B01J2219/3325

Method of preparing aromatic vinyl compound-vinyl cyanide compound polymer and apparatus for preparing the same

A method of preparing an aromatic vinyl compound-vinyl cyanide compound polymer includes polymerizing a reaction mixture containing an aromatic vinyl compound, a vinyl cyanide compound, and an organic solvent in a reactor and transferring the vaporized reaction mixture present in the upper space of the reactor to a heat exchanger via a pipe and condensing the vaporized reaction mixture. The condensed reaction mixture is transferred to one side of the pipe and sprayed into the pipe, the flow velocity of the reaction mixture vaporized in the reactor is reduced, and temperature is lowered. Accordingly, a phenomenon wherein polymer particles in a reactor are sucked into a heat exchanger is prevented, and occurrence of polymerization in the heat exchanger is suppressed. Therefore, productivity and quality may be improved.

Packing, method for manufacturing same, and liquid film-forming structure

A packing for gas-liquid contact has at least one packing element of a thin layer shape, placed in a standing position. The packing element has a main body portion having a planar liquid film-forming surface extending along a liquid flow direction, and at least one wall portion provided to stand relative to the liquid film-forming surface and extending along the liquid flow direction. The wall portion has a side surface inclined at a predetermined angle to the liquid film-forming surface in a surface position of a liquid film to be formed by a liquid on the liquid film-forming surface.

Packing for improving contact between a gas phase and a dispersed solid phase moving in counter-current flow

The present invention describes a packing with a three-dimensional structure which is particularly suited to creating homogenous and anisotropic mixing between a gas phase and a dispersed solid phase moving in counter-current flow. Application of this packing to the stripper of fluidized catalytic cracking units.

Method for recycling carbon dioxide
11142461 · 2021-10-12 · ·

The method for recycling carbon dioxide according to the present invention includes: injecting a reaction gas containing carbon dioxide and a carbon raw material into a rotary heating furnace; reacting the reaction gas and the carbon raw material with each other in the rotary heating furnace to generate a hydrocarbon precursor containing carbon monoxide; and converting the hydrocarbon precursor into a hydrocarbon compound, thereby exhibiting excellent conversion rate of carbon dioxide.

POLYMERISATION UNIT AND POLYMERISATION PROCESS

The present invention relates to processes and apparatus useful for (fast) ionic polymerisation of liquid monomer(s) containing reaction mixture for the production of the corresponding polymer(s).

STRIPPER AND PACKING APPARATUSES

A packing system includes a first packing element layer including a plurality of blades and a second packing element layer including a plurality of blades. The packing system includes intra-layer variation and/or inter-layer variation. Intra-layer variation includes (i) varying spacing between blades within the first and/or the second packing element layer, (ii) varying sizes of the blades within the first and/or the second packing element layer, and/or (iii) varying angle of inclination of the blades within the first and/or second packing element layer. Inter-layer variation includes the blades of the first packing layer having a first spacing, a first size and a first angle of inclination, and the blades of the second packing layer having a second spacing, a second size, and a second angle of inclination. The second spacing, size, and/or angle of inclination is different from the first spacing, size, and/or angle of inclination.

Device for gas solids fluidized system to enhance stripping

A device for the intimate mixing of solid particles and a gaseous medium within a gas-solid fluidized bed, comprising a plurality corrugated and/or ribbed planar stanchions arranged in alternating intersecting planes that provide a plurality of open spaces between or adjacent the alternating intersecting planar stanchions. The element has a three-dimensional lattice configuration and the corrugated and/or ribbed planar stanchions are formed from metal having peaks and valleys or ribs, such that the peaks and valleys or ribs are angled at less than 90 degrees from the fall-line of the planar stanchion when assembled into the element. The angled peaks and valleys or ribs form channels that enhance lateral movement of catalyst particles into the spaces between the stanchions to provide improved vapor/solids mixing and contact.

METHOD OF PREPARING AROMATIC VINYL COMPOUND-VINYL CYANIDE COMPOUND POLYMER AND APPARATUS FOR PREPARING THE SAME

A method of preparing an aromatic vinyl compound-vinyl cyanide compound polymer includes polymerizing a reaction mixture containing an aromatic vinyl compound, a vinyl cyanide compound, and an organic solvent in a reactor and transferring the vaporized reaction mixture present in the upper space of the reactor to a heat exchanger via a pipe and condensing the vaporized reaction mixture. The condensed reaction mixture is transferred to one side of the pipe and sprayed into the pipe, the flow velocity of the reaction mixture vaporized in the reactor is reduced, and temperature is lowered. Accordingly, a phenomenon wherein polymer particles in a reactor are sucked into a heat exchanger is prevented, and occurrence of polymerization in the heat exchanger is suppressed. Therefore, productivity and quality may be improved.

Process for Preparing Fluorobenzene and Benzoic Acid Hypofluorite

The invention relates to a use of a fluorination gas, the elemental fluorine (F2) is preferably present in a high concentration, e.g. in a concentration of elemental fluorine (F2), especially of equal to much higher than 15% or even 20% by volume (i.e., at least 15% or even 20% by volume), and to a process for the manufacture of a fluorinated benzene starting from benzoic acid by direct fluorination employing a fluorination gas. The elemental fluorine (F.sub.2) is preferably present in high concentration, and subsequent decarboxylation of the benzoic acid hypofluorite obtained by direct fluorination. The process of the invention is also directed to the manufacture of benzoic acid hypofluorite by direct fluorination of benzoic acid. Especially the invention is of interest in the preparation of fluorinatedbenzene, final products and as well intermediates, for usage in agro-, pharma-, electronics-, catalyst, solvent and other functional chemical applications.

Process for Preparing Fluorobenzene Derivatives and Benzoic Acid Hypofluorite Derivatives

The invention relates to a use of a fluorination gas, and the elemental fluorine (F.sub.2) is preferably present in a high concentration, for example, in a concentration of elemental fluorine (F.sub.2), especially of equal to much higher than 15% or even 20% by volume, and to a process for the manufacture of a fluorinated benzene derivative starting from benzoic acid derivative by direct fluorination employing a fluorination gas, wherein the elemental fluorine (F.sub.2) is preferably present in a high concentration, and subsequent decarboxylation of the benzoic acid hypofluorite derivative obtained by direct fluorination. The process of the invention is also directed to the manufacture of a benzoic acid hypofluorite derivative by direct fluorination of benzoic acid derivative. Especially the invention is of interest in the preparation of fluorinated benzene derivative, final products and as well intermediates, for usage in agro-, pharma-, electronics-, catalyst, solvent and other functional chemical applications.