Techniques for debinding additively fabricated parts are described that do not require solvent debinding or catalytic debinding, and that may be performed using only thermal debinding in a furnace. As a result, in at least some cases debinding and sintering may take place sequentially within a single furnace. In some embodiments, the techniques may utilize particular materials as binders that allow for a thermal debinding process that does not negatively affect the parts.

A method for heat treating a powder part preform including a titanium alloy, includes heat treating the preform in a furnace at a predefined temperature, wherein the preform is on a holder during the heat treatment. The holder includes a titanium alloy having a mass titanium content no lower than 45%, or a zirconium alloy having a mass zirconium content no lower than 95%, wherein the material making up the holder has a melting temperature higher than the predefined heat treatment temperature, and an antidiffusion barrier is arranged between the preform and the holder to prevent the preform from becoming welded to the holder.

A method for heat treating a powder part preform including a titanium alloy, includes heat treating the preform in a furnace at a predefined temperature, wherein the preform is on a holder during the heat treatment. The holder includes a titanium alloy having a mass titanium content no lower than 45%, or a zirconium alloy having a mass zirconium content no lower than 95%, wherein the material making up the holder has a melting temperature higher than the predefined heat treatment temperature, and an antidiffusion barrier is arranged between the preform and the holder to prevent the preform from becoming welded to the holder.

In an example, a method includes monitoring a temperature of a layer of build material within an additive manufacturing apparatus. A power level of a first heating element heating the layer of build material may be controlled based on the monitored temperature and a power level of a second heating element heating the layer of build material may be controlled according to a predetermined power level scheme.

A method for hot isostatic pressing includes the steps of providing or obtaining an article of manufacture, which optionally includes a copper or nickel alloy, disposing the article of manufacture in a shroud, the shroud defining an enclosed volume wherein the article of manufacture is disposed, the shroud being configured as a multi-piece joined structure to retard gaseous mass transport from outside the shroud to inside the enclosed volume, disposing the shroud in a containment vessel of a hot isostatic pressing apparatus and disposing a getter material in the shroud and/or in the containment vessel, and introducing an inert gas at an elevated temperature and pressure into the containment vessel for hot isostatic pressing.

Systems and methods for a stabilized evaporable getter for increased handleability is provided. In certain embodiments, a method includes preparing a first getter material, a second getter material, and a metal material. Additionally, the method includes mixing the first getter material, the second getter material, and the metal material into a mixed getter material. Further, the method includes placing the mixed getter material into a getter holder. Also, the heat-treating the getter holder at a temperature below an activation temperature for an exothermic reaction of the mixed getter material but above a melting temperature of the metal material.

A method is provided in which a lower box comprising a base, walls that surround the base and an open side, and an upper box comprising a cover, walls that surround the cover and an open side are provided. One or more objects are arranged on the base of the lower box. The object(s) are covered with the upper box such that the open side of the upper is oriented towards the base of the box, the walls of the upper box are arranged on the base of the lower box and a gap is formed between the walls of the upper box and the walls of the lower box. A powder material is introduced into the gap in order to form an assembly having an interior. The powder material provides a mechanical obstacle to gas exchange between the interior and the environment. This assembly is then heat treated.

A sintered body obtainable by a process which includes pressing a powder comprising or consisting of at least one valve metal so as to provide a pellet, providing the pellet together with a reducing agent so that the pellet is not in a direct contact with and does not come into a direct contact with the reducing agent, heating so that the powder in the pellet is sintered to form a sintered body, an oxygen content of the at least one valve metal within the sintered body is simultaneously reduced, and the reducing agent is oxidized to an oxidized reducing agent, and removing the oxidized reducing agent with at least one mineral acid.

A method for making a sputtering target including steps of encapsulating and hot isostatically pressing at least one mass of metal powder (e.g., tantalum), having a particle size ranging from about 10 to about 1000 m, with at least about 10 percent by weight of particles having a particle size greater than about 150 m (for example, about 29 to about 56 percent (e.g., about 35 to about 47 percent) by weight of the particles in the at least one mass of metal powder having a particle size that is larger than 150 microns, but below about 250 m), for defining at least a portion of a sputtering target body, having an essentially theoretical random and substantially uniform crystallographic texture.

A method is provided in which a lower box comprising a base, walls that surround the base and an open side, and an upper box comprising a cover, walls that surround the cover and an open side are provided. One or more objects are arranged on the base of the lower box. The object(s) are covered with the upper box such that the open side of the upper is oriented towards the base of the box, the walls of the upper box are arranged on the base of the lower box and a gap is formed between the walls of the upper box and the walls of the lower box. A powder material is introduced into the gap in order to form an assembly having an interior. The powder material provides a mechanical obstacle to gas exchange between the interior and the environment. This assembly is then heat treated.