A fluidized gas reactor includes a system for preventing a fluidizing gas comprising a reactant from premature reaction. The fluidized gas reactor includes a reaction chamber including a particle bed; a gas distribution plate having a plurality of openings therethrough, wherein each opening opens into the reaction chamber; and a plurality of vertical fluidizing gas inlet tubes, each of the fluidizing gas inlet tubes being in fluid communication with one of the openings in the gas distribution plate. Each fluidizing gas inlet tube is configured to receive a fluidizing gas and transport the fluidizing gas to the reaction chamber. A fluidizing gas source provides a stream of the fluidizing gas to the fluidizing gas inlet tubes. A coolant system prevents the fluidizing gas from undergoing reaction before entering the reaction chamber. The coolant system has a fluid inlet; a coolant flow path in fluid communication with the fluid inlet, the coolant flow path being configured to cool each fluidizing gas inlet tube; and a fluid outlet in fluid communication with the coolant flow path. Each fluidizing gas inlet tube may include a particle outlet and a valve system, where the valve system allows the fluidizing gas flow to the fluidizing gas inlet tubes to be stopped; and allows recovery of particles from the particle bed while the fluidizing gas flow is stopped.

A method and arrangement of producing polymer comprising polymerizing in reactor having a top zone having a generally conical shape, a middle zone in direct contact with and below said top zone having a generally cylindrical shape, a bottom zone having a generally conical shape thereby polymerizing at least one olefin, in the presence of a polymerization catalyst and fluidization gas to obtain (i) a first stream comprising fluidization gas and particles of olefin polymer, (ii) a second stream comprising fluidization gas and agglomerates of olefin polymer, (iii) a third olefin polymer product streamdirecting the first stream comprising fluidization gas and olefin polymer particles to a series of at least three cyclones connected to the fluidized bed reactorseparating agglomerates of olefin polymer from the second stream, withdrawing from the fluidized bed polymerization reactor the third olefin polymer product stream.

Disclosed is a catalyst pre-contact method for the continuous polymerization of an olefin, wherein a primary catalyst, a co-catalyst and, optionally, an external electron donor are mixed and then undergo a pre-contact reaction, with the pre-contact reaction temperature being 30 C. to 35 C. and adjustable, and the pre-contact reaction time being 0.5 min to 10 min and adjustable, and the pre-contacted catalyst is brought into a catalyst prepolymerization system and then into a catalyst polymerization system, or is directly brought into the catalyst polymerization system. Further disclosed is a catalyst pre-contact device for the continuous polymerization of an olefin, which can adjust the pre-contact time and pre-contact temperature of the catalyst so that the performance of the catalyst achieves a better level according to the process.

A fluidized bed reactor includes a gas distributor, a tapered section above the gas distributor, and an expanded head above the tapered section. The gas distributor defines a plurality of inlets surrounding a product withdrawal tube, which extends away from the fluidized bed reactor. The fluidized bed reactor is useful in a process for fluidizing relatively large particles, such as Geldart Group B particles and/or Geldart Group D particles, where said particles are in a bubbling fluidized bed residing, in whole or in part, in the tapered section. The fluidized bed reactor and process may be used for manufacturing polycrystalline silicon.

A solid powder reactor includes: a reaction kettle, including a hollow kettle body and covers; an agitating device, including an agitating shaft and blades, wherein the agitating shaft is arranged in the kettle body and the blades are fixed on the agitating shaft; and a heating system, including a kettle body heater and an agitating heater, wherein the kettle body heater is fixed on the kettle body and the agitating heater is arranged on the agitating device. While the agitating device and the kettle body are driven to agitate, by a driving device fixedly arranged outside the reaction kettle, the heating system heats materials in the reactor. The present invention is applicable to solid reaction of solid powders. The materials containing attached water or not are both feasible, and the materials can directly enter the reactor and react. Compared with conventional solid reactors, the present invention increases the production efficiency.

This invention relates to a robotic device 10.1, 10.2 and method for handling catalyst material 106, 206 in a reactor 100 by removing spent catalyst from the reactor and/or loading the reactor with fresh catalyst without an operator having to enter an interior of the reactor which increases operator safety. The robotic device includes a body 12, which is configured to engage a flange 104 of the reactor, and a handling arm which is configured for use both as a cleaning arm 18 and a loading arm 218. The handling arm is connected to the body and is angularly and longitudinally displaceable relative to the body. The handling arm has a segment which is telescopically extendible/retractable relative to the body. When used as a cleaning arm, the arm receives a vacuum line for removing catalyst. When used as a loading arm, a telescopic loading sleeve is connected to the segment.

A fluidized bed reactor includes a gas distributor, a tapered section above the gas distributor, and an expanded head above the tapered section. The gas distributor defines a plurality of inlets surrounding a product withdrawal tube, which extends away from the fluidized bed reactor. The fluidized bed reactor is useful in a process for fluidizing relatively large particles, such as Geldart Group B particles and/or Geldart Group D particles, where said particles are in a bubbling fluidized bed residing, in whole or in part, in the tapered section. The fluidized bed reactor and process may be used for manufacturing polycrystalline silicon.

Polyolefin polymerization performed by contacting in a reactor an olefin monomer and optionally a comonomer with a catalyst system in the presence of induced condensing agents (ICA) and optionally hydrogen. The ICA may include two or more ICA components where the composition of the ICA (i.e., the concentration of each ICA component) may affect the polyolefin production rate. Changes to the relative concentration of the two or more ICA components may be according to ICA equivalency factors that allow for increasing the polyolefin production rate while maintain a sticking temperature, increasing polyolefin production rate while increasing the dew point approach temperature of the ICA, or a combination thereof.

The number of small gels that form in polyolefin thin films may be reduced by altering certain production parameters of the polyolefin. In some instances, the number of small gels may be influenced by the melt index of the polyolefin. However, in many instances, melt index is a critical part of the polyolefin product specification and, therefore, is not manipulated. Two parameters that may be manipulated to mitigate small gel count while maintaining the melt index are polyolefin residence time in the reactor and ICA concentration in the reactor.

A fluidized bed reactor includes a gas distributor, a tapered section above the gas distributor, and an expanded head above the tapered section. The gas distributor defines a plurality of inlets surrounding a product withdrawal tube, which extends away from the fluidized bed reactor. The fluidized bed reactor is useful in a process for fluidizing relatively large particles, such as Geldart Group B particles and/or Geldart Group D particles, where said particles are in a bubbling fluidized bed residing, in whole or in part, in the tapered section. The fluidized bed reactor and process may be used for manufacturing polycrystalline silicon.