The measured value of a rubber temperature parameter that is related to the temperature of a rubber material to be kneaded by a mixing machine 2 and measured values of correlation parameters that have a correlation with a change in the value of the rubber temperature parameter are acquired. The measured values are assigned to an operational control parameter-calculation model equation, which is modified from a rubber temperature parameter-calculation model equation including operational control parameters and the correlation parameters, and a constant and coefficients of the operational control parameters and the correlation parameters are calculated using a machine learning algorithm. A predetermined operational control parameter, which is required in a case in which the rubber temperature parameter is controlled to a predetermined value, is calculated using an operational control parameter-calculation equation that is specified by the coefficients and the constant calculated using the machine learning algorithm.

The measured value of a rubber temperature parameter that is related to the temperature of a rubber material to be kneaded by a mixing machine 2 and measured values of correlation parameters that have a correlation with a change in the value of the rubber temperature parameter are acquired. The measured values are assigned to an operational control parameter-calculation model equation, which is modified from a rubber temperature parameter-calculation model equation including operational control parameters and the correlation parameters, and a constant and coefficients of the operational control parameters and the correlation parameters are calculated using a machine learning algorithm. A predetermined operational control parameter, which is required in a case in which the rubber temperature parameter is controlled to a predetermined value, is calculated using an operational control parameter-calculation equation that is specified by the coefficients and the constant calculated using the machine learning algorithm.

A method is disclosed for preparing and dispensing a mixture obtained by mixing at least one first chemically reactive component and at least one second chemically reactive component containing a dispersed solid material i.e. a filler, by a high pressure mixing device comprising a head provided with injectors and one or more interception and supply devices defined by respective nozzles for narrowing the passage of the flows and with correlated plug members that are movable axially and settable for controlling said narrowing. The injectors and the interception and supply device transform the pressure energy of the fluids into kinematic energy of the jets that clash in the mixing chamber to mix the components for turbulence induced by the jets, in which a valve member is slidable, in particular a slide-valve, provided with longitudinal slots for recirculating the components to respective storage tanks. The method provides: removing from at least one tank, by pumping arrangement connected to a respective hydraulic delivery line to the head, a dosed quantity of the at least second chemically reactive second component to with filler material is added; preventing, once said quantity is removed, that the second component flows back from the pumping arrangement to the tank; dosing the component with a controlled flowrate B to the delivery line to the mixing head; keeping the slide-valve closed in a recirculating position and preventing the entry of the at least second component to the head and to the respective recirculating slot and pressurizing, by a dosed quantity Vot, the delivery line to subject the at least second polymeric component to a pressure increase along the delivery line until a value is reached that is near that reached by the passage through the nozzle of the respective interception and supply device; subsequently enabling the entry of the second component into the head to make the second component recirculate to the slots of the slide-valve for a period of time that is comparatively very reduced until it is reduced virtually to zero with respect to a recirculating step of the at least first component through the slide-valve, and subsequently opening by retracting the slide-valve to permit mixing by high pressure collision of the first and at least one second components to dispense the resulting mixture through the mixing chamber and the dispensing conduit for pouring the mixture into a cavity or into a shape to make an object by reaction of the aforesaid first and second chemically reactive components. An apparatus for preparing and dispensing the mixture is also disclosed.

A method is disclosed for preparing and dispensing a mixture obtained by mixing at least one first chemically reactive component and at least one second chemically reactive component containing a dispersed solid material i.e. a filler, by a high pressure mixing device comprising a head provided with injectors and one or more interception and supply devices defined by respective nozzles for narrowing the passage of the flows and with correlated plug members that are movable axially and settable for controlling said narrowing. The injectors and the interception and supply device transform the pressure energy of the fluids into kinematic energy of the jets that clash in the mixing chamber to mix the components for turbulence induced by the jets, in which a valve member is slidable, in particular a slide-valve, provided with longitudinal slots for recirculating the components to respective storage tanks. The method provides: removing from at least one tank, by pumping arrangement connected to a respective hydraulic delivery line to the head, a dosed quantity of the at least second chemically reactive second component to with filler material is added; preventing, once said quantity is removed, that the second component flows back from the pumping arrangement to the tank; dosing the component with a controlled flowrate B to the delivery line to the mixing head; keeping the slide-valve closed in a recirculating position and preventing the entry of the at least second component to the head and to the respective recirculating slot and pressurizing, by a dosed quantity Vot, the delivery line to subject the at least second polymeric component to a pressure increase along the delivery line until a value is reached that is near that reached by the passage through the nozzle of the respective interception and supply device; subsequently enabling the entry of the second component into the head to make the second component recirculate to the slots of the slide-valve for a period of time that is comparatively very reduced until it is reduced virtually to zero with respect to a recirculating step of the at least first component through the slide-valve, and subsequently opening by retracting the slide-valve to permit mixing by high pressure collision of the first and at least one second components to dispense the resulting mixture through the mixing chamber and the dispensing conduit for pouring the mixture into a cavity or into a shape to make an object by reaction of the aforesaid first and second chemically reactive components. An apparatus for preparing and dispensing the mixture is also disclosed.

Provided is a cross-linked rubber that can improve long-term sealing properties of a seal member in high-temperature and high-pressure environments. The cross-linked rubber is obtained through cross-linking of a cross-linkable rubber composition containing a fluororubber, carbon black, one or more carbon nanotubes, and an organic peroxide cross-linker, and has a 50% modulus of 5 MPa or more, a compression set (230° C., 500 hours) of 80% or less, and a rate of change of elongation at break between before and after a heat aging test (230° C., 72 hours) of not less than −10% and not more than 10%.

The present invention relates to a production system for manufacturing of formulations, comprising a unit (1). The unit (1) includes a subunit (1.1) which includes a combination of a process mixer and a buffer tank, means of feeding defined amounts of feedstocks into the process mixer, a measurement unit for ascertaining properties of a part-batch of a formulation manufactured in the process mixer, an evaluation unit for determining a deviation of properties of the part-batches manufactured in the process mixer from the properties of a predefined target state, and a unit for adjusting the feed of feedstocks in view of the deviations. The present invention also relates to a process for manufacturing formulations.

The present invention relates to a production system for manufacturing of formulations, comprising a unit (1). The unit (1) includes a subunit (1.1) which includes a combination of a process mixer and a buffer tank, means of feeding defined amounts of feedstocks into the process mixer, a measurement unit for ascertaining properties of a part-batch of a formulation manufactured in the process mixer, an evaluation unit for determining a deviation of properties of the part-batches manufactured in the process mixer from the properties of a predefined target state, and a unit for adjusting the feed of feedstocks in view of the deviations. The present invention also relates to a process for manufacturing formulations.

It is described an apparatus for the extrusion and mixing of plastic materials, for example rubber-based and silicone-based materials, comprising a dump extruder body whereon two conical screws (2) converging towards an extrusion die (3) suitable for being occluded by closing means (4) are mounted, the conical screws (2) being accommodated within a low-pressure compounding chamber (1) and within a pair of converging conical channels also defining a high-pressure chamber (2′), said low-pressure chamber (1) corresponding to an upstream area with respect to an extrusion direction, wherein said high-pressure chamber (2′) and/or said low-pressure chamber (1) accommodate a presser body (5, 5′, 6), defining a movable wall suitable for causing a controlled change in the volume of the respective chamber (1, 2′).

A method for producing a powder comprising at least one polymer for use in a method for the additive manufacture of a three-dimensional object is described. The method includes the step of mechanically treating the powder in a mixer with at least one rotating mixing blade, wherein the powder is exposed to a temperature T.sub.B and T.sub.B is at least 30° C. and is below the melting point T.sub.m of the polymer (determined according to DIN EN ISO 11357) if the polymer is a semi-crystalline polymer, or wherein T.sub.B is at least 30° C. and wherein T.sub.B is at most 50° C. above the glass transition temperature T.sub.g of the polymer (determined according to DIN EN ISO 11357) if the polymer is a melt-amorphous polymer. Compared to a time before the start of the treatment, it may be achieved that after the treatment, the bulk density of the powder is increased by at least 10% (or in the case of polymer, copolymer or polymer blend of polyamide at least 2% and more) and the BET surface area is decreased by at least 10%, and optionally also the pourability is improved by at least 10%.

A method of forming a polyethylene terephthalate (PET) mixture with talc includes: providing a feed of PET (PET feed); providing a feed of talc (talc feed); mixing the feed of PET with the feed of talc in a mixer at a PET:talc ratio of about 3:1 to about 1:3 to form a PET/talc mixture; and providing the PET/talc mixture as output. A method of forming a Polyethylene Terephthalate (PET) alloy having talc includes: providing a feed of the PET/talc mixture (PET/talc feed); providing a feed of PET (PET feed); mixing the feed of PET with the feed of PET/talc in a mixer to form a PET alloy having from about 1% (w/w) talc to about 50% talc (w/w); and providing the PET alloy as output.