B01J19/126

MICROWAVE-ASSISTED CATALYTIC REACTIONS USING MODIFIED BED PARTICLES
20200223692 · 2020-07-16 ·

A modified bed particles, related methods and applications in processes involving microwave-assisted catalytic reactions. The bed particles modified to be used as a microwave receptor that is capable to simultaneously sustain heat generation mechanisms under microwave irradiations and physically act as catalyst support. The bed particle comprises a dielectric coating deposited on an external surface of a core, the bed particle being sized for use in a fixed bed reactor or a fluidized bed reactor. The bed particles may further comprise a catalytically active material supported on a surface of the dielectric coating. Irradiating the gas-solid reactor with microwaves enables heating the dielectric coating of the solid bed particles, the dielectric coating locally transferring thermal energy to the surrounding gaseous reactants which are thereby selectively converted into the primary products.

Processing apparatus

A processing apparatus includes a microwave processing chamber. In addition, the processing apparatus includes a rigid, rotatable feed wheel rotatable about an axis of rotation such that a part of the feed wheel is located within the processing chamber. Further, the processing apparatus includes a feed device configured to deposit materials to be processed onto the feed wheel. Still further, the processing apparatus includes an output into which processed materials from the feed wheel can be deposited.

Method and device for the plasma-catalytic conversion of materials
10702847 · 2020-07-07 ·

Methods and devices are provided for the plasma-catalytic conversion of materials to produce chemical base materials. The methods and devices allow a plurality of chemical processes to be carried out in a plasma-catalytic manner to produce chemical base materials from simple raw materials (for example methane and biogas) with an improved selectivity and energy balance. A hydrocarbon-containing or other starting material is reacted under the action of a plasma to produce chemical base materials, or such a starting material is converted into an intermediate product in a first step under the action of a plasma, and the intermediate product is converted into the desired base material in a subsequent step. The devices for carrying out plasma-catalytic reactions are characterized by a jet pump arranged downstream of the plasma reactor, a tubular recipient (reaction chamber) having a diameter of at least 4 cm, or a catalyst-containing wall of the recipient.

High temperature pressure digestion vessel system with dual action seal
10695738 · 2020-06-30 · ·

A vessel system for high-pressure reactions is disclosed. The system includes a plugged polymer cylinder reaction vessel with a pressure vent opening extending radially through the wall of the reaction vessel and a supporting frame into which the vessel is received. Complementing keying structure elements on the vessel and on the frame limit the orientation of the reaction vessel in the supporting frame and the radially extending vent opening to a defined single position.

MICROWAVE REACTOR AND MANUFACTURING METHOD OF BIODIESEL
20200179898 · 2020-06-11 ·

A microwave reactor includes a chamber, at least one microwave source, a sprayer and a vapor extractor. The chamber includes a containing space and a reacting space. The containing space is communicated with the reacting space and provided for containing a reactant. The microwave source is connected to one side wall of the reacting space of the chamber. The sprayer is communicated with the containing space of the chamber for turning the reactant into a mist and spraying the mist in the reacting space of the chamber. The vapor extractor is connected to the reacting space. When the water contained in the mist is gasified to produces a water vapor, the water vapor can be exhausted from the chamber by the vapor extractor.

Systems and methods for processing gases

The invention includes a gas processing system for transforming a hydrocarbon-containing inflow gas into outflow gas products, where the system includes a gas delivery subsystem, a plasma reaction chamber, and a microwave subsystem, with the gas delivery subsystem in fluid communication with the plasma reaction chamber, so that the gas delivery subsystem directs the hydrocarbon-containing inflow gas into the plasma reaction chamber, and the microwave subsystem directs microwave energy into the plasma reaction chamber to energize the hydrocarbon-containing inflow gas, thereby forming a plasma in the plasma reaction chamber, which plasma effects the transformation of a hydrocarbon in the hydrocarbon-containing inflow gas into the outflow gas products, which comprise acetylene and hydrogen. The invention also includes methods for the use of the gas processing system.

METHOD FOR PREPARING GRAPHENE-TIN OXIDE NANOCOMPOSITE, AND GRAPHENE-TIN OXIDE NANOCOMPOSITE

A method of manufacturing a graphene-tin oxide nanocomposite comprises dispersing graphene and tin oxide in an organic solvent to prepare a dispersion solution, drying the dispersion solution to obtain a powdery mixture, and irradiating the mixture with microwaves to obtain a graphene-tin oxide nanocomposite. Irradiation of graphene and tin oxide with microwaves results in the simplification of the manufacturing process of graphene-tin oxide nanocomposites and a decrease in manufacturing time and cost, and produce graphene-tin oxide nanocomposites at low temperatures. Further, the graphene-tin oxide nanocomposite with improved sensitivity to NO2 gas may be produced.

Ferromagnetic-particle manufacturing apparatus

A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including a single mode cavity that resonates with a microwave of a predetermined wavelength; a microwave oscillator electrically connected to the single mode cavity and configured to introduce the microwave of a predetermined wavelength into the single mode cavity; a pipe disposed to pass linearly through an inside of the single mode cavity, the pipe being formed of a dielectric material; and a pump configured to introduce, from one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; and reacting the reaction liquid in the pipe, introduced by the pump, by introducing the microwave into the single mode cavity so as to generate the ferromagnetic-particle in the pipe.

Ferromagnetic-particle manufacturing apparatus

A method for manufacturing a ferromagnetic-particle includes preparing a manufacturing apparatus including an induction heating coil; a radiofrequency power source electrically connected to the induction heating coil and configured to form an alternating field inside the induction heating coil; a pipe disposed to pass through the induction heating coil, in which at least a partial area of the pipe in an axial direction thereof is formed of a dielectric material and an area, which is nearer to one end of the pipe than the area formed of a dielectric material, is formed of a conductive material; and a pump configured to introduce, from the one end of the pipe, an alkaline reaction liquid in which metal ions of a ferromagnetic metal and hydroxide ions are dissolved; reacting the reaction liquid in the pipe, introduced by the pump, by forming an alternating field inside the induction heating coil; and generating the ferromagnetic-particle in the pipe based on the reaction of the reaction liquid in the pipe.

Autoclave and method for welding thermoplastic composite parts
10654021 · 2020-05-19 · ·

An autoclave for welding thermoplastic composite parts comprises a sealed process chamber, a pressure source, a microwave source and a workpiece supporting member configured to support at least two thermoplastic composite parts which contact each other in an abutting section within the process chamber. The pressure source is configured to generate positive pressure in the process chamber which is higher than an ambient pressure surrounding the process chamber while the microwave source emits microwaves towards the abutting section in order to locally melt the thermoplastic composite parts and weld them together in the region of the abutting section.