B01J19/126

Chemical reaction apparatus

In order to provide a chemical reaction apparatus that can suppress a situation where microwaves are concentrated on a partial portion in a reactor, and that can more uniformly irradiate a content with the microwaves, a chemical reaction apparatus includes: a horizontal flow-type reactor in which a liquid content horizontally flows with an unfilled space being provided thereabove; a microwave generator that generates microwaves; and a waveguide that transmits the microwaves generated by the microwave generator to the unfilled space in the reactor, wherein a top of the reactor is curved with respect to a flow direction of the content.

Systems And Methods For Carbon Dioxide Conversion
20230182105 · 2023-06-15 ·

The invention includes a system for producing a carbon dioxide conversion product, where the system includes a carbon dioxide gas source providing carbon dioxide; a delivery system for the carbon dioxide in fluid communication with the carbon dioxide gas source, wherein the delivery system delivers the carbon dioxide gas into a plasma reactor, and wherein the plasma reactor energizes the carbon dioxide gas as a plasma to produce activated carbon dioxide species; a secondary reactant source providing a secondary reactant in a secondary reactant stream that is separated from the carbon dioxide gas, wherein the secondary reactant stream is directed to contact the activated carbon dioxide species in a reaction zone, and wherein the contact between the activated carbon dioxide species and the secondary reactant in the reaction zone produces a reaction that yields the carbon dioxide conversion product. The invention also includes methods of the use of such a system for producing a carbon dioxide conversion product.

Systems and Methods for Nitrogen Fixation
20230182104 · 2023-06-15 ·

The invention includes a system for producing a nitrogen fixation product, where the system includes a nitrogen gas source providing nitrogen gas; a delivery system for the nitrogen gas in fluid communication with the nitrogen gas source, wherein the delivery system delivers the nitrogen gas into a plasma reactor, and wherein the plasma reactor energizes the nitrogen gas as a plasma to produce activated nitrogen species; a secondary reactant source providing a secondary reactant in a secondary reactant stream that is separated from the nitrogen gas, wherein the secondary reactant stream is directed to contact the activated nitrogen species in a reaction zone, and wherein contact between the activated nitrogen species and the secondary reactant produces a reaction that yields the nitrogen fixation product. The invention also includes methods of the use of such a system for producing a nitrogen fixation product.

SYSTEMS AND METHODS FOR SELECTIVE REDOX REACTIONS
20230182106 · 2023-06-15 ·

The invention includes systems for producing a selective oxidation product that include an oxidant gas source providing an oxidizing agent; a delivery system for the oxidizing agent in fluid communication with the oxidant gas source, wherein the delivery system delivers the oxidizing agent into a plasma reactor, and wherein the plasma reactor energizes the oxidizing agent as a plasma to produce activated oxidant species; a secondary reactant source providing a secondary reactant in a secondary reactant stream that is separated from the oxidant gas, wherein the secondary reactant stream is directed to contact the activated oxidant species in a reaction zone, and wherein the contact between the activated oxidant species and the secondary reactant in the reaction zone produces a reaction that yields the selective oxidation product.

Microwave methods for converting hydrocarbon-based waste materials into oil and gas fuels

A portable, sustainable, and efficient system and apparatus for breaking down processed solid plastic waste and other polymer-based feedstock into fuel oil, sustainable energy, carbon char, and other useful products. With minor modifications, biomass can also be treated. Distributed microwave heating sources and mechanical mixing effectively mix heat in a highly insulated reactor that protects the microwave components, makes fast pyrolysis possible, and thereby enables scaling down to compact and highly portable systems. Products include diesel, gasoline, propane, butane, and char. Product materials are distributed using tight temperature control and mechanical routing.

Microwave-based thermal coupling chemical looping gasification method employing two sources, and device for same

A microwave-based thermal coupling chemical looping gasification method and device. The device includes: a microwave radiation cavity; a loading recess of a microwave absorbing material; and a quartz pipe reaction cavity between the microwave radiation cavity and the loading recess of a microwave absorbing material. A microwave generator consisting of magnetrons is provided at a central portion of the microwave radiation cavity and below the loading recess. An infrared temperature-measuring probe group is arranged at two ends of the magnetrons. Two ends of the microwave radiation cavity are connected to a first and second three-way valves, in communication with the ambient atmosphere and a protection gas charging device. A protection gas cooling device and a protection gas circulating fan are sequentially connected in series on a pipeline between the valves.

Pressure vessel with flushing device

The invention relates to a pressure vessel, having: a reaction chamber (2) as a pressure space for the initiation and/or facilitation of chemical and/or physical pressure reactions of samples (P) accommodated in the reaction chamber (2); a fluid inlet (20) with a feed valve (21) which is adjustable between an open position, for the feed of a fluid, preferably a flushing gas, into the reaction chamber (2), and a closed position, for stopping the feed of the fluid; a fluid outlet (30) with a discharge valve (31), which is adjustable between an open position, for the discharge of a fluid out of the reaction chamber (2), and a closed position, for stopping the discharge of the fluid out of the reaction chamber (2); and an oxygen sensor (33) for detecting an oxygen content in the reaction chamber (2). The pressure vessel (1) furthermore has a control device which is configured to control the feed valve (21) and the discharge valve (31) on the basis of the oxygen content detected by the oxygen sensor (33), such that the reaction chamber (2) is flushed via the feed and discharge valves (21, 31) situated in the open position, and at least the discharge valve (31) switches from the open position into the closed position as soon as a predetermined oxygen content is undershot. The invention also relates to a corresponding method.

Electromagnetic hydrocarbon depolymerization process

Applying electromagnetic energy to a hydrocarbon feed in the presence of at least one of a solvent, a catalyst, an electromagnetic receptor or a hydrogenation agent may result in depolymerization and compositional modification of the hydrocarbon feedstock into at least one of smaller hydrocarbon product fractions or viscosity modification.

Microwave-Induced Non-Thermal Plasma Conversion of Hydrocarbons

A non-thermal plasma is generated to selectively convert a precursor to a product. More specifically, plasma forming material and a precursor material are provided to a reaction zone of a vessel. The reaction zone is exposed to microwave radiation, including exposing the plasma forming material and the precursor material to the microwave radiation. The exposure of the plasma forming material to the microwave radiation selectively converts the plasma forming material to a non-thermal plasma including formation of one or more streamers. The precursor material is mixed with the plasma forming material and the precursor material is exposed to the non-thermal plasma including exposing the precursor material to the one or more streamers. The exposure of the precursor material to the streamers and the microwave radiation selectively converts the precursor material to a product.

Microwave chemical processing
09812295 · 2017-11-07 · ·

Methods and systems include supplying pulsed microwave radiation through a waveguide, where the microwave radiation propagates in a direction along the waveguide. A pressure within the waveguide is at least 0.1 atmosphere. A supply gas is provided at a first location along a length of the waveguide, a majority of the supply gas flowing in the direction of the microwave radiation propagation. A plasma is generated in the supply gas, and a process gas is added into the waveguide at a second location downstream from the first location. A majority of the process gas flows in the direction of the microwave propagation at a rate greater than 5 slm. An average energy of the plasma is controlled to convert the process gas into separated components, by controlling at least one of a pulsing frequency of the pulsed microwave radiation, and a duty cycle of the pulsed microwave radiation.