination of sulfamic acid HO—(SO.sub.2)—NH.sub.2 in order to obtain the bis(chlorosulfonyl)imide Cl—(SO.sub.2)—NH—(SO.sub.2)—Cl, said step being carried out in a reactor made of a corrosion-resistant material M3, or in a reactor containing a base layer made of a material M1 coated with a surface layer made of a corrosion-resistant material M2.

A process for producing a lithium bis(fluorosulfonyl)imide salt F(SO.sub.2)NLi(SO.sub.2)-F involving a step (b) with a step of fluorinating bis(chlorosulfonyl)imide Cl(SO.sub.2)NH(SO.sub.2)Cl with anhydrous HF, optionally in at least one organic solvent OS1, said step (b) being carried out in a reactor made of a material M3 that is resistant to corrosion, or in a reactor that contains a base layer made of a material M1 coated with a surface layer made of a material M2 that is resistant to corrosion.

An object of the present invention is to prevent stress-corrosion cracking of a header (40) of a reactor. A reactor for producing trichlorosilane by causing metal silicon powder and a hydrogen chloride gas to react with each other includes a cooler (70), the cooler including a plurality of heat transfer medium pipes (30) and a header (40), the plurality of heat transfer medium pipes being provided in a fluid bed (60) inside the reactor, the header being provided in a freeboard section (50) inside the reactor, the header being comprised of a corrosion-resistant material.