The present invention generally relates to a microwave-assisted pyrolysis system comprised of a microwave chamber body (102); a black carbon platform (104) disposed inside the microwave chamber body for irradiating microwave radiation and absorbing microwave energy; a quartz microwave reactor (106) placed on the black carbon platform for receiving chemical precursor(s) and applying microwave irradiation for absorption of microwave energy thereby heating the black carbon platform for microwave-assisted pyrolysis of the received chemical precursor(s); a cooling unit (108) employed for regulating and maintaining a user-defined temperature level upon detecting the temperature inside the microwave reactor using a temperature sensor (110), if the temperature exceeds the optimum level, wherein the optimum temperature is defined on the type of precursors undergoing pyrolysis; and wherein if the heating temperature is raised extremely high, the cooling unit inside the microwave machine gets activated to bring down the temperature to the user-defined level.

The present invention relates to a pressure vessel (1) for receiving samples (P) to be heated, having a reaction chamber (2) as a pressure space for the initiation and/or facilitation of chemical and/or physical pressure reactions, the reaction chamber (2) being designed for receiving a liquid (5), a magnetic disk (8) mounted rotatably about an axis of rotation in the reaction chamber (2), and a magnet arrangement (10), provided outside the reaction chamber (2), for generating a rotating magnetic field for rotationally driving the magnetic disk (8) about its axis of rotation, the magnetic disk (8) having at least one passage bore (13), which extends transversely in relation to the axis of rotation and is provided in such a way that liquid (5) received in the reaction chamber (2) is driven through the passage opening (13) by rotation of the magnetic disk (8) in order to stir the liquid (5).

A device for rapidly preparing β-Si3N4 by gas-solid reaction and a method thereof, and relates to the technical field of recycling and reuse of waste fine silicon powder. The bottom of a stock bin communicates with a first opening and closing passage, a first connection passage, and the top of a first transitional bin; the bottom of the first transitional bin communicates with the first opening and closing passage, a second connection passage, and the top of a reaction bin; the bottom of the reaction bin communicates with a second opening and closing passage, the first connection passage, and the top of a second transitional bin; the bottom of the second transitional bin communicates with the top of a conveying passage through the first opening and closing passage; a material outlet of the conveying bin communicates with the collection bin.

Disclosed are single atom dispersions and multi-atom dispersions, and systems and methods for synthesizing the atomic dispersions. An exemplary method of synthesizing atomic dispersions includes: positioning a loaded substrate which includes a substrate in which is loaded with at least one of: a precursor of an element or a cluster of an element, applying one or more temperature pulses to the loaded substrate where a pulse of the temperature pulse(s) applies a target temperature for a duration, maintaining a cooling period after the pulse, and providing single atoms of the element dispersed on the substrate after the one or more temperature pulses. The target temperature applied by the pulse is between 500 K and 4000 K, inclusive, and the duration is between 1 millisecond and 1 minute, inclusive.

A fluid treatment device with a new configuration is provided. The fluid treatment device is provided with an upstream treatment unit defined by treatment surfaces that rotate relative to each other, and a downstream treatment unit arranged downstream of the upstream treatment unit. The upstream treatment unit is configured such that, by passing the fluid to be treated into an upstream treatment space defined by the treatment surfaces, the fluid to be treated is subjected to upstream treatment. The downstream treatment unit is provided with a downstream treatment space which performs the function of retaining and mixing the fluid to be treated by means of a labyrinth seal. An upstream outlet of the fluid to be treated from the upstream treatment unit opens into the downstream treatment space, and the downstream treatment space is configured to use the labyrinth seal to perform the function of controlling retention time. The downstream treatment space is provided with narrow seal spaces, and retention spaces arranged upstream of the seal spaces and wider than the seal spaces, and the upstream outlet opens to a retention space.

A stirrer includes a magnetic bar and a microwave absorbing layer around the magnetic bar. The stirrer absorbs a microwave and converts the microwave to thermal energy to heat the mixed solution reactant.

Synthesizing upconverting nanoparticles includes heating a precursor solution comprising one or more rare earth salts, an alkali metal salt or alkaline earth salt, and a solvent comprising a plasticizer in a microwave reactor to yield a product mixture, and cooling the product mixture to yield the upconverting nanoparticles. Core-shell upconverting nanoparticles are synthesized by combining the upconverting nanoparticles with a precursor solution comprising one or more rare earth salts, an alkali metal salt or alkaline earth salt, and a solvent comprising a plasticizer to yield a nanoparticle mixture, heating the nanoparticle mixture in a microwave reactor to yield a product mixture, and cooling the product mixture to yield the core-shell upconverting nanoparticles.

A large capacity natural material composition conversion apparatus using a microwave with a preset pressure function includes a chamber including a sealed reaction space accommodating a material, an radiator configured to heat the material by radiating a microwave into the reaction space, a pressure regulator configured to regulate a pressure of the reaction space by supplying a gas into the reaction space, and a controller configured to control the pressure regulator and the radiator, and preliminarily increase a pressure of the reaction space by controlling the pressure regulator before heating the material.

The present invention provides a microwave pyrolysis reactor (1) comprising an inner pipe element (2) and a housing (4), wherein the inner pipe element (2) is made of a microwave transparent material and is arranged within the housing and comprises a first open end (5) and a second open end (6); the housing (4) comprises a first inner surface, enclosing an annular space (7,44) around the inner pipe element (2), a waste inlet (10), a solids outlet (11), a gas outlet (12), and a port (13) for a microwave waveguide (14), the waste inlet and the solids outlet are in communication with the first open end and the second open end of the inner pipe element, respectively, and the port for a microwave waveguide is in communication with the annular space; the inner pipe element, the waste inlet and the solids outlet of the housing form parts of a conduit not in fluid communication with the annular space around the inner pipe element and wherein the inner pipe element is clamped within the housing via a cylinder-shaped resilient assembly (54) arranged at at least one of the first open end (5) and the second open end of the inner pipe element, the resilient assembly is adapted to allow longitudinal expansion of the inner pipe element (2) and comprises a central through-going passage (57) having a centerline in line with a centerline (C) of the inner pipe element.

A reactor for converting hydrogen sulfide into hydrogen gas and sulfur.