A method for producing a biodegradable magnesium metal composite that includes a polycrystalline magnesium matrix and TiB.sub.2 grains which are homogenously distributed in the polycrystalline magnesium matrix involving spark plasma sintering a milled mixture of magnesium powder and TiB.sub.2 powder. The temperature, pressure, and time of the spark plasma sintering used in the method are used to give high microharness, macrohardness, and density with low porosity by limiting the grain growth in the composite. The method yields a biodegradable magnesium metal composite having an improved microhardness, macrohardness, density, and porosity compared to other composites and methods of making composites.

Certain exemplary embodiments can provide a manufacturing method, process, machine, and/or system for continuously consolidating granular materials, creating new alloys and/or composites, and/or modifying and/or refining material microstructure, by using plastic deformation of feedstock(s) provided in various structural forms. Materials produced during this process can be fabricated directly and/or in forms such as, e.g., wires, rods, tubes, sheets, plate and/or channels, etc.

The present invention relates to an alloy with formula of RE-M-B—Fe as defined herein and oxygen content less than 0.9 wt %, wherein said RE is in the range of 29.0 weight % to 33.0 weight %; M is in the range of 0.25 weight % to 1.0 weight %; B is in the range of 0.8 weight % to 1.1 weight %; and Fe makes up the balance. The present invention also relates to a method for preparing a RE-M-Fe—B magnetic powder, as defined herein comprising the steps of: (a) melt spinning a RE-M-Fe—B alloy composition to obtain a melt-spun powder; (b) pressing the melt-spun powder of step (a) to obtain a compact body; (c) hot deforming the compact body of step (b) to obtain a die-upset magnet; (d) crushing the die-upset magnet of step (c) to obtain a powder; (e) milling and sieving the powder of step (d); and (f) passivating the powder of step (e) to obtain a magnetic powder; wherein: each of steps (d) to (f) is performed under a low oxygen environment and transfer between each of steps (d) to (f) is a sealed transfer; and wherein the oxygen content of the low oxygen environment and during each sealed transfer is below 0.5 weight %.

The present invention pertains to a process for preparing particles of rare earth sulfide comprising the steps of:—preparing a reaction mixture comprising at least one compound comprising at least one rare earth element (A) and at least one alkali metal sulfide (B),—submitting said reaction mixture to a mechanical stress so as to cause a chemical reaction that produces the particles of rare earth sulfide.

The present invention pertains to a process for preparing particles of rare earth sulfide comprising the steps of:—preparing a reaction mixture comprising at least one compound comprising at least one rare earth element (A) and at least one alkali metal sulfide (B),—submitting said reaction mixture to a mechanical stress so as to cause a chemical reaction that produces the particles of rare earth sulfide.

A method for producing hard metal powder suitable for manufacturing hard metal products including metal carbides and a binder is provided. An easy to carry out method that provides high quality hard metal powder includes: a) dissolving in water, water soluble raw materials and a binder source to form an aqueous solution, b) drying the aqueous solution to form a precursor powder having the raw materials homogenously distributed throughout the precursor powder, c) decomposing the precursor powder by heating the powder in an inert atmosphere to remove gas evolved in the decomposition of the raw materials, d) grinding the precursor powder and mixing it with a liquid media to produce a suspension, e) spray drying the suspension to agglomerate the precursor powder, and f) heat treating the agglomerated precursor powder to form a hard metal powder containing agglomerates of carbides evenly distributed and bonded to a metallic matrix.

An oxide dispersion-strengthened (ODS) iron-based alloy powder and a characterization method thereof are provided. The alloy powder comprises a matrix and strengthening phases. The strengthening phases include at least two types of strengthening phase particles with different sizes, wherein a volume of the particles with a particle size of less than or equal to 50 nm accounts for 85-95% of a total volume of all the strengthening phase particles. The matrix is a Fe—Cr—W—Ti alloy. The characterization method of the ODS iron-based alloy powder comprises separating the strengthening phases from the powder matrix through electrolysis, and analyzing and characterizing the strengthening phases using an electron microscope.

An oxide dispersion-strengthened (ODS) iron-based alloy powder and a characterization method thereof are provided. The alloy powder comprises a matrix and strengthening phases. The strengthening phases include at least two types of strengthening phase particles with different sizes, wherein a volume of the particles with a particle size of less than or equal to 50 nm accounts for 85-95% of a total volume of all the strengthening phase particles. The matrix is a Fe—Cr—W—Ti alloy. The characterization method of the ODS iron-based alloy powder comprises separating the strengthening phases from the powder matrix through electrolysis, and analyzing and characterizing the strengthening phases using an electron microscope.

Provided is an Fe—Pt—BN-based sputtering target that has a high relative density and that suppresses particle generation.

The Fe—Pt—BN-based sputtering target has, as a residue after dissolution in aqua regia measured by a procedure below, the particle size distribution in which D90 is 5.5 μm or less and a proportion of fine particles smaller than 1 μm is 35% or less. The procedure includes: (1) cutting out an about 4 mm-square sample piece from the sputtering target, followed by pulverizing to prepare a pulverized product; (2) classifying the pulverized product using sieves of 106 μm and 300 μm in opening size and collecting a powder that has passed through the 300 μm sieve and remained on the 106 μm sieve; (3) immersing the powder in aqua regia heated to 200° C. to prepare a residue-containing solution in which the powder has been dissolved; (4) filtering the residue-containing solution through a 5A filter paper specified in JIS P 3801 and drying a residue on the filter paper at 80° C. to prepare a residue powder; (5) dispersing the residue powder in water containing a surfactant to prepare a sample solution; and (6) setting the sample solution in a particle size analyzer and measuring the particle size distribution.

Provided is an Fe—Pt—BN-based sputtering target that has a high relative density and that suppresses particle generation.

The Fe—Pt—BN-based sputtering target has, as a residue after dissolution in aqua regia measured by a procedure below, the particle size distribution in which D90 is 5.5 μm or less and a proportion of fine particles smaller than 1 μm is 35% or less. The procedure includes: (1) cutting out an about 4 mm-square sample piece from the sputtering target, followed by pulverizing to prepare a pulverized product; (2) classifying the pulverized product using sieves of 106 μm and 300 μm in opening size and collecting a powder that has passed through the 300 μm sieve and remained on the 106 μm sieve; (3) immersing the powder in aqua regia heated to 200° C. to prepare a residue-containing solution in which the powder has been dissolved; (4) filtering the residue-containing solution through a 5A filter paper specified in JIS P 3801 and drying a residue on the filter paper at 80° C. to prepare a residue powder; (5) dispersing the residue powder in water containing a surfactant to prepare a sample solution; and (6) setting the sample solution in a particle size analyzer and measuring the particle size distribution.