A method of manufacturing synthesis gas by catalytic partial oxidation can prevent formation of hot spots from taking place when driving mixture gas to pass through a catalyst-filled layer at high velocity. The method comprises converting mixture gas of source gas containing lower hydrocarbons and oxidative gas containing oxygen into synthesis gas containing hydrogen and carbon monoxide as main components thereof by causing mixture gas to flow through a fixed bed catalyst layer arranged in a reactor. The method of manufacturing synthesis gas by catalytic partial oxidation is conducted such that the mixture gas is made to flow to the catalyst layer under the condition that the Reynolds number does not exceed 20 at the inlet of the catalyst layer.

The present disclosure relates to a manufacturing plant for high-pressure polymerization having a layered tubular reactor and a method for an emergency shutdown in said manufacturing plant. The present disclosure also relates to a process for manufacturing LDPE using said layered tubular reactor.

The present disclosure relates to a manufacturing plant for high-pressure polymerization having a layered tubular reactor and a method for an emergency shutdown in said manufacturing plant. The present disclosure also relates to a process for manufacturing LDPE using said layered tubular reactor.

The present invention relates to a process for the preparation of an alkanesulfonic acid by oxidation of a sulfur containing starting compound with an oxygen containing fluid, wherein the sulfur containing starting compound is provided in a reaction system, comprising a reaction vessel (1) with an expansion vessel (2) on its top, wherein the reaction vessel and the expansion vessel are connected to allow a flow of a fluid stream from the reaction vessel into the expansion vessel.

Systems and methods are disclosed for detecting temperature excursion in a chemical plant or petrochemical plant or refinery. Aspects of the disclosure provide an enhanced control system for a reactor, such as in hydroprocessing. The enhanced control system may provide early warnings of impending undesirable events, directly or indirectly manipulate certain process variables to reduce undesirable outcomes, and/or directly or indirectly manipulate of certain process variables so as to place a reactor unit in a safe park state. This may avoid a high temperature trip, depressuration, associated operating risks, allow for faster recovery from temperature excursions, and/or avoid unplanned emergency shutdowns of the reactor, chemical process, plant, or refinery.

The invention provides apparatus and method of pyrolysing feedstock to produce char. A feedstock advancing mechanism in a lower portion of a substantially sealed reaction chamber advances the feedstock laterally along the lower portion as it pyrolyses in its progression from the proximal end to the distal end. Char is discharged from the distal end of the reaction chamber. A control system controls at least the flow rate of oxygen containing gas entering the chamber via the inlet port in response to the temperature measurements in the reaction chamber so that the temperature measurements are appropriate for the production of char from the feedstock and so that a zone of volatile gas combustion is established in the headspace, involving essentially complete consumption of all incoming free oxygen in the headspace without contacting the feedstock.

A device for carrying out a chemical reaction by a continuous method has a reactor with at least two reactor sections which define a direction of flow. The reactor has plug flow properties along the direction of flow. A recirculation line is present to withdraw a partial flow from the reactor at a first point and return it to the reactor at a second point located above the first point in the direction of flow. Means are provided which prevent a temperature increase in the reactor over a predetermined temperature range, for example change of more than approximately 50 K.

Described herein are improved chemical reactors for carrying out partial oxidation reactions. The chemical reactor permits the use of levels of oxygen above the lower explosion limit (LEL) typically used in partial oxidation reactions, which increases both volumetric reactivity and conversion per pass, resulting in reduced separation and reactant recycle costs. Also described are methods of using the reactors.

The invention provides a method for producing a peroxymonosulfuric acid solution with high stability, including the steps of mixing 35 mass % or more of hydrogen peroxide and 70 mass % or more of sulfuric acid to react them, cooling the reaction solution to 80 C. or lower within five minutes after initiation of the mixing step, and diluting the reaction solution with water four times or more as much as the reaction solution by mass.

A method of manufacturing synthesis gas by catalytic partial oxidation can prevent formation of hot spots from taking place when driving mixture gas to pass through a catalyst-filled layer at high velocity. The method comprises converting mixture gas of source gas containing lower hydrocarbons and oxidative gas containing oxygen into synthesis gas containing hydrogen and carbon monoxide as main components thereof by causing mixture gas to flow through a fixed bed catalyst layer arranged in a reactor. The method of manufacturing synthesis gas by catalytic partial oxidation is conducted such that the mixture gas is made to flow to the catalyst layer under the condition that the Reynolds number does not exceed 20 at the inlet of the catalyst layer.