A method for producing nanoparticulate compressed tablets/pellets from synthetic and/or natural materials, and compressed tablets/pellets produced using the method for producing nanoparticulate compressed tablets/pellets from synthetic and/or natural materials and to uses thereof.

The present invention involves a graphene-containing rare earth permanent magnet material and preparation method thereof. The graphene-containing rare earth permanent magnet material, comprising: 20.6 to 23.4 weight percent of neodymium, 6.6 to 7.5 weight percent of praseodymium, 0.95 to 1.20 weight percent of boron, 0.4 to 0.6 weight percent of cobalt, 0.11 to 0.15 weight percent of copper, 2.0 to 2.4 weight percent of lanthanum, 1.7 to 2.1 weight percent of cerium, 1 to 5 weight percent of graphene, a remainder being iron. The graphene-containing rare earth permanent magnet material exhibits excellent temperature resistance, good conductivity and magnet properties even without any heavy rare earth elements like terbium or dysprosium, which dramatically reduces the cost, promotes the efficient utilization of rare earth resources and improves product quality. The preparation method within this invention is simple to realize, easy to control, cost-effective and has high production efficiency and stable product performances.

A sintered Nd—Fe—B magnet comprising at least one light rare earth element having a weight content between 31 wt. % and 35 wt. %, at least one heavy rare earth element having a weight content of no more than 0.2 wt. %, B having a weight content between 0.95 wt. % and 1.2 wt. %, at least one additive including Ti and having a weight content between 1.31 wt. % and 7.2 wt. %, Fe as a balance, and impurities including C, O, and N. Ti has a weight content between 0.3 wt. % and 1 wt. % and forms a Titanium-Iron-Boron phase with Fe and Boron B and being present in the sintered Nd—Fe—B magnet between 0.86 vol. % and 2.85 vol. %. The C, O, and N satisfy 630 ppm≦1.2C+0.6O+N≦3680 ppm. The sintered Nd—Fe—B magnet has a squareness factor of at least 0.95.

A sintered Nd—Fe—B magnet comprising at least one light rare earth element having a weight content between 31 wt. % and 35 wt. %, at least one heavy rare earth element having a weight content of no more than 0.2 wt. %, B having a weight content between 0.95 wt. % and 1.2 wt. %, at least one additive including Ti and having a weight content between 1.31 wt. % and 7.2 wt. %, Fe as a balance, and impurities including C, O, and N. Ti has a weight content between 0.3 wt. % and 1 wt. % and forms a Titanium-Iron-Boron phase with Fe and Boron B and being present in the sintered Nd—Fe—B magnet between 0.86 vol. % and 2.85 vol. %. The C, O, and N satisfy 630 ppm≦1.2C+0.6O+N≦3680 ppm. The sintered Nd—Fe—B magnet has a squareness factor of at least 0.95.

A method of forming a super hard polycrystalline construction comprises forming a liquid suspension of a first mass of nano-ceramic particles and a mass of particles or grains of super hard material having an average particle or grain size of 1 or more microns, dispersing the particles or grains in the liquid suspension to form a substantially homogeneous suspension, drying the suspension to form an admix of the nano-ceramic and super hard grains or particles, and forming a pre-sinter assembly comprising the admix. The pre-sinter assembly is then sintered to form a body of polycrystalline super hard material comprising a first fraction of super hard grains and a second fraction, the nano-ceramic particles forming the second fraction.

The super hard grains are spaced along at least a portion of the peripheral surface by one or more nano-ceramic grains, the super hard grains having a greater average grain size than that of the grains in the second fraction which have an average size of less than around 999 nm.

A method of forming a super hard polycrystalline construction comprises forming a liquid suspension of a first mass of nano-ceramic particles and a mass of particles or grains of super hard material having an average particle or grain size of 1 or more microns, dispersing the particles or grains in the liquid suspension to form a substantially homogeneous suspension, drying the suspension to form an admix of the nano-ceramic and super hard grains or particles, and forming a pre-sinter assembly comprising the admix. The pre-sinter assembly is then sintered to form a body of polycrystalline super hard material comprising a first fraction of super hard grains and a second fraction, the nano-ceramic particles forming the second fraction.

The super hard grains are spaced along at least a portion of the peripheral surface by one or more nano-ceramic grains, the super hard grains having a greater average grain size than that of the grains in the second fraction which have an average size of less than around 999 nm.

A method of forming a super hard polycrystalline construction comprises forming a liquid suspension of nano-sized super hard particles and particles of super hard material having an average particle or grain size of 1 or more microns, dispersing the particles in the liquid suspension to form a substantially homogeneous suspension which is then dried and sintered to form a body of polycrystalline super hard material comprising a first and second fractions of super hard grains, the nano-sized particles forming the second fraction. The super hard grains in the first fraction are bonded along at least a portion of the peripheral surface(s) thereof to at least a portion of a plurality of nano-sized grains in the second fraction, the grains in the first fraction having a greater average grain size than that of the grains in the second fraction which is less than 999 nm, the average grain size of the first fraction being around 1 micron or more

A method of forming a super hard polycrystalline construction comprises forming a liquid suspension of nano-sized super hard particles and particles of super hard material having an average particle or grain size of 1 or more microns, dispersing the particles in the liquid suspension to form a substantially homogeneous suspension which is then dried and sintered to form a body of polycrystalline super hard material comprising a first and second fractions of super hard grains, the nano-sized particles forming the second fraction. The super hard grains in the first fraction are bonded along at least a portion of the peripheral surface(s) thereof to at least a portion of a plurality of nano-sized grains in the second fraction, the grains in the first fraction having a greater average grain size than that of the grains in the second fraction which is less than 999 nm, the average grain size of the first fraction being around 1 micron or more

Disclosed are a rare-earth permanent magnet having improved magnetic properties and a method of manufacturing the same. A method of manufacturing a rare-earth permanent magnet may include: preparing a mixed powder including i) a first alloy represented by R1.sub.aR2.sub.bB.sub.cM.sub.dFe.sub.bal and ii) a second alloy represented by R2.sub.bB.sub.cM.sub.dFe.sub.bal where R1 is one or two or more of La, Ce, and Y; R2 is a rare-earth element except for La, Ce, and Y; and M is a metal element; press-forming and sintering the prepared mixed powder in a magnetic field to prepare a sintered body; and performing a heat treatment based on diffusion temperature conditions of an R1 component and an R2 component contained in the prepared sintered body.

Disclosed are a rare-earth permanent magnet having improved magnetic properties and a method of manufacturing the same. A method of manufacturing a rare-earth permanent magnet may include: preparing a mixed powder including i) a first alloy represented by R1.sub.aR2.sub.bB.sub.cM.sub.dFe.sub.bal and ii) a second alloy represented by R2.sub.bB.sub.cM.sub.dFe.sub.bal where R1 is one or two or more of La, Ce, and Y; R2 is a rare-earth element except for La, Ce, and Y; and M is a metal element; press-forming and sintering the prepared mixed powder in a magnetic field to prepare a sintered body; and performing a heat treatment based on diffusion temperature conditions of an R1 component and an R2 component contained in the prepared sintered body.